• Composites Research
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• v.19 no.4
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• pp.7-14
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• 2006

Interfacial shear strength between epoxy and carbon fiber has been analyzed utilizing the microbond specimen with an epoxy micro-droplet adhered onto single carbon fiber. The interfacial shear stress distributions along the fiber/matrix interface were calculated by finite element analysis using three kinds of finite element models such as droplet model, circular-crosssection model and pull-out model. Conclusions were obtained as follows. (1) Interfacial shear stress distribution showed that larger stresses were concentrated in the fiber/matrix interface for microbond test than for pull-out test. Thus, debonding at the fiber/matrix interface during microbond test was liable to occur at low load level. (2) Microbond test showed higher interfacial strength which was caused by various effects of micro-droplet geometry and size as well as stress concentration in the region contacting with the micro-vise tip.

• Korean Journal of Materials Research
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• v.23 no.2
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• pp.149-153
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• 2013

Delamination crack detection is very important for improving the structural reliability of laminated composite structures. This requires real-time delamination detection technologies. For composite laminates that are reinforced with carbon fiber, an electrical potential method uses carbon fiber for reinforcements and sensors at the same time. The use of carbon fiber for sensors does not need to consider the strength reduction of smart structures induced by imbedding sensors into the structures. With carbon fiber reinforced (CF/) epoxy matrix composites, it had been proved that the delamination crack was detected experimentally. In the present study, therefore, similar experiments were conducted to prove the applicability of the method for delamination crack detection of CF/polyetherethereketone matrix composite laminates. Mode I and mode II delamination tests with artificial cracks were conducted, and three point bending tests without artificial cracks were conducted. This study experimentally proves the applicability of the method for detection of delamination cracks. CF/polyetherethereketone material has strong electric resistance anisotropy. For CF/polyetherethereketone matrix composites, a carbon fiber network is constructed, and the network is broken by propagation of delamination cracks. This causes a change in the electric resistance of CF/polyetherethereketone matrix composites. Using three point bending specimens, delamination cracks generated without artificial initial cracks is proved to be detectable using the electric potential method: This method successfully detected delamination cracks.

• Composites Research
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• v.36 no.4
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• pp.259-263
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• 2023

This study investigated the open hole tensile (OHT) properties of carbon fiber/epoxy composites and compared them to bolt joint tensile (BJT) properties. The net nominal modulus and strength (1376 MPa) were found to be higher than the gross nominal strength (1041 MPa), likely due to increasing hole size. The OHT and BJT specimens exhibited similar stiffness, as expected without bolt rotation causing secondary bending. OHT specimens experienced a sharp drop in stress indicating unstable crack propagation, delamination, and catastrophic failure. BJT specimens failed through shear out on the bolt side and bearing failure on the nut side, involving fiber kinking, matrix splitting, and delamination, resulting in lower strength compared to OHT specimens. The strength retention of carbon fiber/epoxy composites with open holes was 66%. Delamination initiation at the hole's edge caused a reduction in the stress concentration factor. Filling the hole with a bolt suppressed this relieving mechanism, leading to lower strength in BJT specimens compared to OHT specimens. Bolt joint efficiency was calculated as 15%. The reduction in strength in bolted joints was attributed to fiber-matrix splitting and delamination, aligning with Hart Smith's bolted joint efficiency diagram. These findings contribute to materials selection and structural reliability estimation for carbon fiber/epoxy composites. They highlight the behavior of open hole and bolt joint configurations under tensile loading, providing valuable insights for engineering applications.

• Composites Research
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• v.31 no.6
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• pp.293-298
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• 2018

In this paper, we have studied the physical properties of braided composites for use as aircraft stringers. Process variables such as drum winder speed, braid velocity, and mandrel diameter for $30^{\circ}$, $45^{\circ}$ and $60^{\circ}$ braid preforms were quantified and different epoxy resin types were applied to the braided preform using TGDDM, YD-128. Physical properties such as tensile strength and flexural strength of braided composites were investigated. Thermal properties and decomposition temperature of epoxy resin were investigated by TGA analysis. As a result, the lower the angle of the braid composites, the higher the tensile strength and the Flexural strength. The physical properties of braided composites fabricated using TGDDM epoxy resin were superior to the physical properties of braided composites fabricated using YD-128 epoxy resin. This is because the molecular weight of TGDDM epoxy resin was higher than that of YD-128 epoxy resin.

• Composites Research
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• v.28 no.3
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• pp.94-98
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• 2015

This paper reports the effects of nickel film interleaves on the interlaminar shear strength(ILSS) of carbon fiber reinforced epoxy composites(CFRPs). A nickel thin film was deposited onto the prepreg by radio frequency(RF) sputtering at room temperature. The ILSS of the nickel film interleaved hybrid composites was increased compared to that of the composites without interleaves. To understand the mechanism of enhancement of the ILSS, the fracture surface of the tested specimens was examined by scanning electron microscopy(SEM). The metal interleaves were acted as a reinforcement for the matrix rich interface and the shear property of their composites improved by enhancing the resistance to matrix cracking.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2000.11a
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• pp.79-83
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• 2000

Interfacial and microfailure properties of carbon liber/bismaleimide (BMI) composites were evaluated using both tensile fragmentation and compressive Broutman tests with acoustic emission (AE). Since BMI is rather difficult matrix to apply for the conventional fragmentation test because of its too low elongation and too brittle and high modulus properties, dual matrix composite system was applied. After carbon fiber/BMI composite was prepared for rod shape by controlling differing curing stage, composites rod was embedded in toughened epoxy as outer matrix. The typical microfailure modes including fiber break, matrix cracking, and interlayer failure were observed during tensile testing, whereas the diagonal slippage in fiber ends was observed during compressive test. On the other hand, AE amplitudes of BMI matrix fracture were higher than carbon fiber tincture under tensile test because BMI matrix has very brittle and high modulus. The waveform of signals coming from BMI matrix fractures was consistent with AE amplitude result under tensile tests.

• Journal of the Korean Society of Safety
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• v.34 no.6
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• pp.1-6
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• 2019

Carbon fiber has excellent specific strength, corrosion resistance and heat resistance. And p-Aramid fiber has high toughness and heat resistance and high elasticity, and is used in various fields such as industrial protective materials, bulletproof helmets and vests, as well as industrial fields. However, carbon fiber is relatively expensive, and is susceptible to brittle fracture behavior due to its low fracture strain. On the other hand, the aramid fiber tends to decrease in elastic modulus and strength when applied to the epoxy matrix, but it is inexpensive and has higher elongation and fracture toughness than carbon fiber. Thus the twill hybrid carbonaramid fiber reinforced composite laminate composite was investigated for a delamination fracture toughness under Mode I loading by 2 kinds of MBT and MCC deduction. The specimen was fabricated with 20 hybrid fabric plies. The initial crack was made by inserting the teflon tape in the center plane with a₀/W=0.5 length. The results show that SERR(Strain Energy Release Rate) as the critical and stable delamination fracture toughness were 0.09 kJ/㎡, 0.386 kJ/㎡ by MBT deduction, and 0.192 kJ/㎡, 0.67 kJ/㎡ by MCC deduction, respectively.

• Journal of the Korean Society for Railway
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• v.12 no.6
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• pp.1059-1066
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• 2009

Recently, the amount of thermosetting plastic wastes has increased with the production of reinforced plastic composites and causes serious environmental problems. The epoxy resins, one of the versatile thermosetting plastics with excellent properties, cannot be melted down and remolded as what is done in the thermoplastic industry. In this research, a series of experiments that decompose epoxy resin and recover carbon fibers from carbon fiber reinforced epoxy composites applied to railway vehicles was performed. We experimentally examined various decomposition processes and compared their decomposition efficiencies and mechanical property of recovered carbon fibers. For the prevention of tangle of recovered carbon fibers, each composites specimen was fixed with a Teflon supporter and no mechanical mixing was applied. Decomposition products were analyzed by scanning electron microscope (SEM), gas chromatography mass spectrometer (GC-MS), and universal testing machine (UTM). Carbon fibers could be completely recovered from decomposition process using nitric acid aqueous solution, liquid-phase thermal cracking and pyrolysis. The tensile strength losses of the recovered carbon fibers were less than 4%.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2000.11a
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• pp.12-16
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• 2000

This study is about the effect of braiding on the 2-D biaxial braided hollow composite(BD) compared with unidirectional hollow composite(UD). The specimens were made of T700S Carbon/Epoxy prepreg and T700S dried Carbon yarns. Fiber volume fraction of UD and BD was obtained experimentally and analytically. Fiber volume fraction of BD was derived based on unit cell of braiding yarn section. Bending test was executed to investigate the effect of braiding part. The result of experiment and analysis of fiber volume fraction has good agreement. Bending strength of BD is about 20% higher than that of UD.

• Carbon letters
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• v.19
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• pp.1-11
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• 2016

In efforts to characterize and understand the properties and processing of phenylethynyl-terminated imide (LaRC PETI-5, simply referred to as PETI-5) oligomers and polymers as a high-temperature sizing material for carbon fiber-reinforced polymer matrix composites, PETI-5 imidization and thermal curing behaviors have been extensively investigated based on the phenylethynyl end-group reaction. These studies are reviewed here. In addition, the use of PETI-5 to enhance interfacial adhesion between carbon fibers and a bismaleimide (BMI) matrix, as well as the dynamic mechanical properties of carbon/BMI composites, are discussed. Reports on the thermal expansion behavior of intercalated graphite flake, and the effects of exfoliated graphite nanoplatelets (xGnP) on the properties of PETI-5 matrix composites are also reviewed. The dynamic mechanical and thermal properties and the electrical resistivity of xGnP/PETI-5 composites are characterized. The effect of liquid rubber amine-terminated poly(butadiene-co-acrylonitrile) (ATBN)-coated xGnP particles incorporated into epoxy resin on the toughness of xGnP/epoxy composites is examined in terms of its impact on Izod strength. This paper provides an extensive overview from fundamental studies on PETI-5 and xGnP, as well as applied studies on relevant composite materials.