• Title/Summary/Keyword: Carbon Content Analysis

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A Study on Fatigue Characteristics and Analysis for A 182 F6a Class 4 Materials (A182 F6A Class4 재료의 피로특성과 피로해석에 대한 연구)

  • Jin-Kyung Lee
    • Journal of the Korean Society of Industry Convergence
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    • v.26 no.4_2
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    • pp.585-589
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    • 2023
  • Unlike general carbon steel, stainless steel's mechanical properties change depending on the content of chromium and nickel. In this study, since stainless steel for high-temperature pressure container parts is used as shafts, the fatigue strength and fatigue limit of the materials were evaluated using a rotational bending fatigue test. Meanwhile, fatigue analysis was conducted under the same conditions as the specimen for structural analysis and fatigue analysis of stainless steel for high-temperature pressure container parts. Using the fatigue analysis results, we tried to derive the life of the material and the safety factor for each part. As a result of performing a fatigue test by processing a specimen for the fatigue test of A182 F6A stainless steel, the fatigue limit was 548 MPa. The ratio between the tensile strength and fatigue limit of the material was 0.545, representing 54.5% of the tensile strength.

Research on the Dispersion Stability and Scale up of Carbon Slurry Fuel (카본슬러리 연료의 분산안정성 개선 및 scale up 제조연구)

  • Jo, Min-Ho;Yang, Mun-Kyu;Lee, Ik-Mo;Cho, Joon-Hyun;Kwon, Tae-Soo;Jeong, Byung-Hun;Han, Jeong-Sik
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2008.11a
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    • pp.459-462
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    • 2008
  • In manufacture of slurry fuel, the effects of process parameters on the carbon dispersion stability have been investigated. The particle size and contents of the carbon slurry taken from 3 (top, medium, bottom) positions in fuel reservoir were analyzed to estimate the dispersion of the carbon in Jet A-1. Through the application of various additives, it was found that NB463S84 additive showed the best dispersion and stability of carbon at accelerated gravity condition. The mixer performance was compared by the observation of height change of carbon-containing layer and measurement of particle sizes at the same conditions. Application of the mixing conditions obtained from the lab-scale to bench scale manufacture confirmed the practical feasibility of our research.

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Effect of Y2O3 Additive Amount on Densification of Reaction Bonded Silicon Carbides Prepared by Si Melt Infiltration into All Carbon Preform (완전 탄소 프리폼으로부터 Si 용융 침투에 의해 제조한 반응 소결 탄화규소의 치밀화에 미치는 Y2O3 첨가량의 영향)

  • Cho, Kyeong-Sik;Jang, Min-Ho
    • Korean Journal of Materials Research
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    • v.31 no.5
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    • pp.301-311
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    • 2021
  • The conversion of all carbon preforms to dense SiC by liquid infiltration can become a low-cost and reliable method to form SiC-Si composites of complex shape and high density. Reactive sintered silicon carbide (RBSC) is prepared by covering Si powder on top of 0.5-5.0 wt% Y2O3-added carbon preforms at 1,450 and 1,500℃ for 2 hours; samples are analyzed to determine densification. Reactive sintering from the Y2O3-free carbon preform causes Si to be pushed to one side and cracking defects occur. However, when prepared from the Y2O3-added carbon preform, an SiC-Si composite in which Si is homogeneously distributed in the SiC matrix without cracking can be produced. Using the Si + C = SiC reaction, 3C and 6H of SiC, crystalline Si, and Y2O3 phases are detected by XRD analysis without the appearance of graphite. As the content of Y2O3 in the carbon preform increases, the prepared RBSC accelerates the SiC conversion reaction, increasing the density and decreasing the pores, resulting in densification. The dense RBSC obtained by reaction sintering at 1,500 ℃ for 2 hours from a carbon preform with 2.0 wt% Y2O3 added has 0.20 % apparent porosity and 96.9 % relative density.

Carbon Source Affects Synthesis, Structures, and Activities of Mycelial Polysaccharides from Medicinal Fungus Inonotus obliquus

  • He, Huihui;Li, Yingying;Fang, Mingyue;Li, Tiantian;Liang, Yunxiang;Mei, Yuxia
    • Journal of Microbiology and Biotechnology
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    • v.31 no.6
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    • pp.855-866
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    • 2021
  • The effects of various carbon sources on mycelial growth and polysaccharide synthesis of the medicinal fungus Inonotus obliquus in liquid fermentation were investigated. After 12-d fermentation, mycelial biomass, polysaccharide yield, and polysaccharide content were significantly higher in Glc+Lac group (glucose and lactose used as combined carbon source) than in other groups. Crude polysaccharides (CIOPs) and the derivative neutral polysaccharides (NIOPs) were obtained from mycelia fermented using Glc, fructose (Fru), Lac, or Glc+Lac as carbon source. Molecular weights of four NIOPs (termed as NIOPG, NIOPF, NIOPL, and NIOPGL) were respectively 780.90, 1105.00, 25.32, and 10.28 kDa. Monosaccharide composition analyses revealed that NIOPs were composed of Glc, Man, and Gal at different molar ratios. The NIOPs were classified as α-type heteropolysaccharides with 1→2, 1→3, 1→4, 1→6 linkages in differing proportions. In in vitro cell proliferation assays, viability of RAW264.7 macrophages was more strongly enhanced by NIOPL or NIOPGL than by NIOPG or NIOPF, and proliferation of HeLa or S180 tumor cells was more strongly inhibited by NIOPG or NIOPGL than by NIOPF or NIOPL, indicating that immune-enhancing and anti-tumor activities of NIOPs were substantially affected by carbon source. qRT-PCR analysis revealed that expression levels of phosphoglucose isomerase (PGI) and UDP-Glc 4-epimerase (UGE), two key genes involved in polysaccharide synthesis, varied depending on carbon source. Our findings, taken together, clearly demonstrate that carbon source plays an essential role in determining structure and activities of I. obliquus polysaccharides by regulating expression of key genes in polysaccharide biosynthetic pathway.

Lipase-catalyzed Esterification of (S)-Naproxen Ethyl Ester in Supercritical Carbon Dioxide

  • Kwon, Cheong-Hoon;Lee, Jong-Ho;Kim, Seung-Wook;Kang, Jeong-Won
    • Journal of Microbiology and Biotechnology
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    • v.19 no.12
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    • pp.1596-1602
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    • 2009
  • A lipase-catalyzed esterification reaction of (S)-naproxen ethyl ester by CALB (Candida antarctica lipase B) enzyme was performed in supercritical carbon dioxide. Experiments were performed in a high-pressure cell for 10 h at a stirring rate of 150 rpm over a temperature range of 313.15 to 333.15 K and a pressure range of 50 to 175 bar. The productivity of (S)-naproxen ethyl ester was compared with the result in ambient condition. The total reaction time and conversion yields of the catalyzed reaction in supercritical carbon dioxide were compared with those at ambient temperature and pressure. The experimental results show that the conversion and reaction rate were significantly improved at critical condition. The maximum conversion yield was 9.9% (216 h) at ambient condition and 68.9% (3 h) in supercritical state. The effects of varying amounts of enzyme and water were also examined and the optimum condition was found (7 g of enzyme and 2% water content).

Study on Carbon Dioxide Storage through Mineral Carbonation using Sea Water and Paper Sludge Ash (해수와 제지슬러지소각재의 광물탄산화 반응을 이용한 이산화탄소 저장 연구)

  • Kim, Dami;Kim, Myoung-jin
    • Journal of the Korean Society for Marine Environment & Energy
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    • v.19 no.1
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    • pp.18-24
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    • 2016
  • Mineral carbonation is a technology for permanently storing carbon dioxide by reacting with metal oxides containing calcium and magnesium. In this study, we used sea water and alkaline industrial by-product such as paper sludge ash (PSA) for the storage of carbon dioxide through direct carbonation. We found the optimum conditions of both sea water content (mixing ratio of sea water and PSA) and reaction time required in the direct carbonation through various experiments using sea water and PSA. In addition, we compared the amounts of carbon dioxide storage with the cases when sea water and ultra-pure water were separately used as solvents in the direct carbonation with PSA. The amount of carbon dioxide storage was calculated by using both solid weight increase through the carbonation reaction and the contents of carbonate salts from thermal gravimetric analysis. PSA particle used in this study contained 67.2% of calcium. The optimum sea water content and reaction time in the carbonation reaction using sea water and PSA were 5 mL/g and 2 hours, respectively, under the conditions of 0.05 L/min flow rate of carbon dioxide injected at $25^{\circ}C$ and 1 atm. The amounts of carbon dioxide stored when sea water and ultra-pure water were separately used as solvents in the direct carbonation with PSA were 113 and $101kg\;CO_2/(ton\;PSA)$, respectively. The solid obtained through the carbonation reaction using sea water and PSA was composed of mainly calcium carbonate in the form of calcite and a small amount of magnesium carbonate. The solid obtained by using ultra-pure water, also, was found to be carbonate salt in the form of calcite.

Variation of the Physical Properties of Coal depending upon the Quality (탄질에 따른 석탄의 물성 변화)

  • Kwon, Byung Doo;Heo, Sik
    • Economic and Environmental Geology
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    • v.21 no.1
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    • pp.97-106
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    • 1988
  • The purpose of this study is to collect basic data which are prerequisite for quantitative analysis of coal logging data. The study involves laboratory measurements of physical properties such as seismic velocities (P,S-waves), resitivity and density of domestic and imported foreign coals. The relationships between these properties were analyzed by using cross-plots. Correlation between the physical properties of coal and the results of chemical analysis (calorie, fixed carbon, ash, moisture, volatile matter and sulfur contents) was also studied to obtain ideas about coal quality analysis using logging data. Summarized results are as follows: 1. $V_P$ is exponentialy related to $V_S$. And the average value of $V_P$ is about l.8 times as large as $V_S$. 2. Since coal has very low density compared with surrounding sedimentary rocks, density logging is appeared to be the best method for identifying coal seams and evaluating their qualities. 3. For the case of domestic coals, the ash contents and calorie show a perfect inverse relationship. Since the density increases as increase of ash content with a well-defined functional form, the ash content of domestic coals can be estimated by density measurements. 4. Because of low ash content, low density and high resistivity, foreign coals and domestic lignites are easily distinguished from domestic coals.

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Analysis of Cast Iron by Glow Discharge Emission Spectrometry (글로우 방전/방출분광분석법에 의한 주철시료의 분석)

  • Cho, K.H.;Woo, J.C.;Han, M.S.
    • Analytical Science and Technology
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    • v.6 no.3
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    • pp.297-305
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    • 1993
  • Generally, it is difficult to analyze cast iron samples with spark discharge emission spectrometry since the content of carbon in these samples is high as a few percent. The cast iron samples were analyzed with the developed glow discharge emission spectrometer composed of glow discharge emission source and polychromator. The discharge condition of glow discharge lamp(GDL) has been optimized by variation of Ar gas pressure, discharge voltage and discharge time. Under the optimum conditions obtained in this work, relationships between the measured emission intensities and concentration of two types of cast iron standard samples(BAS, LECO) were investigated. Most of elements(Mn, Si, P, S etc.) showed the good linearity in one calibration curve. And the carbon showed slightly the systematic difference according to the type of standard samples.

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버섯 배지를 이용한 tyrosinase 저해제 발효

  • Jung, Sung-Won;Han, Dae-Seok;Kim, Seok-Joong;Chun, Moon-Jin
    • Microbiology and Biotechnology Letters
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    • v.24 no.2
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    • pp.227-233
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    • 1996
  • Tyrosinase is an enzyme which catalyzes an enzymatic browning of some foods and in vivo synthesis of melanin. In order to produce natural and edible inhibitor of the enzyme which is expected to have whitening effect on melanogenesis, a microorganism was selected from fermented foods. It was named as NU-7, and cultured in mushroom (Lentinus edodes, Shiitake) media. Optimal media to produce tyrosinase inhibitor was formulated by varing nitrogen or carbon content. If glucose content was in a range of 3-20% and ammonium sulfate was in a range of 0-0.25%, production of inhibitor was independent of cell mass. Addition of ammonium sulfate as a nitrogen source had little effect on inhibitor production. Production of inhibitor (Y) was proportionally related to shiitake content (X) with a regression equation of Y= -0.96X$^{2}$ + 13.07X + 14.43 (R = 0.96). These results indicate that shiitake and glucose are necessary for the production of tyrosinase inhibitor. In the analysis of mycotoxin in culture broth, aflatoxin was not detected, suggesting that it would be probably edible.

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Analytical Method for Determination of the Content of Tire Wear Particle in Tire and Road Wear Particles

  • Son, Chae Eun;Choi, Sung-Seen
    • Elastomers and Composites
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    • v.56 no.1
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    • pp.1-5
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    • 2021
  • Tire and road wear particles (TRWPs) were collected from road dust and thermogravimetric analysis (TGA) was performed to measure the content of tire wear particles (TWPs) in the TRWPs. The TGA thermograms of TRWPs showed two weight loss steps associated with polymer decomposition including weight loss after 480℃ which may be due to road wear particles. Different samples gave different TGA thermograms because the types and contents of the road wear particles attached to the TWPs should be different from each other, and each TWP might have different composition. The TGA results of the model asphalt pavement wear particles, with (volatile organics + polymers + carbon black) : ash = 33.5 : 66.5, was applied to the TRWP results, and the TWP contents of TRWPs were found to be 50-65%. The zinc oxide content in the rubber compound was negligible.