• Journal of the Korean Society of Hazard Mitigation
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• v.7 no.5
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• pp.27-35
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• 2007

This study presents a non -prismatic beam element for modeling the elastic and inelastic behavior of the steel beam, which has the post-Northridge connections in steel moment frames that are subjected to earthquake ground motions. The elastic stiffness matrix for non-prismatic members with reduced beam section (RES) connection is in the closed-form. The plasticity model is of a discrete type and is composed of a series of nonlinear hinges connected by rigid links. The hardening rules can model the inelastic behavior for monotonic and random cyclic loading, and the effects of local buckling. Verification and calibration of the model are presented in a companion paper.

• Aerospace Engineering and Technology
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• v.11 no.2
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• pp.87-95
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• 2012

This technical paper describes the analysis results of telemetry data for the initial activation of star trackers for an agile high accuracy low earth orbit satellite. The satellite was recently launched and is in the Launch and Early Operation Phases. It uses two SED36 star trackers manufactured by SODERN. The star tracker is separated by three parts, an optical head, an electronics box, and a baffle with maintaining optical head base plate temperature 20 degC in order to achieve the better performance in low frequency error. This paper presents the initial activation status, requirements and performance, anomaly occurrence, and noise equivalent angle performance analysis during the mission mode by processing the telemetry data.

• Bulletin of the Korean Chemical Society
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• v.26 no.1
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• pp.115-118
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• 2005

The miniaturized NIR (Near-infrared) spectrometer has been utilized for the determination of water content (1-19% range) in ethanol that is the most popular organic solvent in pharmaceutical industries. It has many potential capabilities that can replace the conventional analyzers especially for the on-line measurement since it is compact, versatile and cost-effective. By using two dimensional (2D) correlation spectroscopy, it was preliminarily investigated to find any unforeseen spectral distortion among the spectra collected from the miniaturized spectrometer. The 2D study revealed that the spectral variation clearly followed the variation of water concentration without any spectral distortion or abnormality. PLS (Partial Least Squares) was employed to build the calibration model and the resulting prediction performance was acceptable and stable over several days. Even though the miniaturized NIR system was evaluated to fairly simple chemical matrix, the overall study demonstrates the sufficient feasibility for diverse practical and industrial applications.

• Analytical Science and Technology
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• v.15 no.5
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• pp.445-450
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• 2002

A sensitive gas chromatographic method has been established for the determination of total iodide in seawater as their volatile organic derivative. The method is based on the formation of 4-iodo-2,6-dimethylphenol with 2,6-dimethylphenol in matrix and a single-step extraction of the derivative with ethyl ether, which are then measured by gas chromatography-mass spectrometry (selected ion monitoring). Iodate in sea water was completely reduced to iodide with ascorbic acid and acetic acid. The detection limit was 0.1 ng/mL in seawater and the calibration curve showed good linearity with r=0.9997. The method was sensitive, reproducible and simple enough to permit the reliable routine analysis of total iodide in seawater. Total iodide in sea water was found about 30 ng/ml.

• Mass Spectrometry Letters
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• v.11 no.1
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• pp.10-14
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• 2020

Riboflavin is a water-soluble vitamin, which serves as a precursor to flavin mononucleotide and flavin adenine dinucleotide. This study aimed to develop a simple and rapid liquid chromatography-tandem mass spectrometry (LC-MS/MS) analysis for the quantification of riboflavin in the Beagle dog plasma. This method utilized simple protein precipitation with acetonitrile and ¹³C₄, ¹⁵N₂-riboflavin was used as an internal standard (IS). For chromatographic separation, a hydrophilic interaction liquid chromatography (HILIC) column was used with gradient elution. The mobile phase consisted of 0.1% (v/v) aqueous formic acid with 10 mM ammonium formate and acetonitrile with 0.1% (v/v) formic acid. Since riboflavin is an endogenous compound, 4% bovine serum albumin in phosphate buffered saline was used as a surrogate matrix to prepare the calibration curve. The quantification limit for riboflavin in the Beagle dog plasma was 5 ng/mL. The method was fully validated for its specificity, sensitivity, accuracy and precision, recovery, and stability according to the US FDA guidance. The developed LC-MS/MS method may be useful for the in vivo pharmacokinetic studies of riboflavin.

• The Korean Journal of Nuclear Medicine
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• v.29 no.1
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• pp.118-124
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• 1995

단일광자방출전산화 단층촬영술을 이용한 영상정보를 효과적으로 얻기 위하여 고려되어야 할 사항으로는 1) 조준기(collimator)의 선택, 2) 기질(matrix)의 크기, 3) 회전각의 수 (number of angles), 4) 360도 또는 180도 획득(acquisition), 5) continuous 또는 step& shoot, 6) 원형 또는 비원형회전 등이 있다. 저자들은 비원형회전으로 검체와 검출기 사이의 거리를 단축시킴으로써 직선성, 균일성, 대조도, 해상력에 미치는 영향을 알아보기 위하여 원형회전 방법과 비교하여 다음과 같은 결과를 얻었다. (1) 비원형회전을 하여도 균일성(uniformity)과 직선성(linearlity)을 유지한다. (2) 균일성, 대조도(contrast), 해상력(resolution)들이 비원형 회전을 한 경우에 보다 더 개선되었다. (3) 영상 획득시간은 비원형회전인 경우에 더 소요되었다. (매스캔 당 10분) 따라서 검사자는 영상 화질의 개선효과와 상반되는 보정(calibration)과 설치(set-up)에 소요되는 시간(매스캔당 10분이상)을 비교하여 자료획득(data acquisition) 회전방법을 선택하여야한다.

• Journal of Biosystems Engineering
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• v.14 no.4
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• pp.221-228
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• 1989

A data acquisition system was designed to measure the forces on a rolling coulter in three coordinated directions, angular velocity of the coulter and travel speed of a soil bin. The data acquisition system consisted of a dynamometer, speed transducers, a signal conditioner, an inter-face board, an Aim-65 microcomputer and a digital data recorder. Strain gages were attached on the surface of the dynamometer and connected to form three Wheatstone bridges, which measure the draft force, the vertical force and the side force on the coulter. An interaction among three dimensional forces was found during the calibration. A matrix procedure was used to correct the forces for this interaction. Rotary shaft encoders were mounted on the coulter and on the soil bin drive to measure the angular velocity of the coulter and the travel speed of the soil bin. The angular velocity and the travel speed were computed by counting the number of pulse signals from the rotary shaft encoders every 0.2 second. The digital signals from the rotary shaft encoders were connected to counters and the analog signals from the dynamometer, after passing through the signal conditioner, were connected to the A/D converter. The microcomputer programs, written in assembly language, were developed to read signals from the transducers, convert them to actual unit, display them upon request and record them on a sigital tape every 0.2 second.

• International Journal of CAD/CAM
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• v.9 no.1
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• pp.37-46
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• 2010

Existing methods for the registration of blurred images are efficient for the artificially blurred images or a planar registration, but not suitable for the naturally blurred images existing in the real image mosaic process. In this paper, we attempt to resolve this problem and propose a method for a distortion-free stitching of naturally blurred images for image mosaic. It adopts a multi-resolution and robust feature based inter-layer mosaic together. In each layer, Harris corner detector is chosen to effectively detect features and RANSAC is used to find reliable matches for further calibration as well as an initial homography as the initial motion of next layer. Simplex and subspace trust region methods are used consequently to estimate the stable focal length and rotation matrix through the transformation property of feature matches. In order to stitch multiple images together, an iterative registration strategy is also adopted to estimate the focal length of each image. Experimental results demonstrate the performance of the proposed method.

• Bulletin of the Korean Chemical Society
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• v.33 no.7
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• pp.2224-2228
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• 2012

This study describes the ability of capillary electrochromatography (CEC) for the determination of imidacloprid and carbendazim in tomato samples. A novel liquid crystal crown ether modified hybrid silica monolithic column was synthesized, characterized and developed as separation column for the first time. Baseline separation of imidacloprid and carbendazim could be achieved using a mobile phase containing 90% (v/v) 20 mmol/L phosphate buffer (pH 7.0) and 10% (v/v) acetonitrile. The matrix matched calibration curves were linear with correlation coefficient $r^2$ > 0.9998 in the range of 0.20-10.00 mg/L. The limits of detection for imidacloprid and carbendazim were 0.061 and 0.15 mg/kg, respectively, which were below the maximum residue limits established by the European Union as well as Codex Alimentarius. Average recoveries for imidacloprid and carbendazim varied from 101.6-108.0% with relative standard deviations lower than 6.3%. This method was applied to the analysis of tomatoes collected from local markets.

• Journal of Electrical Engineering and Technology
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• v.13 no.4
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• pp.1759-1768
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• 2018

The energy density, power density and ohm resistance of battery change significantly as results of battery aging, which lead to decrease in the accuracy of the equivalent model. A parameter identification method of the equivale6nt circuit model with 3 R-C branches based on the test database of battery life cycle is proposed in this paper. This database is built on the basis of experiments such as updating of available capacity, charging and discharging tests at different rates and relaxation characteristics tests. It can realize regular update and calibration of key parameters like SOH, so as to ensure the reliability of parameters identified. Taking SOH, SOC and T as independent variables, lookup table method is adopted to set initial value for the parameter matrix. Meanwhile, in order to ensure the validity of the model, the least square method based on variable forgetting factor is adopted for optimizing to complete the identification of equivalent model parameters. By comparing the simulation data with measured data for charging and discharging experiments of Li-ion battery, the effectiveness of the full life cycle database and the model are verified.