• Title/Summary/Keyword: Bulk samples

Search Result 528, Processing Time 0.038 seconds

Sintering and Microwave Properties of Ba Hexagonal Ferrite (Ba 육방정 페라이트의 소결 특성 및 마이크로파 특성)

  • Kim, Jae-Sik;Ryu, Ki-Won;Bae, Seon-Gi;Lee, Young-Hie
    • Proceedings of the KIEE Conference
    • /
    • 2009.07a
    • /
    • pp.1293_1294
    • /
    • 2009
  • The sintering and high frequency electro-magnetic properties of Ba-hexagonal ferrite were investigated. All samples of the Ba-hexagonal ferrite were prepared by the conventional mixed oxide method and sintered at $1150^{\circ}C$~$1400^{\circ}C$. From the X-ray diffraction patterns of sintered Ba-hexagonal ferrite, the $Ba_3Co_2Fe_{24}O_{41}$ phase was represented as main phase in the almost sintering conditions. The bulk densities with sintering temperature and decreased at $1400^{\circ}C$. The permittivity ($\varepsilon$') and loss tangent of permittivity ($\varepsilon$"/$\varepsilon$') of $Ba_3Co_2Fe_{24}O_{41}$ ceramics increased and decreased with sintering temperature, respectively. The permeability of $Ba_3Co_2Fe_{24}O_{41}$ ceramics decreased with sinteirng temperature. The loss tangent of permeability was not changed compared each other with sintering temperature. The bulk density of $Ba_3Co_2Fe_{24}O_{41}$ ceramics sintered at $1300^{\circ}C$ was 4.79 g/$cm^3$. The permittivity, loss tangent of permittivity and permeability, loss tangent of permeability were 19.896, 0.1718 and 14.218, 0.2046 at 210 MHz, respectively.

  • PDF

Densification of Copper Powders using High-pressure Torsion Process (고압비틀림 공정을 이용한 구리 분말의 치밀화)

  • Lee, Dong-Jun;Yoon, Eun-Yoo;Kang, Soo-Young;Lee, Jung-Hwan;Kim, Hyoung-Seop
    • Journal of Powder Materials
    • /
    • v.19 no.5
    • /
    • pp.333-337
    • /
    • 2012
  • In this study, electrolytic copper powders were consolidated by high-pressure torsion process (HPT) which is the most effective process to produce bulk ultrafine grained and nanocrystalline metallic materials among various severe plastic deformation processes. The bulk samples were manufactured by the HPT process at 2.5 GPa and 1/2, 1 and 10 turns. After 10 turns, full densification was achieved by high pressure with shear deformation and ultrafine grained structure (average grain size of 677 nm) was observed by electron backscatter diffraction and a scanning transmission electron microscope.

Evaluation of Material Characteristics with Sintering Temperature in Ti2AlC MAX Phase Material using Spark Plasma Sintering Method (방전플라즈마 소결법을 이용한 Ti2AlC Max Phase 소결체의 소결온도 변화에 따른 재료 특성 평가)

  • Lee, Chang-Hun;Baek, Gyung Rae;Jung, Hee Sang;Jeong, Young-Keun;Kang, Myung Chang
    • Journal of Powder Materials
    • /
    • v.22 no.3
    • /
    • pp.175-180
    • /
    • 2015
  • In this study, ternary compound Max Phase $Ti_2AlC$ material was mixed by 3D ball milling as a function of ball milling time. More than 99.5 wt% pure $Ti_2AlC$ was synthesized by using spark plasma sintering method at 1000, 1100, 1200, and $1300^{\circ}C$ for 60 min. The material characteristics of synthesized samples were examined with relative density, hardness, and electrical conductivity as a function of sintering temperature. The phase composition of bulk was identified by X-ray diffraction. On the basis of FE-SEM result, a terraced structures which consists of several laminated layers were observed. And $Ti_2AlC$ bulk material obtained a vickers hardness of 5.1 GPa at the sintering temperature of $1100^{\circ}C$.

Bulk 건조엽의 편평엽 발생양상과 이화학적 특성

  • 이철환;진점의;한철수
    • Journal of the Korean Society of Tobacco Science
    • /
    • v.20 no.2
    • /
    • pp.139-143
    • /
    • 1998
  • The occurrence and physico-chemical properties of flat leaves found in 1997 curing trial related to the prevention of occurrence of flat leaves at bulk curing of flue-cured tobacco were investigated and compared with those of normal leaves. Cured leaves of NC82 were separated into 4 classes of none, slight, fair and severe symptoms of flat leaf by the percentage of flattened parts to whole leaf area. The flat leaves were mostly found among the leaves of lower stalk position, and it was estimated that growth rate of lower leaves also influenced on the occurrence of flat leaves. In chromatic aberration of cured leaf, flat leaves showed remarkably lower b and L values than in those of normals but there was no difference in a value. On the other hand, in chemical analyses of flat leaf samples, nicotine, total sugar, ether extract and total nitrogen contents were decreased with the degree of flat symptoms. In physical properties, filling capacity of cured leaves was decreased with the degree of flat symptoms comparing with those of normal leaves, while shatter index was showed a reverse tendency, and then within the same leaf, flat parts were decreased in total sugar, ether extract and filling capacity compared with those of normal ones, but remarkably increased in shatter index, and there was no difference in nicotine and total nitrogen contents.

  • PDF

ISSR marker-assisted selection of male and female plants in a promising dioecious crop: jojoba (Simmondsia chinensis)

  • Sharma, Kuldeep;Agrawal, Veena;Gupta, Sarika;Kumar, Ravindra;Prasad, Manoj
    • Plant Biotechnology Reports
    • /
    • v.2 no.4
    • /
    • pp.239-243
    • /
    • 2008
  • Simmondsia chinensis (Link) Schneider, a multipurpose and monogeneric dioecious shrub from arid zones, has emerged as a cash crop all over the globe. Its seed propagation poses severe problems due to its male-biased population: the male:female ratio is 5:1. Investigations have been carried out to generate a sex-specific Inter-simple sequence repeat (ISSR) marker for the early detection of male and female plants. Of the 42 primers analysed with a bulk sample of pooled male DNA and a bulk sample of pooled female DNA, only one primer, UBC-807, produced a unique ~1,200 base-pair fragment in the male DNA. To validate this observation, this primer was re-tested with individual male and female samples from eight cultivars. A similar unique ~1,200 bp fragment was present in the male individuals of all eight cultivars and completely absent in the female individuals tested. This is the first report of the use of ISSR markers to ascertain sex in physiologically mature S. chinensis plants.

Equal Channel Angular Pressing of Rapidly Solidified Al-20 wt % Si Alloy Powder Extrudates (급속응고 Al-20 wt% Si 합금분말 압출재의 ECAP)

  • Yoon, Seung-Chae;Hong, Soon-Jik;Seo, Min-Hong;Quang, Pham;Kim, Hyoung-Seop
    • Journal of Powder Materials
    • /
    • v.11 no.2
    • /
    • pp.97-104
    • /
    • 2004
  • In this paper processing and mechanical properties of Al-20 wt% Si alloy was studied. A bulk form of Al-20Si alloy was prepared by gas atomizing powders having the powder size of 106-145 ${\mu}m$ and powder extrusion. The powder extrudate was subsequently equal channel angular pressed up to 8 passes in order to refine grain and Si particle. The microstructure of the gas atomized powders, powder extrudates and equal channel angular pressed samples were investigated using a scanning electron microscope and X-ray diffraction. The mechanical properties of the bulk sample were measured by compressive tests and a micro Victors hardness test. Equal channel angular pressing was found to be effective in matrix grain and Si particle refinement, which enhanced the strength and hardness of the Al-2OSi alloy without deteriorating ductility in the range of experimental strain of 30%.

The Strength of Sintered Body with the Composition and the Forming Process of LTCC Materials (LTCC 소재의 조성과 성형 공정에 따른 소결체의 강도 특성)

  • Gu, Sin Il;Shin, Hyo Soon;Yeo, Dong Hun;Nahm, Sahn
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • v.26 no.1
    • /
    • pp.27-32
    • /
    • 2013
  • According to the composition of LTCC material, though it was thought that bulk defect which was made in forming process effects on the densification during the sintering, it was not reported systemically. In this study, we evaluated crystal structure, 3 point bending strength, hardness and microstructure of the samples by uniaxial pressing and tape casting using the commercial powders of the crystallizing glass and the glass/ceramic composite. In the case of glass/ceramic composite, Viox-001 powder with residual glass in the sintering, 3 point bending strength was similar regardless of forming process due to fill the bulk defect by residual glass. In the case of crystallizing glass, MLS-22, because glass phase was small in the sintering, glass did not fill the pore in the sample by uniaxial pressing process, therefore, the 3 point bending strength of it was 167 MPa. However, the 3 point bending strength of the sample by tape casting was 352 MPa and much higher. Meanwhile, crystal structure and hardness were similar regardless of forming process.

Preparation and Drawing Property of Poly(vinyl alcohol) Film (폴리비닐알코올 필름의 제조 및 연신 특성)

  • Kim, Hun Min;Lee, Jungeon;Park, Jae Min;Park, Jae Hyeung;Choi, Jin Hyun;Yeum, Jeong Hyun
    • Textile Coloration and Finishing
    • /
    • v.33 no.3
    • /
    • pp.147-152
    • /
    • 2021
  • Bulk polymerization was used to produce poly(vinyl acetate) with different molecular weights, which were then saponified to prepare poly(vinyl alcohol) (PVA) with different molecular weights. With Pn of 2,060 and 3,240, the optimum film formation concentrations of PVA were found 7.5wt.% and 6.5wt.%, respectively. The drawing characteristics of the PVA film prepared at the optimum film formation concentrations were experimented, as well as the thermal characteristics of the PVA film based on the drawing ratio were observed. When the drawing velocity was fixed, it was found that the drawing ratios of all samples decreased as the heat band gap increased, and the melting temperature of the PVA film slightly increased as the drawing ratio increased regardless of the Pn of PVA.

Factors influencing the spatial distribution of soil organic carbon storage in South Korea

  • May Thi Tuyet Do;Min Ho Yeon;Young Hun Kim;Gi Ha Lee
    • Proceedings of the Korea Water Resources Association Conference
    • /
    • 2023.05a
    • /
    • pp.167-167
    • /
    • 2023
  • Soil organic carbon (SOC) is a critical component of soil health and is crucial in mitigating climate change by sequestering carbon from the atmosphere. Accurate estimation of SOC storage is essential for understanding SOC dynamics and developing effective soil management strategies. This study aimed to investigate the factors influencing the spatial distribution of SOC storage in South Korea, using bulk density (BD) prediction to estimate SOC stock. The study utilized data from 393 soil series collected from various land uses across South Korea established by Korea Rural Development Administration from 1968-1999. The samples were analyzed for soil properties such as soil texture, pH, and BD, and SOC stock was estimated using a predictive model based on BD. The average SOC stock in South Korea at 30 cm topsoil was 49.1 Mg/ha. The study results revealed that soil texture and land use were the most significant factors influencing the spatial distribution of SOC storage in South Korea. Forested areas had significantly higher SOC storage than other land use types. Climate variables such as temperature and precipitation had a relative influence on SOC storage. The findings of this study provide valuable insights into the factors influencing the spatial distribution of SOC storage in South Korea.

  • PDF

Strain induced/enhanced ferromagnetism in $Mn_3Ge_2$thinfilms

  • Dung, Dang Duc;Feng, Wuwei;Thiet, Duong Van;Sin, Yu-Ri-Mi;Jo, Seong-Rae
    • Proceedings of the Korean Vacuum Society Conference
    • /
    • 2010.02a
    • /
    • pp.135-135
    • /
    • 2010
  • In Mn-Ge equilibrium phase diagram, many Mn-Ge intermetallic phases can be formed with difference structures and magnetic properties. The MnGe has the cubic structure and antiferromagnetic(AFM) with Neel temperature of 197 K. The calculation predicted that the $MnGe_2$ with $Al_2Cu$-type is hard to separate between the paramagnetic(PM) states and the AFM states because this compound displays PM and AFM configuration swith similar energy. Mn-doped Ge showed the FM with Currie temperature of 285 K for bulk samples and 116 K for thin films. In addition, the $Mn_5Ge_3$ compound has hexagonal structure and FM with Curie temperature around 296K. The $Mn_{11}Ge_8$ compound has the orthorhombic structure and Tc is low at 274 K and spin flopping transition is near to 140 K. While the bulk $Mn_3Ge_2$ exhibited tetragonal structure ($a=5.745{\AA}$;$c=13.89{\AA}$) with the FM near to 300K and AFM below 150K. However, amorphous $Mn_3Ge_2$ ($a-Mn_3Ge_2$) was reported to show spin glass behavior with spin-glass transition temperature (Tg) of 53 K. In addition, the transition of crystalline $Mn_3Ge_2$ shifts under high pressure. At the atmospheric pressure, $Mn_3Ge_2$ undergoes the magnetic phase transition from AFM to FM at 158 K. The pressure dependence of the phase transition in $Mn_3Ge_2$ has been determined up to 1 GPa. The transition was found to occur at 1 GPa and 155 K with dT/dP=-0.3K/0.1 GPa. Here report that Ferromagnetic $Mn_3Ge_2$ thin films were successfully grown on GaAs(001) and GaSb(001) substrates using molecular beam epitaxy. Our result revealed that the substrate facilitates to modify magnetic and electrical properties due to tensile/compressive strain effect. The spin-flopping transition around 145 K remained for samples grown on GaSb(001) while it completely disappeared for samples grown on GaAs(001). The antiferromagnetism below 145K changed to ferromagnetism and remained upto 327K. The saturation magnetization was found to be 1.32 and $0.23\;{\mu}B/Mn$ at 5 K for samples grown on GaAs(001) and GaSb(001), respectively.

  • PDF