• Restorative Dentistry and Endodontics
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• 제29권4호
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• pp.353-364
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• 2004

The purpose of this study was to compare and to evaluate the combination use of 5 kinds of dentin adhesive systems and 5 kinds of composite resins using micro-shear bond test. Five adhesive systems (Prime & Bond NT (PBN). Onecoat bond (OC), Excite (EX), Syntac (SY), Clearfil SE bond (CS)) and five composite resins (Spectrum (SP), Synergy Compact (SC), Tetric Ceram (TC), Clearfil AP-X (CA), Z100 (Z1)) were used for this study ($5{\;}{\times}{\;}5{\;}={\;}25group$, n =14/group). The slices of horizontally sectioned human tooth were bonded with each bonding system and each composite resin, and tested by a micro-shear bond strength test. These results were analyzed statistically. The mean micro-shear bond strength of dentin adhesive systems were in order of CS (22.642 MPa), SY (18.368 MPa), EX (14.599 MPa). OC (13.702 MPa). PBN (12.762 MPa). The mean bond strength of self-etching primer system group (CS, SY) in dentin was higher than that of self-priming adhesive system groups (PBN, EX, OC) significantly (P<0.05). The mean bond strength of composite resins was in order of SP (19.008 MPa), CA (17.532 MPa). SC (15.787 MPa), TC (15.068 MPa). Z1 (14.678 MPa). Micro-shear bond strength of SP was stronger than those of other composite resins significantly (P < 0.05). And those of TC and Z1 were weaker than other composite resins significantly (P < 0.05). No difference was found in micro-shear bond strength of composite resin in self-etching primer adhesive system groups (CS, SY) statistically. However, there was significant difference of micro-shear bond strength of composite resin groups in self-priming adhesive systems group (PBN, EX, OC). The combination of composite resin and dentin adhesive system recommended by manufacturer did not represent positive correlation. It didn't seem to be a significant factor.

• Restorative Dentistry and Endodontics
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• 제21권1호
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• pp.280-288
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• 1996

The purpose of this study was to assess comparatively the shear bond strength on dentin of four dentin bonding agents used in conjunction with light-curing composite resins. Clearfil New Bond, Scotchbond Multipurpose Dentin Adhesive, All-Bond 2 and X-R Bond were applicated on labial dentin surfaces just below dentin - enamel juction of bovine incisor teeth. After shear bond strength testing with the universal testing machine, the bonding interface of the specimens were observed under light stereomicroscope. Following results were obtained. 1. The shear bond strength was high in the order of B,C,D,A and group B Scotchbond Multipurpose Dentine Adhesive revealed greater bond strength than Clearfil New Bond and X-R Bond. (p<.001) 2. When using ANOVA and Duncan's multiple range test, there were statistical differences among the four groups, except between group Band C,group D and A. 3. There was no relationship between mode of failure and shear bond strength.

• Restorative Dentistry and Endodontics
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• 제32권3호
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• pp.208-221
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• 2007

파괴 인성 실험은 상아질-복합레진 계면의 파절 저항성을 평가할 수 있는 임상적으로 신뢰 할 만한 방법이다. 본 연구의 목적은 상아질-레진 계면의 파괴인성과 미세인장결합강도를 측정하여 이 두 실험방법이 상아질-레진 결합을 평가하는 데 가지는 유용성을 비교, 평가하는 것이다 파괴 인성 측정에는 short-rod 시편 형태를 이용하였다. 각 시편에서는 소의 하악절치에서 절단한 치아 절편을 포함시켜 결합면을 얻었다. 미세인장 결합강도 또한 소의 하악절치 순면을 연마하여 상아질을 노출시킨 후 상아질 접착제를 도포하고 레진 블록을 축조하여 측정하였다. 각 시편들은 $37^{\circ}C$ 증류수에 24시간 보관한 후 각 실험방법에 맞게 인장력을 가하여 측정치를 구하였다. 통계분석은 95% 신뢰수준의 ANOVA와 Tukey's test를 이용하였으며, 두 실험방법의 상관관계를 보기 위해 Pearson's 상관계수를 계산하였다. 전자현미경 검사를 통해 미세구조 또한 관찰하여 다음과 같은 결론을 얻었다. 1. 파괴인성은 SE군이 가장 높은 값을 나타냈으며, Adper Single Bond 2 (SB), OptiBond Solo (OB) ONE-STEP PLUS (OS), ScotchBond Multi-purpose (SM)군 순으로 나타났고, Clearfil SE Bond (SE)군은 다른 실험군에 비해 유의하게 높은 값을 나타내었으나 (p <0.05), 다른 실험군 사이에는 유의차가 없었다 (p > 0.05). 2. 미세인장결합강도는 SE군이 가장 높은 값을 나타냈으며, SB, OB, SM, 그리고 OS 순으로 나타났다. SB, OB, SM, SE군 사이에는 통계학적인 유의차가 없었으나 (p > 0.05), OS군의 미세인장결합강도는 다른 4개의 실험군에 비해 낮은 값을 나타내었다 (p < 0.05). 3. FE-SEM관찰에서 피막도가 두껍게 나타난 SM군, SE군과 피막도가 얇은 OS군, OB군, SB군 간에 파괴양상이 다르게 나타났다 즉 전자는 접착층 내 파괴가 일어난 반면, 후자는 resin tag나 레진 침투층 내에서 파절되는 양상을 나타내었다. 4. 파괴 인성과 미세인장결합강도 사이에는 통계학적으로 유의 한 상관 관계가 없었다 ($r^2=0.223$, t=0.927). 이와 같은 결과를 토대로, 상아질 접착제의 임상적 효율성을 평가하고자 할 때는 결합강도 뿐만 아니라. 파괴인성도 함께 고려하여 임상적용의 예견성을 높여야 한다고 결론내릴 수 있다.

• 한국도로학회논문집
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• 제19권6호
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• pp.37-46
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• 2017

PURPOSES : A composite pavement utilizes both an asphalt surface and a concrete base. Typically, a concrete base layer provides structural capacity, while an asphalt surface layer provides smoothness and riding quality. This pavement type can be used in conjunction with rollercompacted concrete (RCC) pavement as a base layer due to its fast construction, economic efficiency, and structural performance. However, the service life and functionality of composite pavement may be reduced due to interfacial bond failure. Therefore, adequate interfacial bonding between the asphalt surface and the concrete base is essential to achieving monolithic behavior. The purpose of this study is to investigate the bond characteristics at the interface between asphalt (HMA; hot-mixed asphalt) and the RCC base. METHODS : This study was performed to determine the optimal type and application rate of tack coat material for RCC-base composite pavement. In addition, the core size effect, temperature condition, and bonding failure shape were analyzed to investigate the bonding characteristics at the interface between the RCC base and HMA surface. To evaluate the bond strength, a pull-off test was performed using different diameters of specimens such as 50 mm and 100 mm. Tack coat materials such as RSC-4 and BD-Coat were applied in amounts of 0.3, 0.5, 0.7, 0.9, and $1.1l/m^2$ to determine the optimal application rate. In order to evaluate the bond strength characteristics with temperature changes, a pull-off test was carried out at -15, 0, 20, and $40^{\circ}C$. In addition, the bond failure shapes were analyzed using an image analysis program after the pull-off tests were completed. RESULTS : The test results indicated that the optimal application rate of RSC-4 and BD-Coat were $0.8l/m^2$, $0.9l/m^2$, respectively. The core size effect was determined to be negligible because the bond strengths were similar in specimens with diameters of 50 mm and 100 mm. The bond strengths of RSC-4 and BD-Coat were found to decrease significantly when the temperature increased. As a result of the bonding failure shape in low-temperature conditions such as -15, 0, and $20^{\circ}C$, it was found that most of the debonding occurred at the interface between the tack coat and RCC surface. On the other hand, the interface between the HMA and tack coat was weaker than that between the tack coat and RCC at a high temperature of $40^{\circ}C$. CONCLUSIONS : This study suggested an optimal application rate of tack coat materials to apply to RCC-base composite pavement. The bond strengths at high temperatures were significantly lower than the required bond (tensile) strength of 0.4 MPa. It was known that the temperature was a critical factor affecting the bond strength at the interface of the RCC-base composite pavement.

• The Journal of Advanced Prosthodontics
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• 제10권4호
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• pp.259-264
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• 2018

PURPOSE. The purpose of this study was to evaluate the effect of the zirconia surface architecturing technique (ZSAT) on the bond strength between veneering porcelain and zirconia ceramic. MATERIALS AND METHODS. 20 sintered zirconia ceramic specimens were used to determine the optimal surface treatment time, and were randomly divided into 4 groups based on treatment times of 0, 1, 2, and 3 hours. After etching with a special solution, the surface was observed under scanning electron microscope, and then the porcelain was veneered for scratch testing. Sixty 3 mol% yttria-stabilized tetragonal zirconia polycrystal ceramic blocks were used for tensile strength testing; 30 of these blocks were surface treated and the rest were not. Statistical analysis was performed using ANOVA, the Tukey post-hoc test, and independent t-test, and the level of significance was set at ${\alpha}=.05$. RESULTS. The surface treatment of the zirconia using ZSAT increased the surface roughness, and tensile strength test results showed that the ZSAT group significantly increased the bond strength between zirconia and veneering porcelain compared to the untreated group (36 MPa vs. 30 MPa). Optimal etching time was determined to be 2 hours based on the scratch test results. CONCLUSION. ZSAT increases the surface roughness of zirconia, and this might contribute to the increased interfacial bond strength between zirconia and veneering porcelain.

• 한국전산구조공학회논문집
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• 제24권1호
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• pp.43-53
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• 2011

철근 콘크리트 부재에서 부착강도는 콘크리트와 보강근 사이에 중요한 요소 중 하나이다. 본 실험에서는 인공경량골재를 사용한 경량콘크리트와 이형철근의 부착강도의 특성을 확인하기 위하여 인발실험을 수행하였다. 콘크리트의 압축강도, 이형철근의 직경과 묻힘길이를 변수로 하는 144개의 인발실험 시험체가 사용되었다. 보통콘크리트와의 비교를 위하여 물/시멘트 비 50%의 보통콘크리트의 인발실험을 수행하였으며, 실험을 통해서 부착응력-미끌림 관계와 파괴형상을 평가하였다. 물/시멘트 비에 따른 콘크리트의 압축강도가 증가할수록 부착강도는 증가하였다. 또한 인발실험을 토대로 회귀분석을 실시하여 경량 콘크리트의 부착응력에 대한 산정식을 제안하였다.

• 대한토목학회논문집
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• 제31권3A호
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• pp.251-260
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• 2011

본 연구는 천연마섬유보강 시멘트 경화체와 폴리올레핀계 매크로섬유의 부착강도, 계면인성, 미세구조 분석을 포함한 부착 특성에 미치는 천연마섬유의 효과를 제시하였다. 다양한 조건에서의 폴리올레핀계 매크로섬유 인발시험의 실험적 결과를 보고하였다. 천연마섬유의 혼입률은 0.1%에서 0.2%까지를 배합설계에 적용하였다. 부착시험은 천연마섬유보강 시멘트 경화체에서 폴리올레핀계 매크로섬유의 부착특성을 측정하기 위하여 실시하였다. 시험결과 천연마섬유의 혼입은 폴리올레핀계 매크로섬유와 시멘트 경화체의 계면강화에 효과적이었다. 폴리올레핀계 매크로섬유와 천연마섬유보강 시멘트 경화체의 부착강도 및 계면인성은 섬유의 혼입률이 증가할수록 증가하였다. 미세구조분석은 섬유의 인발시험결과로부터 획득한 부착 메커니즘을 확인할 수 있었다.

• 콘크리트학회논문집
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• 제19권5호
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• pp.631-637
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• 2007

연구의 촛점은 강섬유 보강 고강도콘크리트와 고장력 철근 사이의 부착 특성을 평가하였다. 강섬유 혼입률에 따른 2가지 종류의 고강도콘크리트에서 고장력 철근의 부착 성능을 평가하기 위하여 직접 부착 실험을 실시하였다. 또한 콘크리트의 압축강도의 영향을 최소로 고려하여 강섬유 혼입률에 따른 부착강도의 영향을 결정하기 위하여 상대 부착강도를 정의하였다. 부착 성능 실험 결과 강섬유의 혼입률이 증가할수록 증가하였으며 강도가 높은 콘크리트 배합에서 더 우수한 결과를 나타내었다. 콘크리트의 강도에 대한 영향을 최소로하여 강섬유 혼입률에 따른 영향을 분석하기 위한 상대부착강도 평가 결과 섬유의 사용량이 증가할수록 상대부착강도가 증가하여 섬유의 혼입률은 고강도콘크리트의 강도에 관계없이 부착강도가 증가하였다.

• 대한건축학회논문집:구조계
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• 제34권1호
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• pp.41-51
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• 2018

In case of evaluating the bond stress of a void deck plate using a wire steel, there is no standard formula considering both the influence on the void and the type of the reinforcing bar. Therefore we proposed a model equation considered the bond characteristics of the void deck plate. A total of 46 specimens was carried out a direct pull-out test and the test variables were the presence of a void body, type of reinforcing bar, the inner cover thickness according to the location of reinforcing bars and bond region. As a result of the comparison between the steel bar and steel wire, the bond stress of the steel wire with the relative rib area of 0.071 is 4.5 ~ 28.58% lower than that of the steel bar with 0.092 and the bond stress reduction rate increases when the inner cover thickness is insufficient. In the case of the inner cover thickness of $1.7d_b$ and $2.7d_b$, the bond stress was reduced to 48.7 ~ 68.4%. In the inner cover thickness was $4.9d_b$ and $5.2d_b$, the bond stresses were equivalent to those of the solid specimens. It was confirmed that the average bond stress and strain were affected by the inner cover thickness. Therefore the predicted model for one module of the void deck plate is proposed and verified by considering the bond characteristics of the void deck plate.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 1992년도 봄 학술발표회 논문집
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• pp.74-79
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• 1992

The confinement of concrete from splitting bond failure is studied with the experiments and finite element models. The cracks in the test beam-end specimens containing various covers show a typical splitting failure with a dominant fracture surface. The finite element model includes representation of the splitting cracking using Hillerborg's fictitious crack model. The increase in bond strength from addition of covers are consistant for both test bars and numerical models. The numerical solution agrees well with results and also with the test results and also with the empirical equations. The splitting crack in the numerical models generally matches the crack surface observed in the laboratory. The confinement of concrete from splitting is one of the governing factors in the ultimate bond force.