• 대한의용생체공학회:의공학회지
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• 제17권3호
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• pp.327-336
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• 1996

This study was performed to investigate the effec% of immersion in water and thermal cycling on the mechanical peoperties of light cured restorative composite resins. Five commerically available light-cured composite resins(Photo Clearfil A : CA, Lite-Fil A . LF, Clearril Photo Posterior CP, Prisms AP.H.. PA, 2100 : ZH) were unto The specimens of 12 m in diameter and 0.7 m in thickness were made, and an immersion in $37^{\circ}C$ water for 7 days and a thermal cycling of 1000 cycles at 15 second dwell time each in $5^{\circ}C$ and $55^{\circ}C$ baths were performed. Biaxial flexure test was conducted using the ball-on-three-ball method at the crosshead speed of 0.5mm/min. In order to investigate the deterioration of composite resins during the thermal cycling test, Weibull analysis for the biaxial flexure strengths was done. Fracture surfaces and the surfaces before and after the thermal cycling test were examined by SEM. The highest Weibull modulus value of 10.09 after thermal cycling tests which means the lowest strength variation, was observed in the CP group, and the lowest value of 4.47 was obsered in the LF Group. Biaxial flexure strengths and Knoop hardness numbers significantly decreased due to the thermal cycling ($\textit{p}$< 0.01), however, they recovered when specimens were drie4 The highest biaxial flexure strength of 125.65MPa was observed in the ZH group after the thermal cycling test, and the lowest value of 64.86MPa was observed in the CA group. Biaxial flexure strengths of ZH and CP groups were higher than those of PA, CF, and CA groups after thermal cycling test($\textit{p}$< 0.05). Knoop hardness numbers of CP group after the thermal cycling test was the highest(95.47 $\pm$ 7.35kg/$mm^2$) among the samples, while that of CA group was the lowest(30.73 $\pm$ 2.58kg/$mm^2$). Knoop hardness numbers showed the significant differences between the CP group and others after the thermal cycling test(($\textit{p}$< 0.05). Fracture surfaces showed that the composite resin failure developed along the matrix resin and the filler/resin interface region, and the cracks propagated in the conical shape from the maximum tensile stress zone.

• 대한치과보철학회지
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• 제59권2호
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• pp.190-200
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• 2021

목적: 본 연구의 목적은 유색의 단일구조 지르코니아의 이축 굴곡 강도와 경도를 평가하고, 착색 용액의 적용에 따른 지르코니아의 강도 변화를 알아보는 것이다. 재료 및 방법: 단일 구조 지르코니아 시편(Eclipse V2.0, AMS, Korea)을 동일 크기의 디스크 형태로 밀링하고, 지르코니아 착색 용액의 적용 시간에 따라 4개의 군으로 분류(n = 12)하였다(PU, ST, OV, PS). 각 시편의 이축 굴곡 강도를 측정하고, Vickers 경도를 측정했다. 파절 시험 이후, 파절된 시편을 이용하여, X-선 회절 분석을 시행하였다. 결과 분석은 One-way ANOVA를 이용하여 분석했다. 결과: 2축 굴곡 강도 실험에서는 그룹 간에 유의한 차이가 없었다. 하지만 Vickers 경도 실험에서 제조사 지시대로 착색용액을 적용한 그룹이 착색 용액을 적용하지 않은 그룹보다 유의하게 값이 높았다 (P = .038). 나머지 그룹 간 Vickers 경도는 유의한 차이가 없었다 (P > .05). X-ray 회절 분석 결과 모든 군의 X-ray 회절 분석 상에는 정방정상의 특이적 피크를 보여주었고, 모든 단사정상 분율은 25%미만이었다. 결론: 지르코니아 착색용액의 적용 여부 및 적용 시간은 이축 굴곡 강도에 유의한 영향을 미치지 않았다. Vickers 경도는 제조사 지시대로 착색 용액을 적용한 그룹과 착색 용액을 적용하지 않은 그룹 간에는 유의한 차이가 있었으나, 나머지 그룹 간에는 유의한 차이가 없었다. 본 실험에 사용한 지르코니아 시편의 이축 굴곡 강도 결과는 치과용 세라믹 용도에 따른 최소 굴곡 강도 기준의 Class 5에 해당하였다.

• 콘크리트학회논문집
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• 제17권5호
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• pp.803-809
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• 2005

본 연구는 1축 및 2축 압축응력을 받는 고강도 콘크리트 및 섬유보강 고강도 콘크리트의 역학적 거동 및 재료 특성을 규명함에 목적이 있다. 이를 위하여, 본 연구에서는 82.7MPa(12,000psi) 뽀일 압축강도를 발현하는 고강도 콘크리트 및 섬유보강 고강도 콘크리트 큐브 시편을 제작하여 2축 압축 응력비($\sigma_2/\sigma_1$=0.00, 0.50 , 0.75, 1.00) 및 섬유혼입률($V_f$=0.0, 0.5, 1.0, 1.5%)을 주된 실험 변수로 하는 실험을 수행하였다. 위 실험 연구를 통하여, 부응력 방향으로 도입된 구속응력은 주응력 방향으로의 강도 및 변형 거동에 좋은 개선 효과를 보이며, 고강도 콘크리트 및 강섬유 보강 고강도 콘크리트의 강성 및 극한강도가 현저히 증대되었음을 알 수 있었다. 또한 주응력 방향 및 부응력 방향 압축응력비($\sigma_2/\sigma_1$)가 0.5일 때 극한강도의 효과가 가장 크게 나타났으며, 최대 증진 효과는 1축의 그것과 비교할 때 약 $30\%$의 효과가 있는 것으로 나타났다. 1축 압축을 받는 고강도 보통 콘크리트 및 강섬유보강 콘크리트는 재하 방향과 평행한 쪼갬인장응력으로 인한 균열이 발생하는 것으로 나타났으나, 2축 압축을 받는 섬유보강 고강도 콘크리트는 전단 형태의 파괴가 일어났다. 본 실험 결과로부터 도출된 2축 압축 상태에서의 탄성계수 값은 ACI, CEB식에서 도출된 탄성계수보다 높게 나타났으며, 따라서 현재 사용되는 ACI 및 CEB 탄성계수 식은 2축 압축을 받는 고강도 콘크리트에도 적용이 가능한 것으로 사료된다.

• 한국강구조학회 논문집
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• 제14권6호
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• pp.823-834
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• 2002

Steel-Concrete Column은 H형강의 플랜지 사이에 후프를 용접하고 플랜지 사이의 공간에 콘크리트가 채워진 새로운 합성기둥이다. 본 연구에서는 이 새로운 합성 기둥의 구조성능을 평가하기 위하여 단주압축, 휨, 전단실험을 수행하였다. 각 실험별 실험체들을 순철골 실험체와 철골 콘크리트 실험체로 구성하여 Steel-Concrete Column을 구성하는 철골, 내부 콘크리트, 후프의 내력기여도를 평가할 수 있도록 하였다. 실험결과 Steel-Concrete Column은 $\ulcorner$강구조 한계상태 설계 기준$\lrcorner$ 에 의해 계산된 내력값을 충분히 만족하여 구조부재에 적용 가능하다고 판단된다.

• The Journal of Advanced Prosthodontics
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• 제7권5호
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• pp.349-357
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• 2015

PURPOSE. The purpose of this study was to assess the impact of the core materials, thickness and fabrication methods of veneering porcelain on prosthesis fracture in the porcelain fused to metal and the porcelain veneered zirconia. MATERIALS AND METHODS. Forty nickel-chrome alloy cores and 40 zirconia cores were made. Half of each core group was 0.5 mm-in thickness and the other half was 1.0 mm-in thickness. Thus, there were four groups with 20 cores/group. Each group was divided into two subgroups with two different veneering methods (conventional powder/liquid layering technique and the heat-pressing technique). Tensile strength was measured using the biaxial flexural strength test based on the ISO standard 6872:2008 and Weibull analysis was conducted. Factors influencing fracture strength were analyzed through three-way ANOVA (${\alpha}{\leq}.05$) and the influence of core thickness and veneering method in each core materials was assessed using two-way ANOVA (${\alpha}{\leq}.05$). RESULTS. The biaxial flexural strength test showed that the fabrication method of veneering porcelain has the largest impact on the fracture strength followed by the core thickness and the core material. In the metal groups, both the core thickness and the fabrication method of the veneering porcelain significantly influenced on the fracture strength, while only the fabrication method affected the fracture strength in the zirconia groups. CONCLUSION. The fabrication method is more influential to the strength of a prosthesis compared to the core character determined by material and thickness of the core.

• 한국전산구조공학회:학술대회논문집
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• 한국전산구조공학회 2007년도 정기 학술대회 논문집
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• pp.399-402
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• 2007

The classical two dimensional modulus of rupture test was generalized to three dimensions. Using this new method, the biaxial tensile strength can be measured with only one actuator. A circular plate is used in this method unlike a prismatic beam in the classical modulus of rupture test. The stress field in this specimen is isotropic and uniform in a plane paralle1 to the bottom surface of the specimen. The relation between the applied load and the maximum stress is derived analytical1y using Timoshenko's solution. A set of experimental data is presented.

• 대한치과보존학회:학술대회논문집
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• 대한치과보존학회 2003년도 제120회 추계학술대회 제 5차 한ㆍ일 치과보존학회 공동학술대회
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• pp.575-575
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• 2003

The majority of studies comparing the mechanical properties of brittle dental restorative materials now include use of the Weibull Modulus (m). This modulus is determined from analysis of the statistical distribution of strength measurements, which can be determined using a variety of methods, including biaxial flexure, 3pt bend and 4pt bend. In comparing materials it is usually implicitly assumed that the modulus (m) is independent of test method although it is recognised to be highly dependent on flaw distributions. However, in some cases flaw distributions can be modified by sample preparation and test method may modify stressing patterns. This study investigated the pattern of strength and m in two light setting materials.

• 한국산업융합학회 논문집
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• 제26권4_2호
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• pp.629-637
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• 2023

This study aimed to evaluate the effect of post-curing equipment and time on the flexural strength of 3D printing resins produced by a liquid crystal display(LCD) printer. The three 3D printing resins(DENTCA Denture Teeth, DT; C&B 5.0 hybrid, CH; C&B Permanent A2, CP) were divided into four groups according to post-curing time(10 min and 30 min) and equipment with or without vacuum treatment. For the three-point flexural strength test and biaxial strength test were prepared by method according to ISO 10477, ISO 6872, respectively. Flexural strength was measured with universal testing machine. Comparison between post-curing time of each post-curing equipment was analyzed by independent sample t-test and Mann-Whitney U test(α=.05), and comparison between groups according to each 3D printing resin was performed by Kruskal-Wallis test and post-hoc by Bonferroni-Dunn test(α=.05). The flexural strength of the resin post-curing under vacuum was higher than that of the resin post-curing in air. In the comparison according to the post-curing time, in the case of the post-curing equipment without vacuum, the 30 minute curing time showed significantly higher flexural strength than the 10 minute curing time, except for the biaxial flexural strength of CH(P<.05). In the post-curing equipment with vacuum, the three-point flexural strength of all 3D printing resins(DT, CH, and CP) showed a higher value at 30 minute curing time than at 10 minute curing time.

• 한국세라믹학회지
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• 제36권3호
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• pp.225-230
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• 1999

Ball-on-3-ball 시험에서 이축 강도를 결정하기 위한 방법에 대해 고찰하였다. 알루미나 시편을 이용하여 ball-on-3-ball 시험과 poston-on-3-ball 시험을 하여 이축 강도를 측정하였다. piston-on-3-ball 시험에서의 강도 식과 등가 반지름을 이용하여 계산한 ball-on-3-ball 시험에서의 이축 강도와, piston-on-3-ball 시험에서의 이축 강도를 분산 분석(ANOVA)한 결과, 두 평균이 동일하다고 할 수 있었다. 따라서, ball-on-3-ball 시험에서의 이축 강도는 piston-on-3-ball 시험에서의 강도 식과 등가 반지름을 이용하여 계산할 수 있다. 또한, 유한 요소법을 이용하여 ball-on-3-ball 시험시 시편에 인가되는 응력 분포를 고찰해 보았다.

• 치위생과학회지
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• 제10권5호
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• pp.335-340
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• 2010

This study was performed to evaluate the fracture strength of the dental zirconia veneering ceramics for zirconia ceramic core. Six commercial zirconia veneering ceramics were used in this study, namely E-Max(Ivoclar vivadent, Inc, Liechtenstein), Creation ZI(KLEMA Dental produckte GmbH, Austria), Cercon ceram kiss(Degudent, GmbH, Hanau-Wolfgang, Germany), Triceram(Dentaurum, Ispringen, Germany), Zirkonzahn(Zirkonzahn GmbH, Italy), Zirmax(Alpadent, korea). All samples were prepared according to the relevant instructions of manufacture. Disc specimens were prepared to the final dimensions of 17 mm in diameter and 1.5 mm in thickness. The biaxial flexure strength test was conducted using a ball-on-three-ball method. All specimens were tested in a moisture-free environment. Average flexural strengths were analyzed with Weibull analysis and one-way analysis of variance(ANOVA). Significant differences were founded between the mean flexural strength values of five commercials zirconia veneering ceramics and the other. The flexural strengths and Weibull modulus were similar to those of five groups E-Max(EM), Creation ZI(CR), Cercon ceram kiss(CE), Triceram(TR), Zirkonzahn(ZI) with the exception of Zirmax(ZM). The biaxial flexural strength from Cercon ceram kiss(CE) was higher than those of other groups. Fracture analysis showed similar results for these five groups.