• Journal of Biomedical Engineering Research
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• v.17 no.3
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• pp.327-336
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• 1996

This study was performed to investigate the effec% of immersion in water and thermal cycling on the mechanical peoperties of light cured restorative composite resins. Five commerically available light-cured composite resins(Photo Clearfil A : CA, Lite-Fil A . LF, Clearril Photo Posterior CP, Prisms AP.H.. PA, 2100 : ZH) were unto The specimens of 12 m in diameter and 0.7 m in thickness were made, and an immersion in $37^{\circ}C$ water for 7 days and a thermal cycling of 1000 cycles at 15 second dwell time each in $5^{\circ}C$ and $55^{\circ}C$ baths were performed. Biaxial flexure test was conducted using the ball-on-three-ball method at the crosshead speed of 0.5mm/min. In order to investigate the deterioration of composite resins during the thermal cycling test, Weibull analysis for the biaxial flexure strengths was done. Fracture surfaces and the surfaces before and after the thermal cycling test were examined by SEM. The highest Weibull modulus value of 10.09 after thermal cycling tests which means the lowest strength variation, was observed in the CP group, and the lowest value of 4.47 was obsered in the LF Group. Biaxial flexure strengths and Knoop hardness numbers significantly decreased due to the thermal cycling ($\textit{p}$< 0.01), however, they recovered when specimens were drie4 The highest biaxial flexure strength of 125.65MPa was observed in the ZH group after the thermal cycling test, and the lowest value of 64.86MPa was observed in the CA group. Biaxial flexure strengths of ZH and CP groups were higher than those of PA, CF, and CA groups after thermal cycling test($\textit{p}$< 0.05). Knoop hardness numbers of CP group after the thermal cycling test was the highest(95.47 $\pm$ 7.35kg/$mm^2$) among the samples, while that of CA group was the lowest(30.73 $\pm$ 2.58kg/$mm^2$). Knoop hardness numbers showed the significant differences between the CP group and others after the thermal cycling test(($\textit{p}$< 0.05). Fracture surfaces showed that the composite resin failure developed along the matrix resin and the filler/resin interface region, and the cracks propagated in the conical shape from the maximum tensile stress zone.

• The Journal of Korean Academy of Prosthodontics
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• v.59 no.2
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• pp.190-200
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• 2021

Purpose. The aim of this study was to evaluate biaxial flexural strength and hardness of colored monolithic zirconia after dipping in different time intervals of coloring solution. Materials and Methods. Disk shaped specimens were prepared from monolithic zirconia (Eclipse V2.0, AMS, Gimpo, Korea). Four experimental groups were categorized (n = 12) due to coloring time (PU (0s); ST (8s); OV (1 min); PS (preshade)), to evaluate biaxial flexural strength and Vickers hardness. After fracture, X-ray diffraction analysis was performed using fractured specimens. Results were analyzed with one-way ANOVA test. Results. There was no significant difference between groups in the biaxial flexural strength test. However, in the Vickers hardness test, the group with standard dipping time (ST) showed significantly higher value than the group without dipping in coloring liquid (PU)(P=.038). Also, there was no significant difference in the rest of the groups (P>.05). As a result of X-ray diffraction analysis, specific peaks of tetragonal phase were shown and the volume of monoclinic phase fraction was lower than 25%. Conclusion. Although this study has several limitations, coloring liquids had no significant effect on biaxial flexural strength. Vickers hardness was significantly different between the group to which the coloring liquid was applied and the group to which the coloring solution was not applied, but there was no significant difference between the other groups. Also, the flexural strength of monolithic zirconia corresponds to Class 5 of the minimal flexural strength standard according to the use of dental ceramics.

• Journal of the Korea Concrete Institute
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• v.17 no.5 s.89
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• pp.803-809
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• 2005

The purpose of this study is to investigate the mechanical characteristics of plain and steel fiber high strength concrete under uniaxial and biaxial loading condition. A number of plain and steel fiber high strength concrete cubes having 28 days compression strength of 82.7MPa(12,000 psi) were made and tested. Four principal compression stress ratios ($\sigma_2/\sigma_1$=0.00, 050, 0.75 and 1.00), and four fiber concentrations($V_f$ =0.0, 0.5, 1.0 and $1.5\%$) were selected as major test variables. From test results, it is shown that confinement stress in minor stress direction has pronounced effect on the strength and deformational behavior. Both of the stiffness and ultimate strength of the plain and fiber high strength concrete Increased. The maximum increase of ultimate strength occurred at biaxial stress ratio of 0.5($\sigma_2/\sigma_1=0.5$) in the plain high strength concrete and the value were recorded $30\%$ over than the strength under uniaxial condition. The failure modes of plain high strength concrete under uniaxial compression were shown as splitting type of failure but steel fiber concrete specimens under biaxial condition showed shear type failure. The values of elastic modulus were also examined higher than that from ACI and CEB expression under biaxial compression condition.

• Journal of Korean Society of Steel Construction
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• v.14 no.6
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• pp.823-834
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• 2002

Maximum-strength concrete-filled steel square tubular columns were tested under concentric and biaxial eccentric load. Buckling length-section depth ratio $L_k/D$, magnitude of eccentricity e, and angle of eccentric load ${\theta}$ were selected as experimental parameters. Strength and behavior were also examined. Test results showed that the maximum strength of columns under biaxial eccentric load could be predicted using the previously proposed strength formula of columns undr uniaxia eccentric load. Likewise, the behavior and maximum strength of columns could be predicted using the analysis.

• The Journal of Advanced Prosthodontics
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• v.7 no.5
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• pp.349-357
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• 2015

PURPOSE. The purpose of this study was to assess the impact of the core materials, thickness and fabrication methods of veneering porcelain on prosthesis fracture in the porcelain fused to metal and the porcelain veneered zirconia. MATERIALS AND METHODS. Forty nickel-chrome alloy cores and 40 zirconia cores were made. Half of each core group was 0.5 mm-in thickness and the other half was 1.0 mm-in thickness. Thus, there were four groups with 20 cores/group. Each group was divided into two subgroups with two different veneering methods (conventional powder/liquid layering technique and the heat-pressing technique). Tensile strength was measured using the biaxial flexural strength test based on the ISO standard 6872:2008 and Weibull analysis was conducted. Factors influencing fracture strength were analyzed through three-way ANOVA (${\alpha}{\leq}.05$) and the influence of core thickness and veneering method in each core materials was assessed using two-way ANOVA (${\alpha}{\leq}.05$). RESULTS. The biaxial flexural strength test showed that the fabrication method of veneering porcelain has the largest impact on the fracture strength followed by the core thickness and the core material. In the metal groups, both the core thickness and the fabrication method of the veneering porcelain significantly influenced on the fracture strength, while only the fabrication method affected the fracture strength in the zirconia groups. CONCLUSION. The fabrication method is more influential to the strength of a prosthesis compared to the core character determined by material and thickness of the core.

• Proceedings of the Computational Structural Engineering Institute Conference
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• 2007.04a
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• pp.399-402
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• 2007

The classical two dimensional modulus of rupture test was generalized to three dimensions. Using this new method, the biaxial tensile strength can be measured with only one actuator. A circular plate is used in this method unlike a prismatic beam in the classical modulus of rupture test. The stress field in this specimen is isotropic and uniform in a plane paralle1 to the bottom surface of the specimen. The relation between the applied load and the maximum stress is derived analytical1y using Timoshenko's solution. A set of experimental data is presented.

• Proceedings of the KACD Conference
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• 2003.11a
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• pp.575-575
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• 2003

The majority of studies comparing the mechanical properties of brittle dental restorative materials now include use of the Weibull Modulus (m). This modulus is determined from analysis of the statistical distribution of strength measurements, which can be determined using a variety of methods, including biaxial flexure, 3pt bend and 4pt bend. In comparing materials it is usually implicitly assumed that the modulus (m) is independent of test method although it is recognised to be highly dependent on flaw distributions. However, in some cases flaw distributions can be modified by sample preparation and test method may modify stressing patterns. This study investigated the pattern of strength and m in two light setting materials.

• Journal of the Korean Society of Industry Convergence
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• v.26 no.4_2
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• pp.629-637
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• 2023

This study aimed to evaluate the effect of post-curing equipment and time on the flexural strength of 3D printing resins produced by a liquid crystal display(LCD) printer. The three 3D printing resins(DENTCA Denture Teeth, DT; C&B 5.0 hybrid, CH; C&B Permanent A2, CP) were divided into four groups according to post-curing time(10 min and 30 min) and equipment with or without vacuum treatment. For the three-point flexural strength test and biaxial strength test were prepared by method according to ISO 10477, ISO 6872, respectively. Flexural strength was measured with universal testing machine. Comparison between post-curing time of each post-curing equipment was analyzed by independent sample t-test and Mann-Whitney U test(α=.05), and comparison between groups according to each 3D printing resin was performed by Kruskal-Wallis test and post-hoc by Bonferroni-Dunn test(α=.05). The flexural strength of the resin post-curing under vacuum was higher than that of the resin post-curing in air. In the comparison according to the post-curing time, in the case of the post-curing equipment without vacuum, the 30 minute curing time showed significantly higher flexural strength than the 10 minute curing time, except for the biaxial flexural strength of CH(P<.05). In the post-curing equipment with vacuum, the three-point flexural strength of all 3D printing resins(DT, CH, and CP) showed a higher value at 30 minute curing time than at 10 minute curing time.

• Journal of the Korean Ceramic Society
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• v.36 no.3
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• pp.225-230
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• 1999

Ball-on-3-ball 시험에서 이축 강도를 결정하기 위한 방법에 대해 고찰하였다. 알루미나 시편을 이용하여 ball-on-3-ball 시험과 poston-on-3-ball 시험을 하여 이축 강도를 측정하였다. piston-on-3-ball 시험에서의 강도 식과 등가 반지름을 이용하여 계산한 ball-on-3-ball 시험에서의 이축 강도와, piston-on-3-ball 시험에서의 이축 강도를 분산 분석(ANOVA)한 결과, 두 평균이 동일하다고 할 수 있었다. 따라서, ball-on-3-ball 시험에서의 이축 강도는 piston-on-3-ball 시험에서의 강도 식과 등가 반지름을 이용하여 계산할 수 있다. 또한, 유한 요소법을 이용하여 ball-on-3-ball 시험시 시편에 인가되는 응력 분포를 고찰해 보았다.

• Journal of dental hygiene science
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• v.10 no.5
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• pp.335-340
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• 2010

This study was performed to evaluate the fracture strength of the dental zirconia veneering ceramics for zirconia ceramic core. Six commercial zirconia veneering ceramics were used in this study, namely E-Max(Ivoclar vivadent, Inc, Liechtenstein), Creation ZI(KLEMA Dental produckte GmbH, Austria), Cercon ceram kiss(Degudent, GmbH, Hanau-Wolfgang, Germany), Triceram(Dentaurum, Ispringen, Germany), Zirkonzahn(Zirkonzahn GmbH, Italy), Zirmax(Alpadent, korea). All samples were prepared according to the relevant instructions of manufacture. Disc specimens were prepared to the final dimensions of 17 mm in diameter and 1.5 mm in thickness. The biaxial flexure strength test was conducted using a ball-on-three-ball method. All specimens were tested in a moisture-free environment. Average flexural strengths were analyzed with Weibull analysis and one-way analysis of variance(ANOVA). Significant differences were founded between the mean flexural strength values of five commercials zirconia veneering ceramics and the other. The flexural strengths and Weibull modulus were similar to those of five groups E-Max(EM), Creation ZI(CR), Cercon ceram kiss(CE), Triceram(TR), Zirkonzahn(ZI) with the exception of Zirmax(ZM). The biaxial flexural strength from Cercon ceram kiss(CE) was higher than those of other groups. Fracture analysis showed similar results for these five groups.