• Korean Journal of Materials Research
• /
• v.21 no.12
• /
• pp.703-707
• /
• 2011

The electrochromic properties of tungsten oxide films grown by RF sputtering were investigated. Among the sputter parameters, first the $Ar:O_2$ ratios were controlled with division into only an $O_2$ environment, 1:1 and 4:1. The structure of each film prepared by these conditions was studied by X-ray diffraction, X-ray photoelectron spectroscopy and Rutherford backscattering spectroscopy. The sputter-deposited tungsten oxide films had an amorphous structure regardless of the $Ar:O_2$ ratios. The chemical compositions, however, were different from each other. The stoichiometric structure and low-density film was obtained at higher $O_2$ contents. Electrochemical tests were performed by cyclic voltammetry and chronoamperometry at 0.05 M $H_2SO_4$ solutions. The current density and charge ratio was estimated during the continuous potential and pulse potential cycling at -0.5 V and 1.8 V, respectively. The film grown in a higher oxygen environment had a higher current density and a reversible charge reaction during intercalation and deintercalation. The in-situ transmittance tests were performed by He-Ne laser (633 nm). At higher oxygen contents, a big transmittance difference was observed but the response speed was too slow. This was likely caused by higher film resistivity. Furthermore, the effect of sputtering pressure was also investigated. The structure and surface morphology of each film was observed by X-ray diffraction and scanning electron microscopy. A rough surface was observed at higher sputtering pressure, and this affected the higher transmittance difference and coloration efficiency.

• Journal of the Korean institute of surface engineering
• /
• v.27 no.5
• /
• pp.253-260
• /
• 1994

Ta-N films were reactively sputter deposited by dc magnetron sputtering from a Ta target with a various Ar-N, gas ratio. Electrical resistivity of pure Ta film was 150$\mu$$\Omega$cm and decreased initially with nitrogen addition, and then increased to a value of 220$\mu$$\Omega$-cm~260$\mu$$\Omega$-cm at 9%~23% nitrogen partial flow. Rutherford backscattering spectrometry(RBS) and Auger electron spectroscopy (AES) analysis show that nitrogen content in the film is increased with the nitrogen partial flow. The film contains 58at.% nitrogen at 36% nitrogen partial flow. Both the phase and the microstructure of the as-deposisted films were investigated by x-ray diffractometry(XRD) adn transmission electron microscopy (TEM) at various nitrogen content. The phase of pure Ta film is identified as $\beta$-Ta with a 200$\AA$~300$\AA$ grain size. The phase of Ta film is changed to bcc-Ta as small amount of nitrogen is added. Crystalline Ta2N film was deposited at 24at.% nitrogen content. Amorphous phase is formed over a range of nitrogen content from about 33at.% to 35at.% while crystalline fcc-TaN is observed to form at 39at.%~48at.% nitrogen content.

• Korean Journal of Metals and Materials
• /
• v.49 no.2
• /
• pp.104-111
• /
• 2011

An ultrafine grained Mg-9Al-1Zn magnesium alloy with the mean grain size less than $1{\mu}m$ was produced by using high-ratio differential speed rolling. The processed alloy exhibited excellent superplasticity at relatively low temperatures. The micro-forming tests were carried out using a micro-forging apparatus with micro V-grooved shaped dies made of silicon and the micro-formability was evaluated by means of micro-formability index, $R_f$ ($=A_f/A_g$, $A_f$: formed and inflowed area into the V-groove, $A_g$: area of the V-groove). The $R_f$ value increased with temperature up to $280^{\circ}C$ and then decreased beyond $300^{\circ}C$. The decrease of the $R_f$ value at $300^{\circ}C$ was attributed to the accelerated grain coarsening. Increasing the micro-forging pressure increased the $R_f$ values. At a given die geometry, die filling ability decreased as the die position moved away from the die center to the end. FEM simulation predicted this behavior and a method of improving this problem was proposed.

• Korean Journal of Metals and Materials
• /
• v.48 no.7
• /
• pp.644-650
• /
• 2010

Interstitial free (IF) steel sheets were cold rolled by the cross-roll rolling mill in which the roll axes are tilted by ${\pm}7.5^{\circ}$ away from the transverse direction of the rolled sample. After cross-roll rolling of IF steel sheets, the cold rolling and the recrystallization textures were distinguished from those observed after rolling in a normal rolling mill. The three-dimensional finite element method (FEM) simulation revealed that the operation of a large shear strain ${\varepsilon}_{23}$ during cross-roll rolling leads to the formation of a distinct cold rolling texture. During recrystallization annealing, a pronounced change in texture components was not observed, which is attributed to the lack of either selective growth or oriented nucleation during the recrystallization process. Cold cross-roll rolling led to the formation of finer recrystallized grains in IF steel sheets.

• Korean Journal of Metals and Materials
• /
• v.49 no.8
• /
• pp.649-656
• /
• 2011

The present study evaluated the microstructures and mechanical properties of severely deformed Ni-30Cr alloys. Cross-roll rolling (CRR) process was introduced as a severe plastic deformation (SPD), and Ni-30Cr alloy sheets were cold rolled to 90% thickness reduction and subsequently annealed at $700^{\circ}C$ for 30 min to obtain the recrystallized microstructure. Electron back-scattering diffraction (EBSD) was introduced to analyze grain boundary character distributions (GBCDs). The application of CRR to the Ni-30Cr alloy was effective in enhancing the grain refinement through heat treatment; consequently, the average grain size was significantly refined from $33{\mu}m$ in the initial material to $0.6{\mu}m$. This grain refinement directly improved the mechanical properties, in which yield and tensile strengths significantly increased relative to those of the initial material. We systematically discuss the grain refinement and accompanying improvement of the mechanical properties, in terms of the effective strain imposed by CRR relative to conventional rolling (CR).

• Korean Journal of Remote Sensing
• /
• v.26 no.1
• /
• pp.1-7
• /
• 2010

This paper proposes a new decomposition technique for polarimetric synthetic aperture radar (SAR) images. This new decomposition technique is based on the degree of polarization (DoP) and co-polarized phase-difference (CPD) of the measured polarimetric backscattering coefficients. This decomposition technique is compared with the existing three- and four-component decomposition techniques with the ALOS PALSAR full polarimetric L-band data acquired in 2009. It is shown that the new decomposition technique is better or comparable to the existing techniques for the study areas such as sea, bare soil, forest, and urban area.

• Korean Journal of Remote Sensing
• /
• v.14 no.3
• /
• pp.285-294
• /
• 1998

A bio-optic survey was made in the Yellow Sea in May, 1998 for OSMI cal/val and application project. Optical measurements were made in nine stations. From these measurements, apparent and inherent optical properties such as $K_d$, R, a, and $b_b$ were estimated. The patterns of reflectance indicated that all three major constituents, namely, chlorophyll-a, suspended sediments, and CDOM were active in determining the optical properties in the Yellow Sea. Their relative contribution was different among the stations. All the stations had high backscattering and their values fell in Case 2 category. Although the total absorption was very high, it could not be explained by the level of CDOM concentration. It is suggested that the suspended sediment might be highly absorptive and further study is needed to investigate the optical properties of the suspended sediments.

• Journal of the Society of Naval Architects of Korea
• /
• v.42 no.2 s.140
• /
• pp.159-164
• /
• 2005

Monostatic RCS analysis of complex structures has been done with a combined method of physical and geometric optics, commonly applied to high frequency electromagnetic backscattering problems. In the analysis, the complex structure is modeled as a number of flat surfaces and the RCS of whole structure is calculated by summing RCS of each surface, which can be obtained from an analytical solution of flat surface phase integral derived from physical optics. The reflected and hidden surfaces are searched by an object precision method based on adaptive triangular beam method, which can take account for effects of multiple reflections and polarizations of electromagnetic wave. The validity of the presented RCS analysis method has been verified by comparing with exact solutions and measured data for various structures.

• Solar Energy
• /
• v.14 no.2
• /
• pp.29-37
• /
• 1994

Radiative charaacteristics of glass windows and porous absorbing media which can be used for a solar air heater are determined through the measurements of spectral transmittances. Those in the visible range are measured by the UV-IR spectrometer. Refractive index of glass are obtained by the comparison of the measured transmittances and the correlations derived from the electromagnetic theory and are compared to the theoretical ones calculated from the classical dispersion theory. Absorption and back-scattering coefficients of 15-mesh stainless wire screens are calcuated by the comparison of the measured transmittances and the correlations derived from the two flux model.

• Journal of the Korea Society of Computer and Information
• /
• v.17 no.2
• /
• pp.207-214
• /
• 2012

This paper is to improve an identification ratio of tags by analyzing Slotted ALOHA, Dynamic Slotted ALOHA, Binary-tree and Query-tree and shortening the tag identification time in mobile RFID. Also, it enables the stable information transmission of tags by saving backscattering power of tags through shortening of identification time. As a result, this increases the available time of the battery and accessibility to a RFID service. For this, we proposed the energy-efficient tag anti-collision protocol for mobile RFID. The proposed scheme shows advanced result in identification time and collision counts. This scheme may be the first attempt for the mobile anti-collision.