• 제목/요약/키워드: Asb-4

검색결과 24건 처리시간 0.023초

이모골라이트의 합성 (Synthesis of Imogolite by a Hydrothemal Method)

  • 장영남;류경원;서용재;채수천;배인국
    • 한국광물학회지
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    • 제21권3호
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    • pp.283-287
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    • 2008
  • $SiO_2$를 함유한 테트라에시실란(Tetracthoxysilanc: TEOS)과 알루미늄-섹-버트옥사이드(alumimum-sec-butoxide: ASB)를 출발물질로 이용하여 $100^{\circ}C$ 이하에서 결정성이 양호한 이모골라이트를 합성하였다. 합성실험은 환류장치가 부착된 둥근 플라스크에서 연속교반하면서 수열법으로 수행하였다. 이때, 화학조성은 $Al_{2}O_{3}/SiO_2$ = 1의 조건이었다. TEOS와 ABS의 농도 0.5 M의 조건에서 합성된 이모골라이트의 분말 X-선 회절 분석결과. d = 22.4. 9.5 등에서 회절선들을 관찰할 수 있었고, DTA/TG 분석견과에서는 $68^{\circ}C$에서 탈수반응에 의한, 그리고 $249^{\circ}C$에서 탁수산화 반응에 의한 흡열반응이 관찰되었으며 중량손실은 약 41%이었다. 또한, 합성된 이모골라이트는 Si-O-Al 신축진동(953과 $993cm^{-1}$)과 O-Si-O 굽힘 진동$(562cm^{-1})$에 의해서 미약하고 비대핑형의 피크 분리가 관찰되었고, TEM 분석결과, 이모골라이트 결정은 섬유상이었으며 거리줄 모양의 네트워크 구조를 보였다.

Effect of Dentin Bonding Agent Acidity on Surface Microhardness of Mineral Trioxide Aggregate

  • Yun-Hui Im;Yoon Lee
    • Journal of Korean Dental Science
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    • 제17권1호
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    • pp.36-44
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    • 2024
  • Purpose: This study investigated the effect of dentin bonding agent acidity on surface microhardness of MTA. Materials and Methods: Forty cylindrical molds (3 mm×5 mm) were prepared, and three dentin bonding agents with different acidities: Adper Single Bond 2 (ASB), Single Bond Universal (SBU), and Clearfil SE bond 2 (CSE) were applied to the inner surface of the molds (n=10). No bonding agent was applied in the control group. MTA was mixed and inserted into the molds and sealed with a wet cotton pellet for 4 days. After setting, the Vickers microhardness (HV) test was done at 200, 400, 600 ㎛ from the inner surface of the mold. One-way ANOVA was conducted for all samples. A P-value of less than .05 was considered significant. Tukey HSD test was performed for post-hoc analysis. Results: The mean HV values and standard deviations were 67.02±11.38 (Con), 48.76±11.33 (ASB), 43.78±11.19 (CSE), 37.84±9.36 (SBU), respectively. The difference between the control group and the experimental groups was statistically significant (P<0.001). The difference between ASB and SBU was statistically significant (P<0.001), while the difference between SBU and CSE was not. There were no statistically significant differences between the various points from the inner surface of the mold within each group (P>0.05). Conclusion: Results of the current study indicate that use of dentin bonding agents with MTA can reduce the surface microhardness of MTA. Moreover, there is a direct relationship between the acidity of dentin bonding agents and the surface microhardness of MTA.

Microsatellite DNA Typing Using 16 Markers for Parentage Verification of the Korean Native Horse

  • Cho, G.J.;Cho, B.W.
    • Asian-Australasian Journal of Animal Sciences
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    • 제17권6호
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    • pp.750-754
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    • 2004
  • This study was performed for parentage verification of the Korean native horse (KNH). 103 random KNH samples (including 19 foals for parentage testing) were genotyped by using 16 microsatellite markers. The number of alleles per locus varied from 5 to 13 with an average value of 8.56 in the KNH. The observed heterozygosity and the expected heterozygosity ranged 0.398-0.893 (the average value was 0.683) and 0.368-0.871 (the average value was 0.727) in the KNH, respectively. The PIC value and the exclusion probability ranged 0.347-0.853 (the average value was 0.692) and 0.208-0.736, respectively, and the total exclusion probability of 16 microsatellite loci was 0.9999. Of the 16 markers, AHT4, AHT5, ASB2, ASB17, HMS2, HMS3, HTG10, LEX33, TKY321 and VHL20 loci have a relatively high PIC value (>0.7) in the KNH. Of the 19 foals, 5 foals were disqualified by an incompatibility of 4-7 markers according to a Mendelian fashion in the present DNA typing for parentage testing. These results present basic information for developing a system for parentage verification and individual identification in the KNH.

비대칭 H형강을 사용한 슬림플로어 보의 내화성능에 관한 연구 (A Study on the Fire Resistance Capacity of Slimfloor Beam with Asymmetric H Beam)

  • 한상훈;최승관;김희주
    • 한국강구조학회 논문집
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    • 제19권4호
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    • pp.357-366
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    • 2007
  • 본 연구는 비대칭 H형강을 사용한 슬림플로어 보의 화재시 구조성능에 관한 실험 및 해석적 연구로서, 화재시 본 합성부재의 구조거동을 파악하여 합리적 내화설계의 자료를 얻는 것이 목적이다. 화재실험으로 계획된 여러 변수의 시험체를 제작하고 상온과 고온에서 휨실험을 수행하여 시간에 따른 온도분포, 하중-처짐 관계를 분석하였다. 해석적 방법은 설계된 단면에 대하여 완전 합성을 가정으로, 열전도 해석으로 온도분포를 구하고 재료의 잔존강도를 분할된 메쉬에 입력하여 휨강도를 예측하였다. 웨브의 두께와 깊이를 변수로 하여 슬림플로어 보의 화재시 휨내력을 고찰하였다.

Variation of Practice in Prophylactic Protocol to Reduce Prosthetic Joint Infection in Primary Hip and Knee Arthroplasty: A National Survey in the United Kingdom

  • James Morris;Lee Hoggett;Sophie Rogers;John Ranson;Andrew Sloan
    • Hip & pelvis
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    • 제35권4호
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    • pp.228-232
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    • 2023
  • Purpose: Prosthetic joint infection (PJI) has an enormous physiological and psychological burden on patients. Surgeons rightly wish to minimise this risk. It has been shown that a standardised, evidence-based approach to perioperative care leads to better patient outcomes. A review of current practice was conducted using a cross-sectional survey among surgeons at multiple centers nationwide. Materials and Methods: An 11-question electronic survey was circulated to hip and knee arthroplasty consultants nationally via the BOA (British Orthopaedic Association) e-newsletter. Results: The respondents included 56 consultants working across 19 different trusts. Thirty-four (60.7%) screen patients for asymptomatic bacteriuria (ASB) preoperatively, with 19 (55.9%) would treating with antibiotics. Fifty-six (100%) screen for methicillin-resistant Staphylococcus aureus and treat if positive. Only 15 (26.8%) screen for methicillin-sensitive S. aureus (MSSA) or empirically eradicate. Zero (0%) routinely catheterize patients perioperatively. Forty-one (73.2%) would give intramuscular or intravenous gentamicin for a perioperative catheterisation. All surgeons use laminar flow theatres. Twenty-six (46.4%) use only an impervious gown, 6 (10.7%) exhaust pipes, and 24 (42.3%) surgical helmet system. Five different antimicrobial prophylaxis regimens are used 9 (16.1%) cefuroxime, 2 (3.6%) flucloxacillin, 19 (33.9%) flucloxacillin and gentamicin, 10 (17.9%) teicoplanin, 16 (28.6%) teicoplanin and gentamicin. Twenty-two (39.3%) routinely give further doses. Conclusion: ASB screening, treatment and intramuscular gentamicin for perioperative catheterisation is routinely practiced despite no supporting evidence base. MSSA screening and treatment is underutilised. Multiple antibiotic regimens exist despite little variation in organisms in PJI. Practice varies between surgeons and centers, we should all be practicing evidence-based medicine.

Genetic diversity of Halla horses using microsatellite markers

  • Seo, Joo-Hee;Park, Kyung-Do;Lee, Hak-Kyo;Kong, Hong-Sik
    • Journal of Animal Science and Technology
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    • 제58권11호
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    • pp.40.1-40.5
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    • 2016
  • Background: Currently about 26,000 horses are breeding in Korea and 57.2% (14,776 horses) of them are breeding in Jeju island. According to the statistics published in 2010, the horses breeding in Jeju island are subdivided into Jeju horse (6.1%), Thoroughbred (18.8%) and Halla horse (75.1%). Halla horses are defined as a crossbreed between Jeju and Thoroughbred horses and are used for horse racing, horse riding and horse meat production. However, little research has been conducted on Halla horses because of the perception of crossbreed and people's weighted interest toward Jeju horses. Method: Using 17 Microsatellite (MS) Markers recommended by International Society for Animal Genetics (ISAG), genomic DNAs were extracted from the hair roots of 3,880 Halla horses breeding in Korea and genetic diversity was identified by genotyping after PCR was performed. Results and conclusion: In average, 10.41 alleles (from 6 alleles in HTG7 to 17 alleles in ASB17) were identified after the analysis using 17 MS Markers. The mean value of $H_{obs}$ was 0.749 with a range from 0.612(HMS1) to 0. 857(ASB2). Also, it was found that $H_{\exp}$ and PIC values were lowest in HMS1 (0.607 and 0.548, respectively), and highest in LEX3(0.859 and 0.843, respectively), and the mean value of $H_{\exp}$ was 0.760 and that of PIC was 0.728. 17 MS markers used in this studies were considered as appropriate markers for the polymorphism analysis of Halla horses. The frequency for the appearance of identical individuals was $5.90{\times}10^{-20}$ when assumed as random mating population and when assumed as half-sib and full-sib population, frequencies were $4.08{\times}10^{-15}$ and $3.56{\times}10^{-8}$, respectively. Based on these results, the 17 MS markers can be used adequately for the Individual Identification and Parentage Verification of Halla horses. Remarkably, allele M and Q of ASB23 marker, G of HMS2 marker, H and L of HTG6 marker, L of HTG7 marker, E of LEX3 marker were the specific alleles unique to Halla horses.

A 4W GaAs Power Amplifier MMIC for Ku-band Satellite Communication Applications

  • Ryu, Keun-Kwan;Ahn, Ki-Burm;Kim, Sung-Chan
    • JSTS:Journal of Semiconductor Technology and Science
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    • 제15권4호
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    • pp.501-505
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    • 2015
  • In this paper, we demonstrated a 4W power amplifier monolithic microwave integrated circuit (MMIC) for Ku-band satellite communication applications. The used device technology relies on $0.25{\mu}m$ GaAs pseudomorphic high electron mobility transistor (PHEMT) process. The 4W power amplifier MMIC has linear gain of over 30 dB and saturated output power of over 36.1 dBm in the frequency range of 13.75 GHz ~ 14.5 GHz. Power added efficiency (PAE) is over 30 %.

CRM 정보의 질, 적응적 판매행위 및 영업사원 성과 -고객관계의 질을 매개변수로 하여- (Information Quality of CRM, Adaptive Selling Behavior and Salesperson Performance: The Mediating Role of Quality of the Customer Relationships)

  • 이형택;전종근;채명수
    • 한국유통학회지:유통연구
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    • 제11권4호
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    • pp.49-70
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    • 2006
  • 본 연구는 CRM 정보의 질과 적응적 판매행위가 영업사원의 성과에 미치는 영향력을 살펴보고자 하였으며, 특히 고객관계의 질을 매개변수로 하는 연구모형과 가설을 설정하고 이를 검증하였다. 총 161명의 영업사원들에 대한 설문자료를 LISREL을 활용하여 분석한 결과, CRM 정보의 질은 영업사원의 성과에 직접적으로 영향을 미치는 것이 아니라 고객관계의 질을 통해 간접적으로만 영향을 미치는 것으로 확인되었다. 이와는 달리 영업사원의 적응적 판매행위는 영업성과에 직 간접적으로 영향을 미치는 것으로 나타났으나, 영향력의 크기를 비교한 결과 직접적 영향보다는 고객관계의 질을 통한 간접적 영향이 상대적으로 큰 것으로 밝혀졌다. 이러한 분석결과는 우수한 영업성과를 창출하기 위해서는 개별적인 고객들과의 좋은 관계를 유지하는 것이 무엇보다도 중요함을 의미한다. 따라서 CRM을 통해서 제공되는 고객정보나 영업사원의 적응적 판매행위 등이 고객과의 관계의 질을 향상시킬 수 있도록 하여야한다.

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호기성 침지형 생물막법을 이용한 Polyester 감량폐수의 처리 (Treatment of Polyester Weight Loss Wastewater by Aerated Submerged Biofilm Process)

  • 박종웅;김대희
    • 한국환경보건학회지
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    • 제23권3호
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    • pp.85-90
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    • 1997
  • The objective of this study was to investigate biodegradation of TPA(terephthalic acid) and EG (ethylene glycol), treatment efficiency of polyester weight loss wastewater and microbial characteristics by aerated submerged biolfilm(ASB) p.rocess. In a batch reactor, pH increased from 7.0 to 8. 5 in the biodegradation of TPA. Whereas, in case of EG, decreased from 7.0 to 5.2. COD concentration rapidly decreased within 24hr in the biodegradation of TPA and EG. COD removal velocity constant(k) were 0.065-0.088 hr$^{-1}$. The biodegradation velocity of TPA was 1.4 times faster than that of EG. The ratio of suspended biomass to the total biomass in the reactor was 18.3-33.3%, increased as a high ratio of EG content. Biofilm thickness, biofilm dry density and attached biomass were 346-432 $\mu$m, 41.8-61.9 mg/cm$^3$, 1.45-2.67 mg/cm$^2$, respectively. There values increased as a high ratio of TPA content. In the hydraulic retention time of 36 hr, organic loading rate of 4 kgCOD/m$^3\cdot$ day and packing ratio of 70%, the effluent concentrations of TCOD, SCOD in a continuous flow reator were 1,388 mg/l, 147 mg/l and removal efficiencies were 77%, 97.6%, respectively.

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저온소결용 알루미나 세라믹스 복합체 합성(I) (Synthesis of the Low-Temperature Sintered Alumina Ceramic Composite(I))

  • 김병익
    • 마이크로전자및패키징학회지
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    • 제5권1호
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    • pp.19-30
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    • 1998
  • Aluminium secondary butoxide(ASB)를 출발물질로 하여 졸-겔방법에 의해 소결거 동에 미치는 $\alpha$-Al2O3 seed의 첨가효과에 따른 알루미나의 저온소결 가능성과 알루미나의 상전이에 대하여 TEM, DTA, XRD, FT-IR등으로 고찰을 하였다. TEM 분석결과 초기 생 성물인 boehmite가 비정질에서 단결정질로 진행되어 가고 있음을 확인하였다. 그리고 DTA 분석결과 $\alpha$-Al2O3 seed의 첨가한 경우 seed의 함량이 증가함에 따라 상전이 온도는 점차 낮아졌으며 약 0.4wt%일 때 seed를 첨가하지 않은 시료의 전이온도(약 1126$^{\circ}C$)에 비하여 약 7$0^{\circ}C$ 저하된 약 1056$^{\circ}C$로나타났으며 그 이상의 seedcja가에 있어서는 전이온도에 크게 영향을 나타내지 않았다. 또한 XRD분석결과 $\alpha$-Al2O3 seed를 첨가하지 않은 경우 110$0^{\circ}C$이 상의 온도에서 $\alpha$상이 생성되었음을 알수 있었다. 또한 100$0^{\circ}C$이상의 온도에서 $\alpha$상이 생성 되었음을 나타내는 Al-O 흡수특성 피크가 400~1000cm-1 범위에서 나타내고 있는 것을 FT-IR 분석결과에서도 확인할수 있었다. 그리고 $\alpha$-Al2O3 seed를 약 0.4wt% 첨가시 900~ 95$0^{\circ}C$에서 $\alpha$상이 형성됨을 관찰할 수 있었다.