• Title/Summary/Keyword: Arc plasma

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A Study on the Tetrahedral Amorphous Carbon (ta-C) Coating on Medical Polymer Materials for 3D Printing Artificial Teeth (의료용 폴리머 소재를 활용한 3D 프린팅 인공치아용 사면체 비정질 카본 코팅 기술 연구)

  • Jang, Young-Jun;Kim, Jongkuk;Shin, Chang-Hee;Yu, Sung-Mi
    • Tribology and Lubricants
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    • v.38 no.6
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    • pp.255-260
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    • 2022
  • This research presents tetrahedral amorphous (ta-C) coating on the artificial tooth for improving the durability and functionality (esthtics, foreign body of tooth) by filtered cathodic vacuum arc (FCVA). A differentiated coating method is required for a ta-C coating on polymer owing to the low melting point of the polymer, inter-facial adhesion, low friction, and non-conductivity. Herein, ta-C coating is applied below 50℃, and the potential difference of the carbon plasma drawn to the substrate was controlled by applying a positive duct bias voltage without using a substrate bias voltage. Consequently, the ta-C coating with a thickness of 70nm using the duct bias condition of 20V with the highest plasma intensity satisfies the esthetics of the artificial tooth and had a 5B level of inter-facial adhesion. In addition, the composite hardness of ta-C/polymer is 380 MPa, and correlations with esthetics, sp3 bonding, and mechanical properties. The friction coefficient (CoF) of the ta-C coating in a water-lubricated environment is 0.07, showing a six-fold reduction in CoF compared with that of a polymer.

Characterization of SiC/C Nanocomposite Powders Synthesized by Arc-Discharge

  • Zhou, Lei;Yu, Jie Yi;Gao, Jian;Wang, Dong Xing;Gan, Xiao Rong;Xue, Fang Hong;Huang, Hao;Dong, Xing Long
    • Applied Microscopy
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    • v.45 no.4
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    • pp.242-248
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    • 2015
  • In this paper, three carbon sources, i.e., solid graphite, gaseous CH4 and liquid ethanol, and one solid silicon source were employed to synthesize SiC/C nanocomposite powders by arc-discharge plasma. The processing conditions such as the component ratios of raw materials, atmospheric gases, etc. were adjusted for controllable synthesis of the nanopowders. It is indicated that both of solid graphite and silicon can be co-evaporated and reacted to form nanophases of cubic ${\beta}$-SiC with ~50 nm in mean size and a little free graphite; the carbon atoms decomposed from gaseous $CH_4$ favor to combine with the evaporated silicon atoms to form the dominant SiC nanophase; liquid carbon source of ethanol can also be used to harvest the main ${\beta}$-SiC and minor 6H-SiC phases in the assembly of nanoparticles. The as-prepared SiC/C nanocomposite powders were further purified by a heat-treatment in air and their photocatalytic performances were then greatly improved.

The Characteristics of Energy Distribution to Arc Length and Hydrogen Mixing in GTA Welding (GTA 용접에서 아크 길이와 수소 혼합에 따른 에너지분포 특성)

  • Oh, Dong-Soo;Baek, Sang-Yeob;Lee, Chil-Soon;Hwang, Dong-Soo;Ham, Hyo-Sik;Park, Kyung-Do;Jung, Yun-Ho;Cho, Sang-Myung
    • Proceedings of the KWS Conference
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    • 2009.11a
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    • pp.30-30
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    • 2009
  • GTA 용접에서 용입, 용접부의 크기와 형상이 형성되는 아크 물리학적 현상을 이해함에 있어서 에너지 분포특성은 매우 중요한 인자이다. GTA 용접에서 아크 길이의 변화와 사용된 실드 가스 종류에 따라 음극인 텅스텐 전극 팁의 아크 루트 직경에 큰 변화를 주며, 양극인 모재 쪽의 에너지 분포에 영향을 미치며 된다. 기존의 연구자들은 저전류나 중전류 영역의 GTA 용접에서 텅스텐 전극의 선단각과 용입 형태와 의 관계를 plasma 기류 등에 의해 고찰하거나, 최대 아크압력에 미치는 전극형상의 영향에 대하여 연구하였다. 용접부에 작용하는 아크 압력의 분포는 결국 운동 에너지의 분포이다. 기존의 연구자들에 비하여 보다 간편한 실험을 통하여 양극 모재위의 아크 압력에 의한 에너지 분포특성을 규명하는 연구가 필요하다. 본 연구의 목적은 GTA 용접의 용접전류 100A~200A 영역에서 아크 길이 변화와 Ar 가스에 $H_2$ 혼합에 따른 측정된 아크 압력으로부터 기존연구자들의 아크 물리학적 결과들을 활용하여 양극 모재 위에 작용하는 전류밀도 분포를 유도하는 것이다. GTA 용접에서 아크 길이의 변화와 Ar 가스에 $H_2$ 혼합은 아크 압력분포에 큰 영향을 미치며, 이에 따라 에너지 분포특성에 많은 영향을 미친다. 아크 길이가 증가함에 따라 Ar가스와 $H_2$ 혼합가스의 에너지 분포는 감소하였고, Ar가스에 $H_2$ 혼합에 의해 아크 에너지가 증가하여 용입형상에 큰 영향을 미칠 것으로 판단된다. 이에 대한 연구는 향후 GTA 용접 응용분야 확대 적용될 것이며, 아크 물리학 연구에 기초적이고 아주 중요한 과학적인 자료가 될 것으로 판단된다.

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Formation Behavior and Properties of PEO Films on AZ91 Mg Alloy in 0.1 M NaOH + 0.05 M NaF Solution Containing Various Na2SiO3 Concentrations (AZ91 마그네슘 합금의 플라즈마 전해산화 피막 형성 및 물성에 미치는 0.1 M NaOH + 0.05 M NaF 용액 중 Na2SiO3 농도의 영향)

  • Kwon, Duyoung;Song, Pung-Keun;Moon, Sungmo
    • Journal of the Korean institute of surface engineering
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    • v.53 no.2
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    • pp.59-66
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    • 2020
  • Effects of Na2SiO3 concentration added into 0.1 M NaOH + 0.05 M NaF solution on the formation behavior and properties of PEO films on AZ91 Mg alloy were investigated under 1200 Hz of alternating current (AC) by voltage-time curves, in-situ observation of arc generation behavior and measurements of film thickness, surface roughness and micro vickers hardness. In the absence of Na2SiO3 in the 0.1 M NaOH + 0.05 M NaF solution, about 4 ㎛ thick PEO film was formed within 1 min and then PEO film did not grow but white spots were formed by local burning. Addition of Na2SiO3 up to 0.2 M caused more increased formation voltage and growth of PEO film with uniform generation of arcs. Addition of Na2SiO3 from 0.2 M to 0.4 M showed nearly the same voltage-time behavior and uniform arc generation. Addition of Na2SiO3 more than 0.5 M resulted in a decrease of formation voltage and non-uniform arc generation due to local burning. PEO film growth rate increased with increasing added Na2SiO3 concentration but maximum PEO film thickness was limited by local burning if added Na2SiO3 concentration is higher than 0.5 M. Surface roughness of PEO film increased with increasing added Na2SiO3 concentration and appeared to be proportional to the PEO film thickness. PEO film hardness increased with increasing added Na2SiO3 concentration and reached a steady-state value of about 930 HV at more than 0.5 M of added Na2SiO3 concentration.

Plasma D-dimer Determination in the Diagnosis of Pulmonary Embolism (폐색전증의 진단에 있어 혈청 D-dimer 측정의 진단적 가치)

  • Lim, Chae-Man;Kim, Hong-Kyu;Choi, Kang-Hyun;Lee, Sand-Do;Koh, Youn-Suck;Kim, Woo-Sung;Jang, Jae-Suck;Kim, Dong-Soon;Kim, Won-Dong
    • Tuberculosis and Respiratory Diseases
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    • v.43 no.1
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    • pp.69-74
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    • 1996
  • Background: The diagnosis of pulmonary embolism (PE) based on clinical findings is often elusive and therefore requires confirmative diagnostic method. Pulmonary angiography, though the gold standard for the diagnosis of pulmonary embolism, is an invasive method and requires trained personnel and special equipment. Lung V/Q scan, on the other hand, is a noninvasive method but the diagnostic specificity and sensitivity arc not satisfactory in case that the results are either intermediate or low probability scan. Plasma D-dimer is generated when a thrombus is fibrinolysed by plasmin and is known to be increased in various thrombotic disorders. The aim of this study was to investigate the value of the determination of plasma D-dimer level in the diagnosis of pulmonary embolism. Methods: Pulmonary angiography was performed in 17 patients who were clinically suspected to have pulmonary embolism. 9 patients(PE, $56{\pm}13.4$ yrs, M:F=8:1) were diagnosed to have pulmonary embolism by pulmonary angiography. The control group were the 8 patients with negative pulmonary angiography and 13 orthopedic patients with no evidence of pulmonary embolism on scintigraphic and impedance plethysmographic studies(n=21) (non-PE, $54.5{\pm}11.1$ yrs, M:F=11:10). Plasma D-dimer was measured by latex agglutination method in study subjects and the results were analyzed according to the presence or absence of pulmonary embolism. Results: 1) The increased level of plasma D-dimer was more frequently observed in the patients with pulmonary embolism than in the controls(>0.5 mg/L, 8 in PE, 10 in non-PE; <0.5 mg/L, 1 in PE, 11 in non-PE, p=0.049). 2) The diagnostic value of plasma D-dimer level higher than 0.5 mg/L were as follows: sensitivity 88.9%(8/9), specificity 52.4%(11/21), positive predictive value 44.4%(8/18), and negative predictive value 91.7%(11/12). Conclusion: Plasma D-dimer determination showed high sensitivity and negative predictive value in the diagnosis of pulmonary embolism and is therefore thought to be useful in excluding the possibility of pulmonary embolism.

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Ozone Generation Characteristics in Dielectric Barrier Discharge (유전체 장벽 방전내에서 오존발생 특성)

  • Lee, Hyeong-Ho;Jo, Guk-Hui;Kim, Yeong-Bae;Seo, Gil-Su
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.49 no.12
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    • pp.673-678
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    • 2000
  • The dielectric barrier discharge(DBD) is a common method to create a nonthermal plasma in which electrical energy is used to create electrons with a high average kinetic energy. The unique aspect of dielectric barrier discharges is the large array of short lifetime(10ns) silent discharges created over the surface of the dielectric. A silent discharge is generated when the applied voltage exceeds the breakdown voltage of the carrier gas creating a conduction path between the applied electrode and grounded electrode. As charge accumulates on the dielectric, the electric field is reduced below the breakdown field of the carrier gas and the silent discharge self terminates preventing the DBD cell from producing a thermal arc. In fact, the most significant application of dielectric barrier discharges is to generate ozone for contaminated water treatment. Therefore, experiments were perfomed at 1∼2[bar] pressure using a coaxial geometry single dielectric barrier discharge for ozone concentrations and energy densities. The main result show that the concentration and efficiency of ozone are influenced by gas nature, gas quantity, gas pressure, supplied voltage and frequency.

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Development of 3.6 MW, 4 ${\mu}s$, 200 pps Pulse Modulator for a High power magnetron (고출력 마그네트론 구동용 3.6 MW, 4 ${\mu}s$, 200 pps 펄스모듈레이터 개발)

  • Son, Y.G.;Jang, S.D.;Oh, J.S.;Cho, M.H.;NamKang, W.;Lee, H.K.;Bae, Y.S.;Lee, K.T.;Son, B.H.
    • Proceedings of the KIEE Conference
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    • 2004.07c
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    • pp.1778-1780
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    • 2004
  • Microwave heating system of KSTAR consists of ECH and LHCD. ECH and LHCD offer the reliability of operation in the beginning of plasma formation and non-inductive current drive for long time steady state operation with maintaining MHD stability, respectively. LHCD demands 5 GHz of frequency and consists of c-band waveguide, 4-port circuitor, dry dummy load, dual directional coupler, E-bend, arc detector. Our system is a lineup type pulse modulator that has 45 kV of output pulse voltage, 90 A of pulse current, 4 us of pulse width. 1:4 step-up pulse transformer, 7 stages of PFN and thyratron tube (E2V, CX1191D) are used in this modulator. The purpose of this paper is to show the modulator design and experimental result.

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Enhancement of biodegradability of the Refractory Organic Substances in Aqueous Solution with Discharged Water Generating (DWG) System (방전시스템(Discharged Water Generator)을 이용한 난분해성 물질의 생분해능 향상에 관한 연구)

  • Yeo, Inho;Ryu, Seung Min;Park, Heekyung
    • Journal of Korean Society of Water and Wastewater
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    • v.20 no.1
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    • pp.79-85
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    • 2006
  • Innovated technique to oxidize pollutants has been developed. The technique for this study uses plasma discharge in 2-phase (Air-Water) and is called Discharged Water Generating (DWG) system. It produces electric arc which generates not only the physical decomposing power against the pollutants but also oxidants to sterilize pollutants depending on the inlet gas species. These physical and chemical products play an important role in COD decrease and biodegradability enhancement. The enhancement of biodegradability for the refractory organic substances in aqueous solution was estimated in this study. Argon discharge reduced NBDCOD of EDTA from 58.7mg/L to 38.8mg/L, but oxygen discharge and ozonation reduced it to 37.74mg/L and 38.73mg/L respectively. Furthermore, Argon discharge changed 1181mg/L of NBDCOD of dye effluent into 606mg/L but oxygen discharge and ozonation changed it into 888mg/L and 790mg/L respectively.

EFFECT OF EACH LIGHT CURING UNITS ON THE MICROHARDNESS AND MICROLEAKAGE OF COMPOSITE RESIN (각각의 광조사기가 복합레진의 미세경도와 미세누출에 미치는 영향)

  • Jung, Eu-Jin;Lee, Hee-Joo;Hur, Bock
    • Restorative Dentistry and Endodontics
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    • v.29 no.1
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    • pp.58-67
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    • 2004
  • The objectives of this study was to evaluate current visible light curing units regarding microhardness and microleakage. Fourty samples of composite resin(Z-250, 3M) were cured by different light curing units (Flipo, LOKKI; Credi II, 3M; XL 3000, 3M: Optilux 500, Demetron) in acrylic blocks. Microhardness was measured using a calibrated Vickers indenter on both top and bottom surfaces after 24 hours of storage in air at room temperature. Class V cavities were prepared on buccal and lingual surfaces of fourty extracted human molars. Each margin was on enamel and dentin/cementum. Composite resin(Z-250, 3M) was filled in cavities and cured by four different light curing units (Flipo, LOKKl; Credi II, 3M; XL 3000, 3M: Optilux 500, Demetron). The results of this syudy were as follows: Microhardness 1. Flipo showed low microhardness compared to Optilux 500, Credi II significantly in upper surface. Flipo didn't show a significant difference compared to XL 3000. 2. The microhardness resulting from curing with Flipo was lower than that of others on lower surfaces. Microleakage 1. Dentin margin showed significantly high dye penetration rate than enamel margin in all groups(p<0.05). 2. No significant differences were found on both enamel and dentin margin regarding curing units.

Processing and Properties of Engine Valve-shaped TiAl-Mn Intermetallics by Reactive Sintering (반응소결법에 의해 엔진밸브 형상으로 제조한 TiAl-Mn 금속간화합물의 특성)

  • 김영진
    • Journal of Powder Materials
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    • v.4 no.4
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    • pp.243-251
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    • 1997
  • Engine valve-shaped TiAl-Mn intermetallics containing 43.5 to 47.5at%Al (Mn/Al=0.036) are successively fabricated by reactive sintering the elemental powder mixtures near-net shaped by extrusion and die forging. A duplex structure consisted of lamellar grains and equiaxed $\gamma$ grains is developed for all compositions, and the areal fraction of the lamellar grains(or equiaxed $\gamma$ grains) decreases (or increases) with increasing Al content. As Al content increased, the elongation increases with accompanying decrease in yield strength and ultimate tensile strength at both room temperature and 80$0^{\circ}C$. This indicates that the suitable composition is Ti-45at%Al-1.6at%Mn in considering the balance of ambient and elevated tensile properties. The reactive-sintered Ti-45Al-1.6Mn alloy shows superior oxidation resistance not only to the plasma arc melted one but also to the heat resistance steel STR35(representative exhaust valve head material for automotive engine). The reactive-sintered Ti-45Al-1.6Mn alloy coated with an oxidizing scale exhibits a better wear resistance than induction hardened martensitic steel STR11(representative exhaust valve tip material for automotive engine).

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