• 한국표면공학회지
• /
• 제53권5호
• /
• pp.249-256
• /
• 2020

As the size of manufacturing equipment for LCD and OLED displays increases, replacement of existing heavy stainless steel components with light metals, such as aluminum alloys, is being more important in semiconducting and display manufacturing industries. To use aluminum alloys for components in semiconducting and display industries, it is important to develop a new anodization method for improved performance of anodic oxide films than conventional anodization method based on sulfuric acid. In this work, optimum applied current density and the best sealing methods for anodic oxide films in 3% oxalic acid were explored. Experimental results showed 2.5 A/dm2 is the best applied current density for improved hardness and dielectric breakdown voltage. Sealing of the anodic oxide films further improved their hardness, dielectric breakdown voltage and resistance to HCl, by which application of anodic oxide films become applicable for components in semiconducting and display industries.

• Composites Research
• /
• 제13권4호
• /
• pp.42-53
• /
• 2000

차세대 항공기소재로 관심을 가지고 있는 Al 7075/CFRP 적층 복합재인 CARALL(CARbon ALuminum Laminates)하이브리드 복합소재 제조를 위한 중요조건중의 하나인 Al 표면처리조건과 경화방법에 대해 조사하였다. 항공기용 Al 전처리 중 대표적인 것으로 증기탈지, 크롬산 양극산화 피막처리, 황산-중크롬산 나트륨 에칭처리 및 인산 양극산화 피막처리공정이 있다. 본 실험에서는 상기 전처리 공정을 모두 항공 규격에 준해서 실시하여 Lap shear 및 Bell peel strength를 비교함으로써 효과적인 접착강도를 나타내는 표면처리 공정을 찾아내고, 시편의 자연표면상태를 그대로 관찰할 수 있는 AFM(Atomic Force Microscope)장비를 이용하여 각 전처리 시편의 표면형상을 측정함으로써 표면형상과 접착강도와의 상관관계를 고찰 하였다. 그리고 Al 표면처리와 별도로 Al과 접착제 및 탄소섬유 프리프레그를 동시에 경화시키는 방법과 탄소섬유 프리프레그를 미리 경화시킨후 다시 Al과 탄소섬유 라미네이트를 접착필름을 이용하여 재 접착시키는 이차 경화법을 적용하여 상호 접착강도 및 물성을 비교하였다. 또한 이차경화법에서의 오토클레이브 압력 변화와 DMA(Dynamic Mechanical Analysis) 장비를 이용한 접착필름의 유리전이온도($T_g$) 측정을 통해 효과적인 공정압력 및 접착내구성 유지에 필요한 최소 경화시간을 파악하였다. 상기 결과로부터 정밀 치수관리가 필요하며 고접착강도, 내구성 항공기 부품을 제작하기 위한 알루미늄 표면처리 공정과 복합재 경화공정 조건을 제시하고자 하였다.

• 대한치과보철학회지
• /
• 제42권5호
• /
• pp.556-571
• /
• 2004

Statement of problem: Surface texture of the implant is one of the important factors of the implant success, especially in the immediate implant loading. Many methods of the surface treatment of implant have developed and introduced. Purpose : This study was to evaluate the effects of the Ca-P coating implant crystallized the hydroxyapatite on the surface by the removal torque test and the histomorphometric analysis in vivo. Material and methods: 135 screw type implants, 4.0mm in length and 3.75mm in diameter were used in this study. Implants were divided into 3 groups and treated in the different mothods. Group I was not treated, Group II was treated in the SLA method, and Group III was treated in the Ca-P coating with the anodizing method and the hydroxyapatite was crystallized on the surface with the hydrothermal treatment. Firstly, the surface roughness of each group was measured, 45 rabbits were used in this experiment. Two implants were inserted on right tibial metaphysis and one implant was inserted on left side with the alternating order. After the healing periods of 3, 5, and 12 weeks, the rabbits were sacrificed to evaluate the osseointergration by the removal torque test and the histomorphometric analysis. Results : 1. In the analysis for the surface roughness, Group II showed the highest roughness. And Group III showed higher secondly. There was a significant difference one another statistically 2. In the removal torque test, Group III and II were significantly higher than Group I. There was no statistical difference between Group III and Group II. 3. For all Groups, the removal torque values at 12th week were significantly higher than at 3rd and 5th week. 4. In histomorphometric analysis, the bone implant contact rates of Group III and II were higher than that of Group I at 3rd and 5th week. There was a significant difference at 5th week. 5. In histomorphometric analysis, the bone implant contact rate of Group III and II increased from 3rd week to 5th week, but decreased at 12th week. In Group I, the contact rate at 12th week was significantly higher than at 3rd week and 5th week.

• 한국정밀공학회지
• /
• 제33권12호
• /
• pp.993-998
• /
• 2016

In today's manufacturing industries, the demand for light non-ferrous materials is considerable due to the need to improve productivity and manufacturability. Since the surface roughness of a material is important for improving the functionality of machined parts, various techniques for surface treatments have been developed to obtain non-ferrous materials with low roughness. A superfinishing method utilizing polishing films is generally applied to the anodized surface of Al7075 in order to improve its roughness. The objective of this research is to determine through experiment the parameters that facilitate the shortest processing time, using a superfinishing method, for reaching a roughness of Ra $0.2{\mu}m$. This objective is met by applying the Taguchi method in the experiments. Through the experiments of superfinishing, the effectiveness of the parameters adopted for the surface treatment is demonstrated.

• 대한치과보철학회지
• /
• 제44권5호
• /
• pp.594-605
• /
• 2006

Statement of problem: Modification of titanium implant surface has potential to ensure clinically favorable performance that several surface modification technologies have been introduced. Among the methods. anodizing method and sol-gel hydroxyapatite coating method have gained much interest due to its roughness and chemical composition of the coating layer, but more of its biocompatibility result is required. Purpose : The purpose of this study was to compare bone-implant interface shear strength of four different surface treated implants as time elapsed. Resonance frequency analysis(RFA) and removal torque measurement methods were employed to measure implant stability at one week and six week after implantation. Material and method: A total of 80 screw-shaped implant [20 machined, 20 resorbable media blasted(RBM), 20 anodized, and 20 anodized+hydroxyapatite sol-gel coated] were prepared, and one of each group was implanted in the tibia of a New Zealand white rabbit that total 20 of them were used. In order to test the implant stability and implant-tissue interface contact changing in the bone bed, each 10 rabbit were sacrificed 1 week and 6 week later while resonance frequency and removal torque were measured. One-way analysis of variance and the Tukey test were used for statistical analysis. Results : The results were as follows. 1. There was no statistically significant difference of implant stability quotients(ISQ) value in RFA between individual groups after 1 week of implantation and 6 weeks(p>0.05). But, there was statistically significant increase of ISQ value in 6 weeks group compared to 1 week group(p<0.05). 2. There was no statistically significant difference in removal torque analysis between individual groups after 1 week of implantation and 6 weeks(p>0.05). but there was statistically significant increase in all 4 groups after 6 weeks compared to 1 week later(p<0.05). 3. There was no statistically significant difference in removal torque analysis between anodized group and HA coating after anodic oxidation 6 weeks later(p>0.05), but significant difference was appeared in both groups compared to RBM group and smooth-machined group(p<0.05). Conclusions : It can be suggested that changes in surface characteristics affect bone reactions. Anodized and anodized+hydroxyapatite sol-gel coating showed significantly improved bone tissue response to implants, but further study on the effect of hydroxyapatite dissolution is needed.

• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2007년도 춘계학술대회 논문집
• /
• pp.368-370
• /
• 2007

AAO(Anodic Aluminum Oxidation) method has been known that it is practically useful for the fabrication of nano-structures and makes it possible to fabricate the highly ordered nano masters on large surface and even on the 2.5 or 3D surface at low cost comparing to the expensive e-beam lithography or the conventional silicon processing. In this study, by using the multi-step anodizing and etching processes, highly ordered nano patterned master with concave shapes was fabricated. By varying the processing parameters, such as initial matter and chemical conditions; electrical and thermal conditions; time scheduling; and so on, the size and the pitch of the nano pattern can be controlled. Consequently, various alumina/aluminum nano structures can be easily available in any size and shape by optimized anodic oxidation in various aqueous acids. The resulting good filled uniform nano molded structure through hot embossing molding process shows the validity of the fabricated nano pattern masters.

• 대한전자공학회:학술대회논문집
• /
• 대한전자공학회 2008년도 하계종합학술대회
• /
• pp.489-490
• /
• 2008

As anodizing method using poly-Si (polycrystalline silicon) grown by LPCVD (Low Pressure Chemical Vapor Deposition), a ballistic electron emitter was made. An OPPS (Oxidized Porous Poly-Si) structure can generate ballistic electron which can pass through without scattering owing to electric field of oxide layer wrapped around nanocrystal due to applied voltage of between surface and bottom electrode. As electrode, (Al, Au and Pt/ti) were used. In this case, there were the better characteristics in Al and Pt/ti than in Al and Au.

• 대한기계학회:학술대회논문집
• /
• 대한기계학회 2003년도 춘계학술대회
• /
• pp.273-278
• /
• 2003

Recently, high-performance hybrid composite materials have been used for various industrial fields because of their superior high strength, high stiffness and lower weight. In this study, manufactured hybrid composite materials are composed of two parts. One is hard-anodized Al5083-O alloy as a face material and the other is high strength aramid fiber ($Twaron^{(R)}$ CT709) laminates as a back-up material. Resistance to penetration is determined by protection ballistic limit($V_{50}$, a static velocity with 50% probability for complete penetration) test method. $V_{50}$ tests with $0^{\circ}$obliquity at room temperature were conducted with 5.56mm ball projectiles that were able to achieve near or complete penetration during high velocity impact tests.

• 한국정밀공학회:학술대회논문집
• /
• 한국정밀공학회 2003년도 춘계학술대회 논문집
• /
• pp.1378-1381
• /
• 2003

Recently, high-performance composite materials have been used for various industrial fields because of their superior high strength, high stiffness and lower weight. In this study, manufactured fiber reinforced metal laminate materials are composed of two parts. One is hard-anodized A15083-O alloy as a face material and the other is high strength aramid fiber (Twaron CT709) and polyethylene fiber(Dyneema HB25) laminates as a back-up material. Resistance to penetration is determined by protection ballistic limit(V$\sub$50/, a static velocity with 50% probability for complete penetration) test method. V$\sub$50/ tests with 0$^{\circ}$ obliquity at room temperature were conducted with 5.56mm ball projectiles that were able to achieve near or complete penetration during high velocity impact tests.

• 한국표면공학회:학술대회논문집
• /
• 한국표면공학회 2014년도 추계학술대회 논문집
• /
• pp.162-163
• /
• 2014

Aluminum anodizing is a technique that can be formed pores well aligned various diameters. We were prepared CNFs using the polymer as carbon source using the AAO as a template. CNFs can be heat treated at $1400^{\circ}C$ and became soft carbon. It showed electrochemical behavior by Crystallization. In this experiment, I was observing the behavior as a anode material for LIC of CNFs having different diameters.