• Title/Summary/Keyword: Analytical Analysis

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Determination of phosphorous in lubricating oil by XRF and NMR methods (XRF 및 NMR 법에 의한 윤활유 중의 인 함량 비교분석 연구)

  • Lim, Heon-Sung;Han, Gee-Chung;Lee, Sueg-Geun
    • Analytical Science and Technology
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    • v.18 no.2
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    • pp.168-172
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    • 2005
  • A comparison study of XRF and $^{31}P$-NMR method for the analysis of phosphorous in lubricating oil has been described. Pure oil and water were used for the observation of matrices effect variation by different analytical methods. Quantitative analysis was carried out by XRF and $^{31}P$-NMR using real samples. Significant difference is observed from the slopes on the calibration curves by the XRF due to the matrices (water: 124.0, oil: 276.6). While the result obtained from XRF showed a large matrix effect, the slopes obtained from $^{31}P$-NMR results of two different matrices, however, are in good agreement ranged of ${\pm}9%$ (water: 4.9, oil: 5.3).

Analytical Method to Analyze the Effect of Tolerance on the Modal Characteristic of Multi-body Systems in Dynamic Equilibrium (동적 평형위치에 있는 다물체계의 모드특성에 미치는 공차의 영향 분석을 위한 해석적 방법)

  • Kim, Bum-Suk;Yoo, Hong-Hee
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2007.05a
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    • pp.109-114
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    • 2007
  • Analytical method to analyze the effect of tolerance on the modal characteristic of multi-body systems in dynamic equilibrium position is suggested in this paper. Monte-Carlo Method is conventionally employed to perform the tolerance analysis. However, Monte-Carlo Method spends too much time for analysis and has a greater or less accuracy depending on sample condition. To resolve these problems, an analytical method is suggested in this paper. By employing the sensitivity information of mass, damping and stiffness matrices, the sensitivities of damped natural frequencies and the transfer function can be calculated at the dynamic equilibrium position. The effect of tolerance on the modal characteristic can be analyzed from tolerance analysis method.

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Analysis of Trace Trichlorosilane in High Purity Silicon Tetrachloride by Near-IR Spectroscopy (근적외선 분광법을 이용한 고순도 SiCI4 중의 미량 불순물 SiHCI3의 분석)

  • Park, Chan-Jo;Lee, Sueg-Geun
    • Analytical Science and Technology
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    • v.15 no.1
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    • pp.87-90
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    • 2002
  • The content of $SiHCl_3$ as a trace impurity in $SiCl_4$ was analyzed by Near IR spectrophotometer with optical fiber. The strong absorption bands of $5345{\sim}5116cm^{-1}$ and $4848{\sim}4349cm^{-1}$ were used for analysis of $SiHCl_3$, and the detection limit of impurity $SiCl_3$ was appeared to be 0.005 % in the spectrum. The quantitative analysis by Near IR spectrophotometry showed the analytical possibility of trace impurity in $SiCl_4$ without sample pre-treatment not only in the laboratory but also in the field.

Quasi-3D analysis of Axial Flux Permanent Magnet Rotating Machines using Space Harmonic Methods (공간고조파법을 이용한 축 자속 영구자석 회전기기의 준(準)-3D 특성 해석)

  • Choi, Jang-Young
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.60 no.5
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    • pp.942-948
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    • 2011
  • This paper deals with characteristic analysis of axial flux permanent magnet (AFPM) machines with axially magnetized PM rotor using quasi-3-D analysis modeling. On the basis of magnetic vector potential and a two-dimensional (2-D) polar-coordinate system, the magnetic field solutions due to various PM rotors are obtained. In particular, 3-D problem, that is, the reduction of magnetic fields near outer and inner radius of the PM is solved by introducing a special function for radial position. And then, the analytical solutions for back-emf and torque are also derived from magnetic field solutions. The predictions are shown in good agreement with those obtained from 3-D finite element analyses (FEA). Finally, it can be judged that analytical solutions for electromagnetic quantities presented in this paper are very useful for the AFPM machines in terms of following items : initial design, sensitivity analysis with design parameters, and estimation of control parameters.

Time Domain Soil-Structure Interaction Analysis for Earthquake Loadings Based on Analytical Frequency-Dependent Infinite Elements (무한요소를 사용한 지반-구조물 상호작용계의 시간 영역 지진응답해석)

  • 김두기
    • Proceedings of the Earthquake Engineering Society of Korea Conference
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    • 1999.10a
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    • pp.107-112
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    • 1999
  • This paper presents a time domain method for soil-structure interaction analysis for seismic loadings. It is based on the finite element formulation incorporating analytical frequency-dependent infinite elements for the far-field soil. The dynamic stiffness matrices of the far-field region formulated in frequency domain using the present method can be easily transformed into the corresponding matrices in time domain. Hence the response can be analytical computed in time domain. Example analysis has been carried out to verify the present method for an embedded block in a multi-layered half-space. The present methods can be easily extended to the nonlinear analysis since the response analysis is carried out in time domain.

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The Senstivitiy Analysis and Optimiaztion for the Development of the SMD Performance (표면 실장기(SMD) 성능 개선을 위한 민감도 해석 및 최적화)

  • Cha, In-Hyuk;Han, Chang-Soo;Kim, Jung-Duck
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1996.04a
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    • pp.568-573
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    • 1996
  • In this paper, A design strategy of the Surface Mounting Device for accurate and better performance is studied. Analytical Modeling. Sensitivity analysis and optimization are being conducted. The ANSYS software and experimental method are used for verification of the analytical equations withboundary conditons. Through the sensitivity analysis, the most dominant design parameters can be detected. The optimum design parameters for performing given performing given perfomances are selected by using the optimization algorithm. The design tool based on the design strategy for the analysis, modeling and optimization will be useful for a re-design and better perofrmance of the SMD.

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The Sensitivity Analysis and Optimization for the Development of the SMD Performance (표면 실장기(SMD) 성능 개선을 위한 민감도 해석 및 최적화 방안)

  • Cha, In-Hyuk;Han, Chang-Soo;Kim, Jung-Duck
    • Journal of the Korean Society for Precision Engineering
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    • v.14 no.2
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    • pp.120-128
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    • 1997
  • In this paper, A design strategy of the Surface Mounting Device for accurate and better performance is studied. Analytical modeling, sensitivity analysis, and optimization are being conducted. The ANSYS software and experimental method are used for the verification of the analytical equations with boundary conditions. Through the sensitivity analysis, the most dominant design parameter can be detected. The optimum design parameters for improving the given performances are selected by using the optimiza- tion algorithm. The design tool based on the design strategy for the analysis, modeling, and optimization will be useful for are-design and better improving of the SMD.

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Analytical Fragility Curves for Bridge (교량의 해석적 손상도 곡선)

  • Lee, Jong-Heon
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.3 no.4
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    • pp.155-162
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    • 1999
  • This paper presents a generation of analytical fragility curves for bridge. The analytical fragility curves are constructed on the basis of nonlinear dynamic analysis. Two-parameter lognormal distribution functions are used to represent the fragility curves with the parameters estimated by the maximum likelihood method. To demonstrate the development of analytical fragility curves, two of representative bridges with a precast prestressed continuous deck in the Memphis. Tennessee area are used.

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