• Analytical Science and Technology
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• v.8 no.4
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• pp.505-509
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• 1995

The terpenoids in the volatile constituents of Liaoning Shcisandra Chinesis Baillon have been determined by the analytical method of GC/MS. Thirty terpenoids molecular structure were characterized. They are 11.89% monterpenes, 4.60% monoterpene oxides, 58.74% sesquiterpene hydrocarbons, and 1.62% oxygen-containing sesquiterpenoids in the total volatile constituents quantified by chromatograph. Among them, the sesquiterpene make up the characteristic constituents. Every terpenoid constituent percent content was obtained using area normalization method of HP-59970 chemstation.

• ETRI Journal
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• v.27 no.6
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• pp.810-813
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• 2005

This letter presents an analytical framework for a performance analysis of the imperfect direct-sequence code division multiple access (DS-CDMA) closed-loop power control (CLPC) loop with loop delay, channel estimation error, and power control command bit error as the parameters under a Rayleigh flat fading environment. The proposed model is verified through a comparison between analytical results and simulation ones.

• Analytical Science and Technology
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• v.36 no.4
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• pp.198-203
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• 2023

The reaction of cis-protected (Me4en)Pd(II) species with potentially multidentate bis(benzylthio)methylenepropanedioate (L) was carried out to obtain a monometallic compound, [(Me₄en)Pd(L)], in O,O'-coordination mode. The bis(benzylthio)methylene group was bent strikingly from the palladium square plane at the dihedral angle of 70.40°. The physicochemical properties of the present palladium(II) compound were fully characterized by means of infrared and nuclear magnetic resonance spectroscopy, thermogravimetric analysis, and single-crystal X-ray diffraction measurement.

• Structural Engineering and Mechanics
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• v.31 no.2
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• pp.163-180
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• 2009

In the design of tall reinforced concrete (R/C) buildings, the serviceability stiffness criteria in terms of maximum lateral displacement and inter-story drift must be satisfied to prevent large second-order P-delta effects. To accurately assess the lateral deflection and stiffness of tall R/C structures, cracked members in these structures need to be identified and their effective member flexural stiffness determined. In addition, the implementation of the geometric nonlinearity in the analysis can be significant for an accurate prediction of lateral deflection of the structure, particularly in the case of tall R/C building under lateral loading. It can therefore be important to consider the cracking effect together with the geometric nonlinearity in the analysis in order to obtain more accurate results. In the present study, a computer program based on the iterative procedure has been developed for the three dimensional analysis of reinforced concrete frames with cracked beam and column elements. Probability-based effective stiffness model is used for the effective flexural stiffness of a cracked member. In the analysis, the geometric nonlinearity due to the interaction of axial force and bending moment and the displacements of joints are also taken into account. The analytical procedure has been demonstrated through the application of R/C frame examples in which its accuracy and efficiency in comparison with experimental and other analytical results are verified. The effectiveness of the analytical procedure is also illustrated through a practical four story R/C frame example. The iterative procedure provides equally good and consistent prediction of lateral deflection and effective flexural member stiffness. The proposed analytical procedure is efficient from the viewpoints of computational effort and convergence rate.

• Analytical Science and Technology
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• v.32 no.3
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• pp.77-87
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• 2019

High viscosity carbon black dispersions are used in various industrial fields such as color cosmetics, rubber, tire, plastic and color filter ink. However, carbon black particles are unstable to heat due to inherent characteristics, and it is very difficult to keep the quality of the product constant due to agglomeration of particles. In general, particle size analysis is performed by dynamic light scattering (DLS) during the dispersion process in order to select the optimum dispersant in the carbon black dispersion process. However, the existing low viscosity analysis provides reproducible particle distribution analysis results, but it is difficult to select the optimum dispersant because it is difficult to analyze the reproducible particle distribution at high viscosity. In this study, dynamic light scattering (DLS) and asymmetrical flow field-flow fractionation (AsFlFFF) analysis methods were compared for reproducible particle size analysis of high viscosity carbon black. First, the stability of carbon black dispersion was investigated by particle size analysis by DLS and AsFlFFF according to milling time, and the validity of analytical method for the selection of the optimum dispersant useful for carbon black dispersion was confirmed. The correlation between color and particle size of particles in high viscosity carbon black dispersion was investigated by using colorimeter. The particle size distribution from AsFlFFF was consistent with the colorimetric results. As a result, the correlation between AsFlFFF and colorimetric results confirmed the possibility of a strong analytical method for determining the appropriate dispersant and milling time in high viscosity carbon black dispersions. In addition, for nanoparticles with relatively broad particle size distributions such as carbon black, AsFlFFF has been found to provide a more accurate particle size distribution than DLS. This is because AsFlFFF, unlike DLS, can analyze each fraction by separating particles by size.

• International Journal of Aeronautical and Space Sciences
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• v.12 no.2
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• pp.200-209
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• 2011

An analytical solution for rectangular laminated composite plates was obtained via a formal asymptotic method. From threedimensional static equilibrium equations, the microscopic one-dimensional and macroscopic two-dimensional equations were systematically derived by scaling of the thickness coordinate with respect to the characteristic length of the plate. The onedimensional through-the-thickness analysis was performed by applying a standard finite element method. The derived twodimensional plate equations, which take the form of recursive equations, were solved under sinusoidal loading with simplysupported boundary conditions. To demonstrate the validity and accuracy of the present method, various types of composite plates were studied, such as cross-ply, anti-symmetric angle-ply and sandwich plates. The results obtained were compared to those of the classical laminated plate theory, the first-order shear deformation theory and the three-dimensional elasticity. In the present analysis, the characteristic length of each composite was dependent upon the layup configurations, which affected the convergence rate of the method. The results shown herein are promising that it can serve as an efficient tool for the analysis and design of laminated composite plates.

• Journal of the Korean Society for Precision Engineering
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• v.26 no.8
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• pp.79-88
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• 2009

This paper presents the analytical stiffness analysis method for a low-DOF planar parallel manipulator. An n-DOF (n<3) planar parallel manipulator to which 1- or 2-DOF serial mechanism is connected in series may be used as a positioning device in planar tasks requring high payload and high speed. Differently from a 3-DOF planar parallel manipulator, an n-DOF planar parallel counterpart may be subject to constraint forces as well as actuation forces. Using the theory of reciprocal screws, the planar stiffness is modeled such that the moving platform is supported by three springs related to the reciprocal screws of actuations (n) and constraints (3-n). Then, the spring constants can be precisely determined by modeling the compliances of joints and links in serial chains. Finally, the stiffness of two kinds of 2-DOF planar parallel manipulators with simple and complex springs is analyzed. In order to show the effectiveness of the suggested method, the results of analytical stiffness analysis are compared to those of numerical stiffness analysis by using ADAMS.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.60 no.5
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• pp.955-964
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• 2011

In renewable energy system such as flywheel energy storage system, wind power and solar power, the motor/generator is the important key for offering the electric energy to the electric loads. For example, the heavy and large flywheel is rotated by electromagnetic torque of pemanent magnet synchronous motor (PMSM) and, in case of a breakdown of electric current, the PMSM used as generator supplies electric energy for the various electric utilities using mechanical rotation energy of the flywheel. Thus, design of a motor/generator should be performed in effort to reduce cogging torque and electromagnetic loss for high efficiency. In our paper, a slotless permanent magnet synchronous motor/generator (SPMSM/G) with output power 15kW at the rotor speed 18000rpm is designed from electromagnetic analysis and dynamic performance analysis. In analytical approach, design parameters such as back electro-motive force (back EMF), inductance and electromagnetic torque are derived from analytical method which is one of the electromagnetic analysis method. And using the design parameters, this paper deal with system design considering the driving characteristics and electric load in required power. Finally, the analytical results are verified by the experiment and finite element method (FEM).

• Proceedings of the Computational Structural Engineering Institute Conference
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• 2006.04a
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• pp.405-412
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• 2006

Among the various problems involved in the structural analysis of the Korean traditional wooden structure, the analytical model for the Kong-Po is controversial subject as usual. While some experiments are tried for establishing the basis of analytical models, most of these experiments are performed using scale down specimens. So, it is not possible to apply these experimental results to structural analysis of Korean traditional wooden structure directly. A numerical study for analogizing the stiffness of full scale Kong-Po structure is performed on the basis of experimental specimen. Some parameter studies using finite element method are made in this study. The finite element analysis used in this study is geometric material nonlinear analysis. The stiffness of Kong-Po structure found out in this study can be used for modelling the joints of the Korean traditional wood structure in frame analysis.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.13 no.1
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• pp.419-424
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• 2012

This study is a research on the buckling analysis of a portable prestressing device using finite element analysis program, ABAQUS. In order to produce 50m-span PSC girders using pretensioning method, a portable prestressing device has to endure a large jacking force about 10MN. Therefore it shall be safe and stable about the jacking force. In this study, the buckling analysis technique is developed and the buckling analysis of a portable prestressing device is performed using previous studies about the analytical model that the validity of the analytical model was demonstrated by comparing analytical results with experimental results. The stability of the device to produce 10m span PSC girders is investigated.