• 제목/요약/키워드: Aging treatment behavior

검색결과 119건 처리시간 0.024초

전자비임 용접한 250 및 300 Grade 18% Ni Maraging 강의 수소취화 거동에 관한 연구 (A study of hydrogen embrittlement behavior in E.B welded 250,300 grade 18% Ni maraging steel)

  • 윤한상;정병호
    • Journal of Welding and Joining
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    • 제5권2호
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    • pp.53-59
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    • 1987
  • The effect of applied stress, current density and heat-treatment after welding on the time to fracture, fracture behavior was investigated by the method of constant load tensile testing under catholic charging with hydrogen in E.B. welded 250,300 Grade 18% Ni Maraging steel sheet. The main results obtained are as follows: 1. All specimen showed the characteristic delayed failure and the time to fracture showed decreasing tendency with the increase in current density and applied stress. 2. Hydrogen embitterment susceptibility of notched specimen after solution-treatment and aging after welding was more increased than that of aged smooth specimen and as welded specimen. 3. Fracture surface showed a typical intergranular fracture on the border, a dimple pattern in the center of specimen and some quasi-cleavage fracture between the intergranular and the dimple.

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TiAl 금속간 화합물의 미세조직에 따른 고온변형특성 (High Temperature Deformation Behavior of Ti-Al Intermetallic Compound - Microstructure Effect)

  • 하태권;정재영;이광석;장영원
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2003년도 춘계학술대회논문집
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    • pp.295-298
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    • 2003
  • High temperature deformation behavior of a Ti-Al intermetallic compound has been investigated. Specimens with a near gamma and a lamella structures were obtained by performing heat treatment at 1200 and 1330$^{\circ}C$, respectively, for 24 hr and stabilized at 900$^{\circ}C$ for 4 hr followed by air cooling. A series of load relaxation tests has been conducted on these samples at temperatures ranging from 850 to 950$^{\circ}C$ to construct flow curves in the strain rate range from 10$\^$-6//s to 10$\^$-3//s. Strain hardening was observed even at the temperature of 950$^{\circ}C$ in both the near gamma and the lamella structures. Further aging treatment for 12 hr at test temperatures has found to cause no softening in both microstructures.

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Sc 첨가된 Al-Zn-Mg-(Cu)계 알루미늄 합금 압출재의 시효 경화 거동과 기계적 성질 (Age Hardening and Mechanical Property of Extruded Al-Zn-Mg-(Cu) Al Alloys with Sc addition)

  • 심성용;임수근
    • 열처리공학회지
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    • 제20권5호
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    • pp.243-249
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    • 2007
  • The age hardening behavior and mechanical properties of an extruded Al-Zn-Mg-(Cu)-0.1 wt.%Sc alloy were investigated with the Sc addition and ageing temperature. The results showed that the $Al_3Sc$ compounds were formed by Sc addition and distributed preferentially along the extrusion direction. The age hardening of Al-Zn-Mg-Cu-0.1 wt.%Sc alloy which was treated by T6 process was more significant than that of Al-Zn-Mg-0.1 wt.%Sc alloy. The tensile property of Al-Zn-Mg-Cu+0.1 wt.%Sc alloy was also higher than that of Al-Zn-Mg-0.1 wt.%Sc alloy, which is 691 MPa and 584 MPa in strength and 9% and 11% in elongation, respectively.

Fe-Co기 고인성 고강도강의 반복 열처리 거동 - Part 1. 조직제어 (The Repeat Heat Treatment Behavior of Double Remelted Fe-Co Ultra-high Strength Steel. - Part. 1 Microstructure Control)

  • 윤보희;박경태;이태혁;김재훈;김홍규;이성;이종현
    • 한국주조공학회지
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    • 제32권1호
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    • pp.32-37
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    • 2012
  • In this study, microstructural evaluation was carried out on secondary hardening type ultrahigh strength steel, Fe-Co-Ni composition. This paper as a first part of whole research presented the microstructural behavior by cyclic heat treatment. The cyclic heat treatment method includes normalizing, stress relieving, solution treatment and aging. Especially, solution treatments performed triple times to get maximized solution hardening. Phase transformation and microstructure were observed by using optical microscope (OM), Electron back-scattered diffraction (EBSD) and X-ray stress analyzer. During the triple solution treatment, size of grain boundary was dramatically decreased by generating a packet from the martensite transformation of residual austenite in the inner part of grain, whereas the hardness increase was not significant.

SiCp입자강화 Al 복합재료에 대한 합금원소의 영향과 시효특성에 관한 연구 (A Study on Ageing Characteristics and Alloy Elements of SiCp Reinforced Al Matrix Composites)

  • 김석원;이의종;우기도;김동건
    • 한국주조공학회지
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    • 제21권1호
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    • pp.7-14
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    • 2001
  • The research on new DRA(discontinuous reinforced alloy) and CRA(continous reinforced alloy) composites has been carried out to improve the properties of ceramic fiber and particle reinforced metal matrix composites(MMCs). Effects of alloying elements and aging conditions on the microstructures and aging behavior of Al-Si-Cu-Mg-(Ni)-SiCp composite have been examined. The specimens used in this study were manufactured by duplex process. The first squeeze casting is the process to make precomposite and the second squeeze casting is the process to make final composite. The hardening behavior was accelerated with decreasing the size of SiCp particle in the composites. It is considered that the dislocation density increased with increasing SiCp size, due to the different thermal deformation between Al matrix and SiCp during quenching after the solution treatment. Peak aging time to obtain the maximum hardness in 3 ${\mu}m$ SiCp reinforced Al composite was reduced than that in large size(5, 10 ${\mu}m$) of SiCp because of difference in dislocation density. Aging hardening responce(${\Delta}H$ = $H_{Max}.-H_{S.T}$) of composites was greater than that of unreinforced Al alloy because of higher density of second phases in matrix.

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Sn-4.0wt%Ag-0.5wt%Cu 솔더 접합계면의 강도특성과 미세파괴거동에 대한 In-situ관찰 (In-situ Observation on Micro-Fractural Behavior and Strength Characteristics in Sn-4.0wt%Ag-0.5wt%Cu Solder Joint Interface)

  • 이경근;최은근;추용호;김진수;이병수;안행근
    • 한국재료학회지
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    • 제18권1호
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    • pp.38-44
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    • 2008
  • The micro-structural changes, strength characteristics, and micro-fractural behaviors at the joint interface between a Sn-4.0wt%Ag-0.5wt%Cu solder ball and UBM treated by isothermal aging are reported. From the reflow process for the joint interface, a small amount of intermetallic compound was formed. With an increase in the isothermal aging time, the type and amount of the intermetallic compound changed. The interface without an isothermal treatment showed a ductile fracture. However, with an increase in the aging time, a brittle fracture occurred on the interface due mainly to the increase in the size of the intermetallic compounds and voids. As a result, a drastic degradation in the shear strength was observed. From a microshear test by a scanning electron microscope, the generation of micro-cracks was initiated from the voids at the joint interface. They propagated along the same interface, resulting in coalescence with neighboring cracks into larger cracks. With an increase in the aging time, the generation of the micro-structural cracks was enhanced and the degree of propagation also accelerated.

Influence of the preparation design and artificial aging on the fracture resistance of monolithic zirconia crowns

  • Mitov, Gergo;Anastassova-Yoshida, Yana;Nothdurft, Frank Phillip;See, Constantin von;Pospiech, Peter
    • The Journal of Advanced Prosthodontics
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    • 제8권1호
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    • pp.30-36
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    • 2016
  • PURPOSE. The aim of this study was to evaluate the fracture resistance and fracture behavior of monolithic zirconia crowns in accordance with the preparation design and aging simulation method. MATERIALS AND METHODS. An upper first molar was prepared sequentially with three different preparation designs: shoulderless preparation, 0.4 mm chamfer and 0.8 mm chamfer preparation. For each preparation design, 30 monolithic zirconia crowns were fabricated. After cementation on Cr-Co alloy dies, the following artificial aging procedures were performed: (1) thermal cycling and mechanical loading (TCML): 5000 cycles of thermal cycling $5^{\circ}C-55^{\circ}C$ and chewing simulation (1,200,000 cycles, 50 N); (2) Low Temperature Degradation simulation (LTD): autoclave treatment at $137^{\circ}C$, 2 bar for 3 hours and chewing simulation; and (3) no pre-treatment (control group). After artificial aging, the crowns were loaded until fracture. RESULTS. The mean values of fracture resistance varied between 3414 N (LTD; 0.8 mm chamfer preparation) and 5712 N (control group; shoulderless preparation). Two-way ANOVA analysis showed a significantly higher fracture loads for the shoulderless preparation, whereas no difference was found between the chamfer preparations. In contrast to TCML, after LTD simulation the fracture strength of monolithic zirconia crowns decreased significantly. CONCLUSION. The monolithic crowns tested in this study showed generally high fracture load values. Preparation design and LTD simulation had a significant influence on the fracture strength of monolithic zirconia crowns.

국내 노인전문병원 병동부 공용공간의 이용 행태에 관한 연구 - 데이룸 및 복도를 중심으로 (An Architectural Study on the Patient's behavior of Public Space in Geriatrics Hospital - Focused on day-room and aisle of a hospital ward -)

  • 김춘성;김상복;양내원
    • 의료ㆍ복지 건축 : 한국의료복지건축학회 논문집
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    • 제13권4호
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    • pp.7-14
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    • 2007
  • Korea is entered to the aging society with 21C. Also it is forecast we will enter in aging society quickly. for 5 years there are some growth in facility at least 2~3 times but our society needs more. But this quantitative growth is worried about less quality. That's why we needs more research about the facility for an geriatrics hospital. The people who suffered from senile disease needs more treatment days in the ward of geriatric hospital. so we have to consider about better condition in ward of geriatrics than in general. Better environment for eldery is included not only the ward space but also the corridor and the dayroom. This study which it performed to improve their habitability is researched on public space. and this reserch deal with general feature against a public space in the ward of geriatric, and investigate 2 facility for divede the the general feature of the space. and this investigate is recorded according to behavior of patients. It can find us which factor of the space is prefered by them.

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Microstructure of Laser Surface Melted Ni-Base Alloy 600 after Heat Treatment

  • Lim, Yun-Soo;Cho, Hai-Dong;Kuk, Il-Hiun;Kim, Joung-Soo
    • 한국원자력학회:학술대회논문집
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    • 한국원자력학회 1998년도 춘계학술발표회논문집(2)
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    • pp.66-71
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    • 1998
  • A study of treatment effects on laser surface melted Ni-base alloy 600, especially on precipitation behavior ad chemical composition changes on the grain boundary were conducted with microscopic equipments. Long-term aging treatment at 40$0^{\circ}C$ caused no considerable effects on the grain boundary properties. Cr-rich M$_2$$_3$C$_{6}$ and Cr$_{7}$C$_3$ carbides were precipitated and the resultant Cr depletion below 12 wt pct on some high angle grain boundaries was occurred by heat treatment at $600^{\circ}C$ for 24 hours. These results can imply that the resistance of intergranular stress corrosion cracking of heat treated alloy 600 might not be changed considerably in comparion with the as-LSM one.e.e.

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1Cr-1Mo-0.25V 강의 열화거동에 관한 연구 (A Study on Degradation Behavior of 1Cr-1Mo-0.25V Steel)

  • 석창성;구재민;김동중;안하늘;박은수
    • 한국안전학회지
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    • 제15권4호
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    • pp.8-14
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    • 2000
  • The remaining life estimation for the aged components in power plants as well as chemical plants are very important because mechanical properties of the components are degraded with time of service exposure in the high temperature. Since it is difficult to take specimens from the operating components to evaluate mechanical properties of components, accelerated aging technique are needed to estimate and analyse the material degradation. In the this study, test materials with 4 different degradation levels were prepared by isothermal aging heat treatment at $630^{\circ}C$. And tensile test, $k_{IC}$ test, hardness test and Scanning Electron Microscope analysis were performed in order to evaluate the degradation of 1Cr-1Mo-0.25V steels.

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