• 제목/요약/키워드: Aging heat treatment

검색결과 313건 처리시간 0.025초

교반관법으로 제조한 Mg-Al-Zn-X합금의 기계적 특성 (Microstructure and Mechanical Properties of Mg-Al-Zn-X Alloys Fabricated by Rotation-Cylinder Method)

  • 이정일;이주호;김영호;홍태환;이후인;박진태;김준수;박형규
    • 열처리공학회지
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    • 제19권2호
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    • pp.96-102
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    • 2006
  • Development of Rotation-Cylinder Method(RCM) is given for Mg-Al-Zn-X(X=Sr) alloys, identifying some of the key factors that need to be controlled and indicating subsequent casting processes. Effects of Sr addition on the microstructure and mechanical properties of as-cast and T6 heat-treated Mg-Al-Zn-X alloys fabricated by the RCM were investigated. The microstructural and mechanical characterizations were performed by utilizing optical microscope, scanning electron microscope, transmission electron microscope, hardness test and ultimate tensile test. The solution and aging treatment time was varied to optimize the T6 heat treatment conditions, and experimental results were discussed. The grain size of Sr containing alloys was refined by increasing Sr content, but the tensile and yield strengths were increased by addition up to 1wt% Sr.

Lifespan Extending and Stress Resistant Properties of Vitexin from Vigna angularis in Caenorhabditis elegans

  • Lee, Eun Byeol;Kim, Jun Hyeong;Cha, Youn-Soo;Kim, Mina;Song, Seuk Bo;Cha, Dong Seok;Jeon, Hoon;Eun, Jae Soon;Han, Sooncheon;Kim, Dae Keun
    • Biomolecules & Therapeutics
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    • 제23권6호
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    • pp.582-589
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    • 2015
  • Several theories emphasize that aging is closely related to oxidative stress and disease. The formation of excess ROS can lead to DNA damage and the acceleration of aging. Vigna angularis is one of the important medicinal plants in Korea. We isolated vitexin from V. angularis and elucidated the lifespan-extending effect of vitexin using the Caenorhabditis elegans model system. Vitexin showed potent lifespan extensive activity and it elevated the survival rates of nematodes against the stressful environments including heat and oxidative conditions. In addition, our results showed that vitexin was able to elevate antioxidant enzyme activities of worms and reduce intracellular ROS accumulation in a dose-dependent manner. These studies demonstrated that the increased stress tolerance of vitexin-mediated nematode could be attributed to increased expressions of stress resistance proteins such as superoxide dismutase (SOD-3) and heat shock protein (HSP-16.2). In this work, we also studied whether vitexin-mediated longevity activity was associated with aging-related factors such as progeny, food intake, growth and movement. The data revealed that these factors were not affected by vitexin treatment except movement. Vitexin treatment improved the body movement of aged nematode, suggesting vitexin affects healthspan as well as lifespan of nematode. These results suggest that vitexin might be a probable candidate which could extend the human lifespan.

Al-Mg-X (X=Cr, Si)합금의 기계적성질에 미치는 결정립크기와 시효조건의 영향 (Effect of Grain Size and Aging Conditions on Mechanical Properties of Al-Mg-X (X=Cr,Si) Alloy)

  • 한창석;이찬우
    • 열처리공학회지
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    • 제36권2호
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    • pp.77-85
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    • 2023
  • In this study, the mechanical properties of the Al-Mg-X (X=Cr, Si) alloy, which clearly showed the influence of the specimen and grain size, were investigated by changing the specimen size extensively. In addition, the effect on the specimen size, grain size and aging condition on the mechanical properties of the grain refining alloy according to the addition of Cr was clarified, and the relationship between these factors was studied. As the specimen size decreased, the yield stress decreased and the fracture elongation increased. This change was evident in alloys with coarse grain sizes. Through FEM analysis, it was confirmed that the plastic deformation was localized in the parallel part of specimen S2. Therefore, when designing a tensile specimen of plate material, the W/L balance should be considered along with the radius of curvature of the shoulder. In the case of under-aged materials of alloys with coarse grain size, the fracture pattern changed from intergranular fracture to transgranular fracture as W/d decreased, and δ increased. This is due to the decrease in the binding force between grains due to the decrease in W. In the specimen with W/d > 40 or more, intergranular fracture occurred, and local elongation did not appear. Under-aged materials of alloys with fine grain size always had transgranular fracture over a wide range of W/d = 70~400. As W/d decreased, δ increased, but the change was not as large as that of alloys with coarse grain sizes. Compared to the under-aged material, the peak-aged material did not show significant dependence on the specimen size of σ0.2 and δ.

알루미늄 합금 볼트의 제조 공정 설계 (Manufacturing Process Design of Aluminum Alloy Bolt)

  • 김지환;채수원;한승상;손요헌
    • 한국정밀공학회지
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    • 제27권5호
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    • pp.63-68
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    • 2010
  • The use of aluminum alloy parts in the automotive industry has been increasing recently due to its low weight compared with steel to improve fuel efficiency. Companies in the auto parts' manufacturing sector are expected to meet the government's strict environmental regulations. In this study, manufacturing process of aluminum alloy bolt has been designed from forming to heat treatment. Bolt forming process is composed of cold forging for body and rolling for thread. In this study only cold forging process is considered by employing the finite element method. In the cold forging process, preform shape was designed and damage value was considered for die design. Two steps of forging process has been developed by the simulation and a prototype was manugactured accordingly. As a final process, solution heat treatment and aging process was employed. A final prototype was found to meet the required specifications of tensile strength and dimension.

열처리에 따른 제2상 석출이 Al-4.5%Cu 합금의 열 물성에 미치는 영향 (Influences of Precipitation of Secondary Phase by Heat Treatment on Thermal Properties of Al-4.5%Cu Alloy)

  • 최세원
    • 한국재료학회지
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    • 제30권8호
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    • pp.435-440
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    • 2020
  • The relationship between the precipitation of secondary phase and the thermal properties of Al-4.5%Cu alloy (in wt.%) after various heat treatments has been studied. Solid solution treatment of alloy was performed at 808 K for 6 hours, followed by warm water quenching; then, the samples were aged in air at 473 K for different times. The thermal diffusivity of the Al-4.5%Cu alloy changed with the heat treatment conditions of the alloy at temperatures below 523 K. The as-quenched specimen had the lowest thermal diffusivity, and as the artificial aging time increased, the thermal diffusivity of the specimen increased in the temperature range between 298 and 523 K. For the specimen aged for five hours, the thermal conductivity was 12% higher than that of the as-quenched specimens at 298 K. It is confirmed that the thermal diffusivity and thermal conductivity of the Al-4.5%Cu alloy significantly depend on their thermal history at temperatures below 523 K. The precipitation and dissolution of the Al2Cu phase were confirmed via DSC for the alloys, and the formation of coefficient of thermal expansion peaks in TMA was caused by precipitation. The precipitation of supersaturated solid solution of Al-4.5%Cu alloys had an additional linear expansion of ≈ 0.05 % at 643 K during thermal expansion measurement.

Al-Si-Mg-Cu 합금의 자동차 엔진 사용 온도에서 열처리 조건에 따른 열확산도 변화 (Change in Thermal Diffusivity of Al-Si-Mg-Cu Alloy According to Heat Treatment Conditions at Automotive Engine Operating Temperature)

  • 최세원
    • 한국재료학회지
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    • 제31권11호
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    • pp.642-648
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    • 2021
  • The precipitation effect of Al-6%Si-0.4%Mg-0.9%Cu-(Ti) alloy (in wt.%) after various heat treatments was studied using a laser flash device (LFA) and differential scanning calorimetry (DSC). Solid solution treatment was performed at 535 ℃ for 6 h, followed by water cooling, and samples were artificially aged in air at 180 ℃ and 220 ℃ for 5 h. The titanium-free alloy Al-6%Si-0.4%Mg-0.9%Cu showed higher thermal diffusivity than did the Al-6%Si-0.4%Mg-0.9%Cu-0.2%Ti alloy over the entire temperature range. In the temperature ranges below 200 ℃ and above 300 ℃, the value of thermal diffusivity decreased with increasing temperature. As the sample temperature increased between 200 ℃ and 400 ℃, phase precipitation occurred. From the results of DSC analysis, the temperature dependence of the change in thermal diffusivity in the temperature range between 200 ℃ and 400 ℃ was strongly influenced by the precipitation of θ'-Al2Cu, β'-Mg2Si, and Si phases. The most important factor in the temperature dependence of thermal diffusivity was Si precipitation.

Effect of Microwave Heat Treatment on Inhibition of Corn Seed Germination

  • Ambrose, Ashabahebwa;Lee, Wang-Hee;Cho, Byoung-Kwan
    • Journal of Biosystems Engineering
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    • 제40권3호
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    • pp.224-231
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    • 2015
  • Purpose: Corn is a major commercial crop targeted for genetic modification owing to its high consumer demand as a foodstuff for humans and livestock, as well as its other industrial applications. However, the safety of genetically modified (GM) crops is controversial. Indeed, several countries have banned the importation of GM seeds that can germinate. Therefore, development of effective, convenient, and nondestructive methods to inhibit seed germination is required. Methods: This study aimed to examine the efficacy of microwave heat treatment for inhibition of germination of corn kernels and for optimization of power and exposure time required for effective aging treatment. Artificial inhibition was induced in corn kernels using microwave heat treatment. Seven power levels were examined (400, 500, 600, 700, 800, 900, and 1000 W) at each of the four exposure times (0.5, 1.0, 1.5, and 2.0 min). Results: Corn kernels could be aged effectively after heating for 0.5~1.0 min at powers greater than 800 W, with increasing efficacy observed at higher powers. Further analysis showed that the most effective inhibition of germination was observed at 1000 W for 40 s. This setting did not cause any physical damage to the corn kernels. Conclusions: Optimal inhibition of corn kernel germination was achieved using higher power for shorter times, which may be useful for industrial corn seed treatment.

Isolation and Identification of Bacillus cereus from Fermented Red Pepper-Soybean Paste (Kochujang), and Its Heat Resistance Characteristics

  • Kim, Yong-Suk;Ahn, Yong-Sun;Jeon, Do-Youn;Shin, Dong-Hwa
    • Food Science and Biotechnology
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    • 제17권1호
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    • pp.123-129
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    • 2008
  • To isolate Bacillus cereus presenting at a level of 5 log CFU/g in kochujang, a primary dilution ($10^{-1}$) of kochujang was heated at $85^{\circ}C$ for 5 min. Two isolated strains Voges-Proskauer positive colony (KBC) and a negative colony (KBM) were identified as B. cereus and Bacillus mycoides, respectively, by biochemical test and 16S rDNA sequencing. $D_{100^{\circ}C}$-Values of KBC and KBM strains was 8.37 and 7.08 min, respectively. When spores of KBC strain were inoculated to kochujang at the level of 4-5 log spores/g, the number of spores was no significant difference (p<0.05) for each sample from 1 up to 60 day of aging. When kochujang was inoculated with 4 log spores/g and heated at $85^{\circ}C$ for 15 min, the number of spores was similar to that of unheated kochujang. Therefore, we estimated that B. cereus isolated from kochujang resistant on the heat treatment ($85^{\circ}C$, 15 min) and its heat resistance characteristics could be used to count the number in kochtjang.

열분석법에 의한 Al-2.1Li-2.9Cu합금의 석출현상(I) - 석출순서 - (The Precipitation Phenomena of Al-2.1Li-2.9Cu alloy by Differential Scanning Calorimetry(I) - Precipitation sequence -)

  • 박태원
    • 열처리공학회지
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    • 제9권4호
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    • pp.252-260
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    • 1996
  • A study was conducted to examine the precipitation phenomena of Al-2.1Li-2.9Cu alloy by differential scanning calorimetry and transmission electron microscopy. DSC curves were measured over the temperature range of $25{\sim}550^{\circ}C$ at a heating rate of $2{\sim}20^{\circ}C$/min.. Three heat evolution peaks and three heat absorption peaks were observed in the DSC curve for the as-quenched specimen. From DSC results and TEM analysis, it was proved that the precipitation sequence in the as-quenched specimen is supersaturated solid solution ${\rightarrow}$ GP zone ${\rightarrow}{\delta}^{\prime}{\rightarrow}T_1{\rightarrow}T_2$ and ${\theta}^{\prime}$ was detected in the peak aged specimen at $160^{\circ}C$. The major phase formed at peak hardeness in the aging at $160^{\circ}C$ was ${\delta}^{\prime}$ phase. The activation energies for the formation of ${\delta}^{\prime}$ and $T_1$ phases were 22.3kcal/mole and 24.3kcal/mole, respectively. These lower activation energies than those for diffusion of Cu and Li in Al are ascribed to the quenched-in excess vacancies.

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Sc 첨가된 Al-Zn-Mg-(Cu)계 알루미늄 합금 압출재의 시효 경화 거동과 기계적 성질 (Age Hardening and Mechanical Property of Extruded Al-Zn-Mg-(Cu) Al Alloys with Sc addition)

  • 심성용;임수근
    • 열처리공학회지
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    • 제20권5호
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    • pp.243-249
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    • 2007
  • The age hardening behavior and mechanical properties of an extruded Al-Zn-Mg-(Cu)-0.1 wt.%Sc alloy were investigated with the Sc addition and ageing temperature. The results showed that the $Al_3Sc$ compounds were formed by Sc addition and distributed preferentially along the extrusion direction. The age hardening of Al-Zn-Mg-Cu-0.1 wt.%Sc alloy which was treated by T6 process was more significant than that of Al-Zn-Mg-0.1 wt.%Sc alloy. The tensile property of Al-Zn-Mg-Cu+0.1 wt.%Sc alloy was also higher than that of Al-Zn-Mg-0.1 wt.%Sc alloy, which is 691 MPa and 584 MPa in strength and 9% and 11% in elongation, respectively.