• The Transactions of The Korean Institute of Electrical Engineers
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• v.59 no.5
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• pp.912-917
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• 2010

It was known that oil-filled transformer's life depended on insulating paper which was applied to transformers for insulating of transformer. Therefore when paper was aged, its electrical, mechanical and chemical characteristics were changed. Especially if operating temperature was high, paper was quickly damaged. As cellulose paper which was mainly used for solid insulation of transformers was degraded, the cellulose polymer chains broke down into shorter lengths and gases such as CO, $CO_2$, $CH_4$, $C_2H_4$ and so on were produced from paper. Also by-product known as furan compounds were producted from paper and it were dissolved within insulating oil. In this paper accelerating aging cell was aged during 60 hours at 100, 150, 180 and $200^{\circ}C$, respectively, so evaluating the chemical characteristics of cellulose paper by thermal. An it were performed analysis such as tensile strength(TS), dissolved gas analysis(DGA) and high performance liquid chromatography(HPLC). Also for analyzing of correlation between insulating degradation characteristics, it was performed linear regression method as statistical treatment.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.15 no.2
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• pp.119-126
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• 2002

The mica/epoxy composite used in generator(rated 22 kV and 500 MW) stator windings was aged at 180$\^{C}$ for up to 1000 hours in air and hydrogen. The degradation mechanism was investigated through the defect of evolution and microstructural analysis by performing SEM(Scanning Electron Microscope). As the thermal aging time increases, the number of voids per unit volume increases at the mica/epoxy interface of generator stator windings. The aged specimens in hydrogen showed retarded generation and growth of voids. Accelerated aging tests were conducted using the combination of thermal and electrical aging in air and hydrogen. The aging was carried out at a combined stress such as thermal aging at 110$\^{C}$, electrical aging at 5.5 kV/mm and frequencies 420 Hz in air, and electrical aging at 5.5 kV/mm and frequencies 420 Hz in hydrogen (pressure 4 kg/㎠). Thermal and electrical aging generates large voids at the mica/epoxy interface in air. Electrical aging in hydrogen also generates small voids, delaminations and cracks in mica tapes.

• Food Science of Animal Resources
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• v.39 no.3
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• pp.474-493
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• 2019

The aim of the study was to evaluate the effect of an early post-mortem low voltage electrical stimulation (ES) to localized part of carcasses [m. longissimus lumborum (LL) and m. biceps femoris (BF)] and determined the tenderness and flavor compounds of Hanwoo steers (n=16). Carcasses were stimulated within 30 min post-mortem for 60s using 60 volts and muscles aged 2 and 14 d. Degradation of Troponin-T were accelerated by ES and degraded little faster in BF muscle than LL. Level of free amino acid content of stimulated and aged muscles was significantly (p<0.05) greater than control for both muscles. Totally 63 volatile compounds were identified by using SPME-GC. The ES treatment significantly (p<0.05) affected the level of 20 volatile compounds of LL as well 15 volatiles in BF muscle along with total amounts of ketones, sulfur containing, pyrazines and furans. Low voltage ES could be applied to reduce the aging time and improve volatile flavor development by increasing important desirable volatile compounds such as 2-methylpyrazine, 2,5-dimethylpyrazines and 2-acetylthiazole etc. due to released free amino acids from protein degradation.

• Journal of the Korean Society for Nondestructive Testing
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• v.25 no.5
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• pp.377-383
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• 2005

Because explosive fluid is used at high temperature or under high pressure in petrochemistry and refined oil equipment, the interest about safety of equipments is intensive. Specially, the safety of high pressure reactor vessel is required among them. The material selected in this study is 2.25Cr-1Mo steel that is widely used for high pressure reactor vessel material of petrochemical plant. Eight kinds of artificially aged specimens were prepared by differing from aging periods under three different temperatures. The material was iso-thermally heat treated at higher temperatures than $391^{\circ}C$ that is the operating temperature of high pressure reactor vessel. Vickers hardness properties and electrical resistivity properties about artificially aged material as well as un-aged material were measured, and master curves were made out from the correlation with larson-Miller parameter. And electrical resistivity properties as well as Victors hardness properties measured at high pressure reactor vessel of the field were compared with master curves made out in a laboratory. Degradation evaluation possibility in the field of high pressure reactor vessel by using electrical resistivity method was examined. Electrical resistivity property measured in the field is similar with that of artificially aged material in similar aging level.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.25 no.12
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• pp.2116-2124
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• 2001

It's required mechanical properties of in-service facilities to maintain safety operation in power plants as well as chemical plants. In this studdy the four classes of the thermally aged 1Cr-lMo-0.25V specimens were prepared using an artificially accelerated aging method at 630$\^{C}$. Ultrasonic tests, tensile tests, K$\_$IC/ tests and hardness tests were performed in order to evaluate the degree of degradation of the material. The mechanical properties were decreased as degraded, but the attenuation coefficient and the harmonic generation level of a ultrasonic signal were increased. Expecially the nonlinear parameter derived from the harmonic generation level is sensitive and will be a good parameter to evaluate the material degradation.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2004.07b
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• pp.1183-1186
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• 2004

Degradation and insulation failure of traction motor depend on the continuous stress imposed on it. And knowing on insulation condition is important thing for safety operation of EMU(electric multiple unit). In this paper, PD(partial discharge) characteristics for degradation analysis of stator coil is studied. For PD data acquisition, two models are made; one is normal condition coil, the other is aged condition coil. And PD data for discrimination were acquired from PD detector. And these data making use of a computer-aided discharge analyser, statistical and other discharge parameters is calculated to discrimination between different discharge sources. And also these parameter is applied to classify PD sources by neural networks. Neural Networks has good recognition rate for degradation of stator coil.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.30 no.8 s.251
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• pp.965-975
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• 2006

High pressure turbine blades are one of the key components in fossil power plants operated at high temperature. The blade is usually made of 12Cr steel and its operating temperature is above $500^{\circ}C$. Long term service at this temperature causes material degradation accompanied by changes in microstructures and mechanical properties such as strength and toughness. Quantitative assessment of reduction of strength and toughness due to high temperature material degradation is required for residual life assessment of the blade components. Nondestructive technique is preferred. So far most of the research of this kind was conducted with low alloy steels such as carbon steel, 1.25Cr0.5Mo steel or 2.25Cr1Mo steel. High alloy steel was not investigated. In this study one of the high Cr steel, 12Cr steel, was selected for high temperature material degradation. Electrochemical polarization method was employed to measure degradation. Strength reduction of the 12Cr steel was represented by hardness and toughness reduction was represented by change of transition temperature, FATT. Empirical relationships between the electrochemical polarization parameter and significance of material degradation were established. These relationship can be used for assessing the strength and toughness on the aged high pressure blade components indirectly by using the electrochemical method.

• Journal of the Korean Society for Nondestructive Testing
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• v.22 no.3
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• pp.284-291
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• 2002

An attempt was made to evaluate the degree of aging degradation in thermally aged 2.25Cr-1Mo steel by electrical resistivity measurement. Artificial aging was performed to simulate the microstructural degradation in 2.25Cr-1Mo steel arising from long time exposure at $540^{\circ}C$. Microstructural parameter (amount of solid solution element), mechanical property (ductile-brittle transition temperature) and electrical resistivity were measured to investigate the mutual relationship among these parameters. Depletion of solid solution element(Mo and Cr) in matrix was detected after aging. The ductile-brittle transition temperature(DBTT) increased rapidly in the initial stage of aging and then saturated afterward. On the other hand, the electrical resistivity decreased rapidly in the beginning and then saturated in the later stage of aging.

• Journal of the Korean Society for Nondestructive Testing
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• v.21 no.5
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• pp.549-555
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• 2001

Ultrasonic is a powerful nondestructive technique for getting the information of flaws and material properties of in-services facilities. We prepared 4 different 1Cr-1Mo-0.25V specimens by Isothermal aging at $630^{\circ}C$. We evaluated material degradation using ultrasonic parameters, velocity, attenuation and harmonic generation. Attenuation and nonlinear parameter derived from harmonic generation efficiency increased as degradation. Especially the second harmonic of the fundamental wave in the 1,820h aging material was observed to exceed 20dB more than that in the un-aged material. But velocity remained virtually the same for all specimens. We concluded that nonlinear parameter and attenuation are sensitive to material degradation, but velocity was not. It'll be a good parameter for evaluating the material degradation.

• Journal of the Korean Society for Nondestructive Testing
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• v.22 no.3
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• pp.267-274
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• 2002

This research is described on the applicability of a electrochemical techniques for evaluating nondestructive material degradation with various polarization characteristics for Cr-Mo-V steel. The applied electrochemical technique is anodic polarization test which are widely used to evaluate the corrosion rate and/or sensitization at depleted zone of strengthening elements mainly caused by thermal experience for stainless steels. The evaluation of material degradation is performed by small punch test which has been well known as micromechanics test method using specimen size of $10{\times}10{\times}0.5mm$. The 1,000hrs aged material at $630^{\circ}C$ shows the highest material degradation$({\Delta}[DBTT]_{SP})$, but the 2,000hrs and 3,000hrs aged materials show the decrease of ${\Delta}[DBTT]_{SP}$ as aging time increases. It is observed that the difference of current density $({\Delta}I_{FP}\;and\;{\Delta}I_{SP})$.