• The Journal of Advanced Prosthodontics
• /
• 제6권2호
• /
• pp.88-95
• /
• 2014

PURPOSE. The purpose of this study is to evaluate if pre-treatment with desensitizers have a negative effect on microtensile bond strength before cementing a restoration using recently introduced self-adhesive resin cement to dentin. MATERIALS AND METHODS. Thirty-five human molars' occlusal surfaces were ground to expose dentin; and were randomly grouped as (n=5); 1) Gluma-(Glutaraldehyde/HEMA) 2) Aqua-Prep F-(Fluoride), 3) Bisblock-(Oxalate), 4) Cervitec Plus-(Clorhexidine), 5) Smart protect-(Triclosan), 6) Nd:YAG laser, 7) No treatment (control). After applying the selected agent, RelyX U200 self-adhesive resin cement was used to bond composite resin blocks to dentin. All groups were subjected to thermocycling for 1000 cycles between $5-55^{\circ}C$. Each bonded specimen was sectioned to microbars ($6mm{\times}1mm{\times}1mm$) (n=20). Specimens were submitted to microtensile bond strength test at a crosshead speed of 0.5 mm/min. Kolmogorov-Smirnov, Levene's test, Kruskal-Wallis One-way Analysis of Variance, and Conover's nonparametric statistical analysis were used (P<.05). RESULTS. Gluma, Smart Protect and Nd:YAG laser treatments showed comparable microtensile bond strengths compared with the control group (P>.05). The microtensile bond strengths of Aqua-Prep F, and Cervitec Plus were similar to each other but significantly lower than the control group (P<.05). Bisblock showed the lowest microtensile bond strength among all groups (P<.001). Most groups showed adhesive failure. CONCLUSION. Within the limitation of this study, it is not recommended to use Aqua-prep F, Cervitec Plus and Bisblock on dentin when used with a self-adhesive resin cement due to the decrease they cause in bond strength. Beside, pre-treatment of dentin with Gluma, Smart protect, and Nd:YAG laser do not have a negative effect.

• 산업경영시스템학회지
• /
• 제23권54호
• /
• pp.137-144
• /
• 2000

The chloroprene adhesive for ladies' shoe-making applied by the cementing method in KS G 3116 has been evaluated.. For the quality test of adhesive for pump whole cut vamp using chloroprene adhesive, general property and adhesion strength were measured and duration for environmental exposure was tested. Also, a list of experiments for field application was prepared. In case of adhesion-strength measurement,, the KS G 3116 method of peel strength at end of toe was found to be reasonable by measurement through a whole length, toe to heel seat on feather edge.

• Restorative Dentistry and Endodontics
• /
• 제29권5호
• /
• pp.423-429
• /
• 2004

The purpose of this study was to evaluate the effect of multiple application of all-in-one dentin adhesive system on microtensile bond strength using confocal laser scanning microscope and microtensile bond strength test. Flat occlusal dentin surfaces were prepared using low-speed diamond saw. In group I, Scotchbond Multipurpose (SM) was applied by manufacturer's recommendation. In group II, after Adper Prompt L-Pop was applied for 15s and light cured for 10s. the second coat was re-applied and light-cured. In group III, after light-curing the second layer. the third coat was re-applied and light-cured. Specimens bonded with a resin-composite were sectioned into resin-dentin stick for measuring the adhesive layer thickness by confocal laser scanning microscope and evaluating micro-tensile bond strength. The adhesive layers of three-step dentin adhesive system. 3 coats of Adper Prompt L-Pop had significantly thicker than SM. 2 coats of Adper Prompt L-Pop (p < 0.05). However. there was no significant differences in bond strengths between SM and 3 coats of Adper Prompt L-Pop (p > 0.05). And SM. 3 coats of Adper Prompt L-Pop had significantly higher than 2 coats of Adper Prompt L-Pop in bond strengths (p < 0.05).

• 한국해양공학회지
• /
• 제24권1호
• /
• pp.146-152
• /
• 2010

Recently, the applied frequency of composite materials was increased from the viewpoint of lightweight, high strength and low cost when a leisure boat and a fishing boatwere built. However, studies on the mechanical properties of composite material with ship are rare. Specially, a leisure boat and fishing boat with FRP had been built by hand lay-up method. However, the vacuum infusion method is rising recently for ship building. The manufactured these FRP plates were combined by using the adhesive. Therefore, in this study Cleavage peel strength, Shear strength and fatigue limit of adhesive bonds by tensileloading were estimated. From test results, the strengths of FRP specimens made by the vacuum infusion method are higher than that of the hand lay-up method.

• 대한기계학회:학술대회논문집
• /
• 대한기계학회 2008년도 추계학술대회A
• /
• pp.115-120
• /
• 2008

In this study, effects of surface roughness on adhesive strength of heat-resistant adhesive RTV88 were examined. Sandblast was used to generate rough surfaces on aluminum adherends, and then tensile-shear tests of Al/RTV88 single lap joints were performed. The shear strength was shown to be affected by the surface roughness. Effective area, peel failure area, and cohesive failure area were introduced to explain the effects of surface roughness on the adhesive strength. An empirical relation for the failure force was proposed based on these parameters and verified by the test results.

• 한국항공운항학회지
• /
• 제27권3호
• /
• pp.24-29
• /
• 2019

The paste-type adhesive can be stored for a certain period of time and can be cured at room temperature. So it is mainly used for crack patching repair of aircraft airframe structures. This study analysed the influence of environmental factors and evaluated the adherence strength characteristics according to the adherence delay time of the paste-type adhesive. The test specimens were made of aluminum alloy(AL 2024-T3) with reference to ASTM D1002 which is generally performed to measure the adherence strength of the adhesive used for metal bonding. As a result of analysing the influence of temperature and humidity, it was found that the optimal temperature range is $24.5{\pm}0.5^{\circ}C$ and the optimal humidity range is $71{\pm}1%$ for maintenance work of the aircraft using EA-9320 adhesive. In addition, the adherence strength did not decrease with the inherent application time of the EA-9320, but it was found that the adherence strength dropped rapidly when the applied time exceeded the inherent application time of it.

• Restorative Dentistry and Endodontics
• /
• 제40권4호
• /
• pp.299-305
• /
• 2015

Objectives: The purpose of this study was to investigate the effectiveness of multiple decontamination procedures for salivary contamination after curing of a universal adhesive on dentin bond strength according to its etch modes. Materials and Methods: Forty-two extracted bovine incisors were trimmed by exposing the labial dentin surfaces and embedded in cylindrical molds. A universal adhesive (All-Bond Universal, Bisco) was used. The teeth were randomly divided into groups according to etch mode and decontamination procedure. The adhesive was applied according to the manufacturer's instructions for a given etch mode. With the exception of the control groups, the cured adhesive was contaminated with saliva for 20 sec. In the self-etch group, the teeth were divided into three groups: control, decontamination with rinsing and drying, and decontamination with rinsing, drying, and adhesive. In the etch-and-rinse group, the teeth were divided into four groups: control, decontamination with rinsing and drying, decontamination with rinsing, drying, and adhesive, and decontamination with rinsing, drying, re-etching, and reapplication of adhesive. A composite resin (Filtek Z350XT, 3M ESPE) was used for filling and was cured on the treated surfaces. Shear bond strength was measured, and failure modes were evaluated. The data were subjected to one-way analysis of variation and Tukey's HSD test. Results: The etch-and-rinse subgroup that was decontaminated by rinse, drying, re-etching, and reapplication of adhesive showed a significantly higher bond strength. Conclusions: When salivary contamination occurs after curing of the universal adhesive, additional etching improves the bond strength to dentin.

• 구강회복응용과학지
• /
• 제25권4호
• /
• pp.437-444
• /
• 2009

본 연구에서는 여러 automixing 레진시멘트의 물성과 상아질에 대한 전단결합강도를 평가, 비교하고자 하였다. Self-adhesive automixing 레진시멘트인 Rely-X Unicem(3M ESPE, St. Paul, USA), Embrace resin cement(Pulpdent, Oakland, USA)와 chemical polymerizing automixing 레진시멘트인 Resiment Ready-Mix(J.L.Blosser Inc., Liberty Missouri, USA)를 사용하였다. 물성을 평가하기 위하여 레진시멘트를 테프론 주형에 주입한 후 자가중합을 시키고 24시간 동안 빛이 차단된 상태로 100% 상대습도에 보관 후 만능 시험기를 이용하여 압축강도, 간접인장강도, 굴곡강도를 측정하였다. 상아질에 대한 전단결합강도를 평가하기 위하여 발거한 하악 제3대구치의 협측 상아질을 노출 시킨 후 일정한 크기로 레진시멘트를 부착시킨 뒤 만능 시험기를 이용하여 전단결합강도를 측정하였다. SPSS Ver 12.0(SPSS Inc., Chicago, IL, USA)을 사용하여 95% 유의수준에서 One way ANOVA test로 분석하였으며 Scheffe test로 사후검정 하였다. 연구결과, chemical polymerizing automixing 레진시멘트가 self-adhesive automixing 레진시멘트에 비해 상대적으로 높은 물리적 성질과 상아질에 대한 전단결합강도를 보였다.

• 한국건축시공학회:학술대회논문집
• /
• 한국건축시공학회 2005년도 춘계 학술기술논문발표대회 논문집
• /
• pp.173-178
• /
• 2005

The tile construction methods for existing have been used materials within limit which adhesion by wet method in masonry wall and concrete structure. These existing adhesive tech can caused many problems in construction of large and reform tile, after that it can be happened loose scale, peel off, falling off tile by heat and vibration or impact. In according to, this study is to test tile for bond stability, adhesive property by impact, vibration. low property by heat and then, we have the results as below; (1) The tile adhesive stability can be effected as adhesive area between bond agent and tile, adhesive area can more wide and press enough to ensure property. (2) Existing adhesive strength and standard relative tile construction is limited to adjust performance tile on the concrete and masonry wall. In summary, It is necessary to establish standard of performance and test method to ensure tile adhesive salability in dry wall.

• 한국도로학회논문집
• /
• 제16권4호
• /
• pp.21-33
• /
• 2014

PURPOSES: The purpose of this study was to break away from the workforce method using cold-mix asphalt mixtures and has a constant quality and has develop repair materials of pre-production asphalt-precast types. METHODS: The selection of the repair material was determined as the results obtained through physical properties of materials and the field applicability. In case of repair materials, values obtained through Marshall stability test & the dynamic stability test & retained stability test as well as the site conditions was considered. In case of adhesive, test results were obtained through examination of the bond strength(tensile, shear) and the field applicability of the adhesive was examined through combined specimens to simulate field applications. RESULTS : According to the results of laboratory tests, in the case of repair materials, Marshall stability and dynamic stability, retained stability of cold-mix reaction type asphalt mixture is the highest. In the case of adhesive, two-component epoxy-urea has a very high bonding strength(tensile, shear) was most excellent. According to the results of field tests, when epoxy-urea was excellent workability. Also, the repair body through actual mock-up test did not occur large deformation and fracture after 12 months. CONCLUSIONS : A suitable repair material is cold-mix reaction type mixture of asphalt-precast, a suitable adhesive is a two-component epoxy-urea.