Physical Properties of Different Automixing Resin Cements and the Shear Bond Strength on Dentin

수종 Automixing 레진시멘트의 물성과 상아질에 대한 전단결합강도

  • Song, Chang-Kyu (Department of Conservative Dentistry, College of Dentistry, Kangnung-Wonju National University) ;
  • Park, Se-Hee (Department of Conservative Dentistry, College of Dentistry, Kangnung-Wonju National University) ;
  • Kim, Jin-Woo (Department of Conservative Dentistry, College of Dentistry, Kangnung-Wonju National University) ;
  • Cho, Kyung-Mo (Department of Conservative Dentistry, College of Dentistry, Kangnung-Wonju National University)
  • 송창규 (강릉원주대학교 치과대학 치과보존학교실) ;
  • 박세희 (강릉원주대학교 치과대학 치과보존학교실) ;
  • 김진우 (강릉원주대학교 치과대학 치과보존학교실) ;
  • 조경모 (강릉원주대학교 치과대학 치과보존학교실)
  • Received : 2009.08.20
  • Accepted : 2009.12.25
  • Published : 2009.12.31

Abstract

The purpose of this study was to evaluate the physical properties of different automixing resin cements and the shear bond strength on dentin. For this study, two self-adhesive automixing resin cement(Rely-X Unicem(3M ESPE, St. Paul, USA), Embrace resin cement(Pulpdent, Oakland, USA)) and one chemical polymerizing resin cement(Resiment Ready-Mix(J.L.Blosser Inc., Liberty Missouri, USA)) were used. To evaluate the physical properties, compressive strength, diametral tensile strength and flexural strength were measured. The specimens were fabricated using Teflon mould according to manufacturers' instructions and stored for 24 hours in an atmosphere of 100% humidity. To evaluate the shear bond strength on dentin, each cements were adhered to buccal dentinal surface of extracted human lower molars in 2mm diameter. Physical properties and shear bond strengths were measured using universal testing machine(Z010, Zwick GmbH, Ulm, Germany) at a crosshead speed of 0.5mm/min. The physical properties and shear bond strength of different automixing resin cements were statistically analyzed and compared between groups using One-way ANOVA test and Schffe post-hoc test at the 95% level of confidence. The result shows that chemical polymerizing automixing resin cement represents the relatively higher physical properties and shear bond strength than self-adhesive automixing resin cements.

본 연구에서는 여러 automixing 레진시멘트의 물성과 상아질에 대한 전단결합강도를 평가, 비교하고자 하였다. Self-adhesive automixing 레진시멘트인 Rely-X Unicem(3M ESPE, St. Paul, USA), Embrace resin cement(Pulpdent, Oakland, USA)와 chemical polymerizing automixing 레진시멘트인 Resiment Ready-Mix(J.L.Blosser Inc., Liberty Missouri, USA)를 사용하였다. 물성을 평가하기 위하여 레진시멘트를 테프론 주형에 주입한 후 자가중합을 시키고 24시간 동안 빛이 차단된 상태로 100% 상대습도에 보관 후 만능 시험기를 이용하여 압축강도, 간접인장강도, 굴곡강도를 측정하였다. 상아질에 대한 전단결합강도를 평가하기 위하여 발거한 하악 제3대구치의 협측 상아질을 노출 시킨 후 일정한 크기로 레진시멘트를 부착시킨 뒤 만능 시험기를 이용하여 전단결합강도를 측정하였다. SPSS Ver 12.0(SPSS Inc., Chicago, IL, USA)을 사용하여 95% 유의수준에서 One way ANOVA test로 분석하였으며 Scheffe test로 사후검정 하였다. 연구결과, chemical polymerizing automixing 레진시멘트가 self-adhesive automixing 레진시멘트에 비해 상대적으로 높은 물리적 성질과 상아질에 대한 전단결합강도를 보였다.

Keywords

References

  1. Theodore M, Harald O, Edward J. Dental Materials. St. Louis, USA, Mosby. Sturdevant's art & science of operative dentistry. 4th ed., 2001: 217-219
  2. Zhen Chun Li, Shane N. Mechanical properties of dental luting cements. J Prosthot Dent 1999;81: 597-609 https://doi.org/10.1016/S0022-3913(99)70216-7
  3. De Munck J, Vargas M, Van Landuyt K, Hikita K, Lambrechts P, Van Meerbeek B. Bonding of an auto-adhesive luting material to enamel and dentin. Dent Mater 2004;20: 963-71 https://doi.org/10.1016/j.dental.2004.03.002
  4. Mak YF, Lai SC, Cheung GS, Chan AW, Tay FR, Pashley DH. Micro-tensile bond testing of resin cements to dentin and an indirect resin composite. Dent Mater 2002;18: 609-621 https://doi.org/10.1016/S0109-5641(02)00005-2
  5. Fusayama T, Nakamura M, Kurosaki N, Iwaku M. Non-pressure adhesion of a new adhesive restorative resin. J Dent Res 1979;58(4): 1364-1370 https://doi.org/10.1177/00220345790580041101
  6. Nicholls JI. The effect of convergence angle variation on the computed stresses in the luting agent. J Prosthet Dent 1974;31: 651-7 https://doi.org/10.1016/0022-3913(74)90120-6
  7. Nicholls JI. Stress analysis of symmetric restorations. J Prosthet Dent 1974;31: 179-84 https://doi.org/10.1016/0022-3913(74)90053-5
  8. Yettram AL, Wright KW, Pickard HM. Finite element stress analysis of the crowns of normal and restored teeth. J Dent Res 1976;55: 1004-11 https://doi.org/10.1177/00220345760550060201
  9. Craig RG, Farah JW. Stress analysis and design of single restorations and fixed bridges. Oral Sci Rev 1977;10: 45-74
  10. Farah JW, Craig RG. Stress analysis of three marginal configurations of full posterior crowns by three- dimensional photoelasticity. J Dent Res 1974;53: 1219-25 https://doi.org/10.1177/00220345740530052501
  11. Chai JY, Steege JW. Effects of labial margin design on stress distribution of a porcelain-fused-to-metal crown. J Prosthodont 1992;1: 18-23 https://doi.org/10.1111/j.1532-849X.1992.tb00421.x
  12. Goldstein GR, Wesson A, Schweitzer K, Cutler B. Flexion characteristics of four-unit fixed partial denture frameworks using holographic interferometry. J Prosthet Dent 1992;67: 609-13 https://doi.org/10.1016/0022-3913(92)90156-5
  13. Kamposiora P, Papavasilious G, Bayne SC, Felton DA. Finite element analysis estimates of cement microfracture under complete veneer crowns. J Prosthet Dent 1994;71: 435-41 https://doi.org/10.1016/0022-3913(94)90179-1
  14. O'Brien WJ. Dental Cements. Dental materials: properties and selection. 2nd ed. Chicago, USA, Quintessence, 1997: 167-171
  15. Harry F. Material Science. Tooth-colored restoratives. 9th ed. London, England, BC Decker Inc 2002: 93-97
  16. Derkson GD, Richardson AS, Weldman R. Clinical evaluation of posterior composite restorations : Two year results. J Dent Res 1983;49(4): 277-9
  17. Chae MS, Chu YH, Bae TS. A study on the compressive strength of experimental light-actived composite resins. J Kor Res Soc Dent Mat 1995;22(2): 113-121
  18. Kawaguchi M, Fukushima T, Horibe T, Watanabe T. Mechanical properties and curing depth of urethane tetramethacrylate-based composite resins. Shika Zairyo Kikai 1990;9(5): 762-6
  19. Soeno K, Suzuki S, Taira Y et al.. Influence of mechanical properties of two resin cements on durability of bond strength to dentin after cyclic loading. Dent Mater J 2005;24(3): 351-5 https://doi.org/10.4012/dmj.24.351
  20. Salz U, Zimmermann J, Salzer T. Self-curing, self-etching adhesive cement systems. J Adhes Dent 2005;7(1): 7-17
  21. Abo-Hamar SE, Hiller KA, Jung H et al.. Bond strength of a new universal self-adhesive resin luting cement to dentin and enamel. Clin Oral Investig 2005;9(3): 161-7 https://doi.org/10.1007/s00784-005-0308-5
  22. Bateman GJ, Lloyd CH, Chadwick RG, Saunders WP. Retention of quartz-fibre endodontic posts with a self-adhesive dual cure resin cement. Eur J Prosthodont Restor Dent 2005;13(1): 33-7
  23. Mallmann A, Jacques LB, Valandro LF, Mathias P, Muench A. Microtensile bond strength of light- and self-cured adhesive systems to intraradicular dentin using a translucent fiber post. Oper Dent 2005;30(4): 500-6
  24. Seltzer S. The penetration of micro-organism between the tooth and direct resin fillings. J Am Dent Assoc 1955;51: 560-566