• 한국산학기술학회논문지
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• 제13권10호
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• pp.4365-4370
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• 2012

MAO 법을 이용하여 전류밀도 4A/$cm^2$조건에서 3종류의 전해액과 코팅시간에 따라 AZ31 마그네슘 합금을 산화피막 처리하였다. 코팅시간이 길어짐에 따라 코팅층의 표면형상은 기공이 더욱 커지고, 표면에 균열이 발생하기도 하였다. 또한 코팅시간이 길어짐에 따라 코팅층의 두께와 경도(HV)값은 증가하였다. AZ31합금의 코팅층 상들은 MgO, $Mg_2SiO_4$ 그리고 $MgAl_2O_4$ 산화물로 이루어졌다. 산화코팅된 AZ31합금을 5% NaCl 용액에서 168시간동안 염수분무실험결과 우수한 내식성을 나타냈다.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2007년도 춘계학술대회 논문집
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• pp.114-117
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• 2007

In the present study, the effects of initial texture on the twinning formation of AZ31 Mg rolled sheet was investigated. Uniaxial compression tests were performed on samples cut along the normal direction and rolling direction of rolled AZ31 Mg alloy sheet at various temperatures (RT, 200, 250, 300, 350, $400^{\circ}C$) with the 0.01/s strain rate. Pole figure of rolling planes showed that basal planes of most gain were located parallel to the rolling direction. After compression test, microstructures and stress-strain curves results indicated that active deformation twining occurred only at the specimen cut along the rolling direction. The slip-twin transition with the increase of temperature was also investigated.

• 소성∙가공
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• 제16권6호
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• pp.467-472
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• 2007

In this study, the effects of initial texture on the twinning formation of AZ31 Mg rolled sheet was investigated. Uniaxial compression tests were carried out on samples cut along the normal direction(ND) and roiling direction(RD), respectively, of rolled AZ31 Mg alloy sheet at various temperatures (RT, 200, 250, 300, 350, $400^{\circ}C$) with the fixed strain rate($10^{-2}/s$). The results showed that deformation twining occurred actively only in the RD specimens, which promoted homogeneous deformation as compared to the ND specimens. The effect of temperature on the formation of deformation twins was also investigated, and the slip/twin transition temperature was found to be approximately $250^{\circ}C$.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2007년도 추계학술대회 논문집
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• pp.60-63
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• 2007

The effect of process parameters on springback of AZ31B magnesium alloy sheet was investigated by performing 2D draw bending test at the elevated temperatures. And also the springback characteristics were studied different blank holding forces between 30 to 250 kgf. Springback was considerably reduced at higher temperatures than $200^{\circ}C$. The blank holding force in the range used, however, had little influence on springback in isothermal tests. For a given temperature, springback decreased with increasing blank holding force in non-isothermal tests.

• 소성∙가공
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• 제15권3호
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• pp.232-240
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• 2006

Magnesium alloys are expected to be widely used fur the parts of structural and electronic appliances due to their lightweight and EMI shielding characteristics. While the die casting has been mainly used to manufacture the parts from the magnesium alloys, the press forming is considered as an alternative to the die casting for saving the manufacturing cost and improving the structural strength of the magnesium alloy parts. However, the magnesium alloy has low formability at room temperature and therefore, in many cases, forming at elevated temperatures is necessary to obtain the required material flow without failure. In the present study, square cup deep drawing tests using the magnesium alloy AZ31 sheet were experimentally conducted at various elevated temperatures as well as room temperature, and the corresponding finite-element simulations, which calculated the damage evolution based on the Oyane's criterion, were conducted using the stress-strain relations from the tensile tests at various temperatures. The formability predictability by the finite-element analysis was investigated by comparing the predicted damage distributions over the deformed AZ31 sheet at elevated temperatures with the corresponding experimental deformations with failures.

• 한국표면공학회지
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• 제50권2호
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• pp.72-84
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• 2017

In this work, electrophoretic paint (E-paint) was deposited on AZ31 Mg alloy after four different surface pretreatments: knife abrading, SiC paper abrading, deionized (DI) water immersion and NaOH immersion. The deposition process of E-paint was studied by analyses of voltage-time and current-time curves, amount of deposited paint, current efficiency and surface oxide film resistance and the adhesion of E-paint was examined by tape test before and after immersion in DI water for 500 h at $40$^{\circ}C$. It was found that the induction time for the deposition, the amount of deposited paint and the current efficiency are inversely proportional to the resistances of surface films prepared by different surface pretreatment methods. The electrophoretic painting showed longer inductance time, larger amount of deposited paint and higher current efficiency on the highly conducting surfaces, such as knife-abraded and SiC-abraded surfaces than on the less conducting surfaces, such as DI water-immersed and NaOH-immersed samples. Excellent adhesion was observed on the E-paintings deposited onto knife-abraded and SiC-abraded AZ31 Mg alloy samplesSiC-abraded AZ31 Mg alloy samples.

• 소성∙가공
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• 제17권7호
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• pp.466-472
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• 2008

In this paper, tension tests and formability tests are performed to construct a database related to mechanical properties and the formability of the AZ31B Mg alloy sheet. A forming test with a hemi-spherical punch is conducted at varying temperatures to establish a forming limit diagram. In order to verify the applicability of the analysis using the conventional flow hardening model, a finite element analysis is performed on the hemi-spherical punch forming process and the results are compared with experimental ones. The study investigates problems involving a computational analysis that does not consider flow softening of the magnesium alloy at elevated temperatures.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2006년도 춘계학술대회 논문집
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• pp.67-69
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• 2006

Since magnesium alloy has a limited formability at room temperature, forming should be carried out at the elevated temperature. If the initial grain size is small, superplasticity could be expected over $400^{\circ}C$. Using superplastic behavior, blow forming can be used to overcome the low formability of Mg alloys. In the present study, the optimization of blow forming of AZ31 alloy at the elevated temperature was investigated. Finite element simulation was carried out and verified with the blow forming experiments.

• 소성∙가공
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• 제19권7호
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• pp.429-434
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• 2010

The material used is a commercial magnesium based alloy AZ31(Mg-3Al-1Zn) sheet with a thickness of 0.8 mm. Friction tests at various temperatures(R.T. to $200^{\circ}C$) and at various holding forces in the 4 type molds were carried out to investigate the coefficient of friction. A warm drawing process with a local heating and cooling technique was developed in the Mg alloy sheet forming to improve formability because it is very difficult for Mg alloy to deform at room temperature by the conventional method. So, the coefficient of friction at various mold surface treatment conditions in this study was needed to develop the Mg alloy sheet forming technology.

• 한국표면공학회지
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• 제49권5호
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• pp.395-400
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• 2016

This article reports improved corrosion resistance and adhesion of electro-paint (E-paint) with fluoride conversion coating (FCC) on AZ31 Mg alloy for the first time. These improvements were observed in comparison to chemically polished samples with no chemical conversion coating and samples with cerium conversion coatings (CeCC). FCCs were prepared in a hydrofluoric acid (HF) solution for four different times; 10, 30, 60, and 120 s. The colour of the samples changed from light gold to brown with increasing immersion time, indicating the formation of thicker FCC coatings with increasing immersion time. The adhesion of the E-paint on FCC-coated AZ31 Mg alloy was tested after 500 h of immersion in deionized (DI) water. Salt spray test (SST) results revealed delamination of E-paint on the chemically polished sample, severe blistering on the samples with CeCC, but no delamination and no blistering on the samples with FCC.