• Transactions of Materials Processing
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• v.22 no.8
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• pp.486-491
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• 2013

A numerical investigation of the butting process for an AZ31B magnesium alloy tube at elevated temperatures was conducted to develop a double-butted magnesium alloy tube. As a result of the current study, it was found that the amount of doming of the tube end, prior ironing-extrusion to obtain high wall thickness reduction are important factors for the butting process of magnesium alloy tubes. There is also a limitation of the thickness profile of butted tube due to buckling of tube wall during the stripping stage.

• Journal of Power System Engineering
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• v.22 no.1
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• pp.87-93
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• 2018

Specimens were machined out from hot-rolled AZ31 magnesium alloy, and deformed at 623K with rolling reduction of 30%. After hot rolling, specimens were annealed at various range of temperature and time. In this study, static recrystallization was occurred during heat treatment, however, variation of main component and intensity of texture was not revealed. The results of microstructure observation, damping capacity test and dislocation mechanism indicated that increasing of damping capacity was caused by grain growth. It means that grain size is effective factor to damping capacity.

• Journal of the Korean Society of Safety
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• v.24 no.6
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• pp.20-26
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• 2009

The creep deformation behavior of AZ31 magnesium alloy was examined in the temperature range from 573 to 673K (0.62 to 0.73 Tm) under various constant stresses covering low strain rate range from $4{\times}10^{-9}\;s^{-1}$ to $2{\times}10^{-2}\;s^{-1}$. At low stress level, the stress exponent for the steady-state creep rate was ~3 and the present results were in good agreement with the prediction of Takeuchi and Argon model. At high stress level, the stress exponent was ~5 and the present results were in good agreement with the prediction of Weertman model. The transition of deformation mechanism from solute drag creep to dislocation climb creep could be explained in terms of solute-atmospherebreakaway concept.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2009.10a
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• pp.105-106
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• 2009

AZ31 (3% Al, 1% Zn) Mg 판재의 내식성 향상을 위해 Ti/Zr/Polymer 복합계의 Cr-free 화성처리 방법을 이용하였다. 염수분무시험을 통해 최고 72시간 ($5{\sim}10%$ 발청) 내식성이 나타남을 확인하였다. 화성피막의 내식성은 그 피막이 가진 성분, 균일도, 치밀도, 형상 및 두께에 의해 좌우되는 만큼 TEM, SEM을 통해 화성피막 구조가 내식성과 어떠한 관련이 있는지 조사하였다. 또한, 화성처리 전 단계 공정인 탈지와 산세 및 중화 공정의 변수 조절을 통해 전처리 공정이 최종 화성피막의 물성에 어떠한 영향을 미치는지 조사하였다. 탈지조건을 $35{\sim}40^{\circ}C$, 5분에서 $50{\sim}80^{\circ}C$, $10{\sim}20$분으로 변경 시 좀 더 균일한 외관을 얻을 수 있었고, 적절한 중화제 선택을 통해 화성피막을 균일하게 형성시킬 수 있었다. 투과전자현미경 결과로 미루어 화성피막의 두께보다 균일도와 치밀도가 내식성에 결정적인 영향을 미치는 것을 확인할 수 있었다.

• Korean Journal of Metals and Materials
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• v.48 no.4
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• pp.305-314
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• 2010

The development of textures and microstructures during plastic deformation in a hot-extruded AZ 31 Mg alloy was investigated using a compression test with such parameters as deformation temperature, strain rate. It was observed from true stress-strain curves that twinning involves changes of the flow stresses. In the early stages of deformation at temperatures lower than $200^{\circ}C$, the occurrence of twins resulted in a decrease of the work-hardening rate, which increased drastically at a true strain of -0.05. The evolution of the deformation textures were assessed with the aid of EBSD analyses in terms of the competition between twinning and slip activity.

• Transactions of Materials Processing
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• v.30 no.1
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• pp.43-48
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• 2021

The success of warm forming of Mg alloy sheet is greatly influenced by friction at elevated temperature, depending on the surface treatment of the tool. The tool coating affected the frictional characteristics of AZ31B Mg alloy sheet at elevated and room temperatures. The frictional behavior of the Mg alloy sheet at room temperature was not significantly affected by surface treatment conditions of the tool, but was significantly affected at elevated temperature. When the contact pressure is high, a few surface-treated tools exhibit a higher coefficient of friction than those without surface treatment. It is important to select the surface treatment conditions of the tool in order to ensure appropriate friction during warm forming of Mg alloy sheet.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.29 no.4
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• pp.218-224
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• 2016

The surface of Mg alloy, AZ31 and AZ91, were treated by PEO (plasma electrolytic oxidation) in Na-P system electrolyte, with different applied voltage and time. Thickness, roughness and X-ray crystallographic analysis revealed several results. The more applied time and voltage of PEO treated, the thicker oxidized surface coating layer were covered. And surface roughness increased with the thickness of oxidized layer. It was thought that when oxide layer grew, resistivity and breakdown voltage increased with the thickness of layer, and then, the energy of micro plasma need to be higher then before. So, it made craters and pores of surface become greater, which were responsible for the coarse surface.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.29 no.4
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• pp.225-230
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• 2016

Effect of electrolyte composition and concentration on PEO coating layer were investigated. Mg alloy, Surface of AZ31 and AZ91 were oxidized using PEO with different electrolyte system, Na-P and Na-Si. and applied voltage and concentration. We measured thickness, roughness, X-ray crystallographic analysis and breakdown voltage of the oxidized layer. When increasing concentration of electrolyte, the thickness of oxide layer also increased too. And roughness also increased as concentration of electrolyte increasing. Breakdown voltage of coated layer showed same behavior, the voltage goes high as increasing thickness of coating layer, as increasing concentration of electrolyte, and increasing applied voltage of PEO. $Mg_2SiO_4$ phase were observed as well as MgO.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.10a
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• pp.62-65
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• 2008

Extrusion characteristics of Mg alloys were studied experimentally. The Al-Zn-Mg alloys, AZ31, AZ6l, AZ80, and AZ91 were extruded with hot hydrostatic extrusion process. The hydrostatic process was efficient to reduce surface friction and extend steady state region in extrusion which made it more convenient to examine deformation behavior of the alloys avoiding the disturbance caused by temporary contact state between billet and die, and billet and container. High pressure was cooperative to expand forming limit of the alloys which were applied on the billet during the extrusion process. Extrusion limits were traced in temperature and extrusion speed domain with changing composition of the alloying elements. Effects of process parameters on extrusion load and microstructure evolution were investigated also.

• Journal of Korean Ophthalmic Optics Society
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• v.15 no.4
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• pp.313-317
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• 2010

Purpose: The purpose of this study was to investigate the surface characteristics of plasma electrolytic oxidation (PEO) surface treatment on AZ31 magnesium alloy eyeglass frames. Methods: The plasma electrolytic oxidation (PEO) surface was created by varying the DC voltage. The oxidation layer of coating was measured using phase analysis by X-ray diffraction. The microstructural morphology was observed using a scanning electron microscopy. Coating layer and the concentration of elements were investigated using the energy dispersive X-ray spectra. Results: The MgO XRD peak was increased as the voltage increased, and the density of the surface oxide film was also increased. The changes in the composition of the EDS also showed a good agreement. Conclusions: The compound oxide crystallization of PEO oxide film layer was done by increasing formation of MgO as the voltage increased. The treatment at 65V and 60 sec showed the best results at surface state, contact angles and salt spray test.