• 대한기계학회논문집A
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• 제27권8호
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• pp.1398-1408
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• 2003

Tensile and LCF(low cycle fatigue) tests were carried out in air at wide temperature range 20$^{\circ}C$-750$^{\circ}C$ and strain rates of 1${\times}$10$\^$-4//s-1${\times}$10$\^$-2/ to ascertain the influence of strain rate on tensile and LCF properties of prior cold worked 316L stainless steel, especially focused on the DSA(dynamic strain aging) regime. Dynamic strain aging induced the change of tensile properties such as strength and ductility in the temperature region 250$^{\circ}C$-600$^{\circ}C$ and this temperature region well coincided with the negative strain rate sensitivity regime. Cyclic stress response at all test conditions was characterized by the initial hardening during a few cycles, followed by gradual softening until final failure. Temperature and strain rate dependence on cyclic softening behavior appears to result from the change of the cyclic plastic deformation mechanism and DSA effect. The DSA regimes between tensile and LCF loading conditions in terms of the negative strain rate sensitivity were well consistent with each other. The drastic reduction in fatigue resistance at elevated temperature was observed, and it was attributed to the effects of oxidation, creep and dynamic strain aging or interactions among them. Especially, in the DSA regime, dynamic strain aging accelerated the reduction of fatigue resistance by enhancing crack initiation and propagation.

• 한국해양공학회지
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• 제24권1호
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• pp.161-165
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• 2010

In the present study, process optimization for thermal-sprayed STS316 coating has been performed using $L_9(3^4)$ orthogonal array and analysis of variance (ANOVA). STS316 coatings were fabricated by flame spray process on steel substrate, and the hardness test and microstructure observation of the coatings were studied. The results of hardness test were analyzed by ANOVA. The ANOVA results showed that the spray distance had the greatest effect on hardness of the coating, on the other hands, the effects of oxygen gas flow and spray distance were ignorable. From these results, the optimal combination of the flame spray parameters could be derived, and confirmation experiment was carried out to verify these derived results. The calculated hardness of the coatings by ANOVA was found to approximately close to that of confirmation experimental result. Thus, it was considered that design of experiments using orthogonal array and ANOVA was effective for process optimization of thermal-sprayed STS316 coating.

• 대한기계학회논문집A
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• 제25권2호
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• pp.296-303
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• 2001

Kachanov-Rabotnov(K-R) creep damage theory was reviewed, and applied to design a creep curve for type 316LN stainless steel. Seven coefficients used in the theory, i.e., A, B, k, m, λ, r, and q were determined, and their physical meanings were analyzed clearly. In order to quantify a damage parameter ($\omega$), cavity amount was measured in the crept specimen taken from interrupted creep test with time variation, and then the amount was reflected into K-R damage equations. Coefficient λ, which is regarded as a creep tolerance feature of a material, increased with creep strain. Mater curve with λ=2.8 was well coincided with an experimental one to the full lifetime. The relationship between damage parameter and life fraction was matched with the theory at exponent ${\gamma}$=24 value. It is concluded that K-R damage equation was reliable as the modelling equation for type 316LN stainless steel. Coefficient data obtained from type 316LN stainless steel can be utilized for life prediction of operating material.

• 한국자동차공학회논문집
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• 제10권2호
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• pp.110-116
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• 2002

At elevated temperature, very complex precipitations occur in STS316. To investigate the effect of the precipitation on mechanical properties in SIS316, tensile tests and fatigue crack growth tests were carried out at $650^{\circ}C$ using artificially degraded materials. The material degradation was simulated by aging for up to 20000 hrs. at $750^{\circ}C$, which is equal to 179000hrs (about 20yrs) of service life at $650^{\circ}C$, after conducting solution treatment for 20 min. at $11300^{\circ}C$. The result of the hardness test and the tensile test showed that both properties are closely related to the mean free distance of carbides. Also, from the results of fracture tests at $650^{\circ}C$, ${\triangle}K_{th}$, after values were found to decrease as aging time and microstructure, as the volume fraction of $\sigma$ phase increased.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2004년도 추계학술대회
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• pp.1058-1062
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• 2004

High-temperature cylindrical stainless steel/sodium heat pipe was manufactured and tested under long-term operation. The container material was stainless steel 316L and the working fluid was sodium. The heat pipe was 25.4 mm in diameter and 1000 mm in length with a two-layer screen mesh wick. The evaporator part was 600 mm and the condenser part was 300 mm in length. Total measurement points on heat pipe were 15 points and 12 points were located in condenser part. The heat pipe was heated for 142 days(3400 hours) at $800^{\circ}C$. In the test period, the maximum temperature difference was increased from $18^{\circ}C$ o $28^{\circ}C$ and the maximum thermal resistance was as low as $0.015^{\circ}CW$.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2005년도 춘계학술대회 논문집
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• pp.1406-1411
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• 2005

The creep rupture data for type 316LN stainless steels were collected through literature survey or experimental data produced in KAERI. Using these data, polynomial equations for predicting creep life were obtained by Larson-Miller (L-M), Orr-Sherby-Dorn (O-S-D) and Manson-Haferd (M-H) etc. time-temperature parametric (TTP) methods. Standard error of estimate (SEE) values for the each parameter was obtained with different temperatures through the statistical process of the creep data. The results of L-M, O-S-D and M-H methods showed good creep-life prediction, but M-H method showed better agreement than L-M and O-S-D methods. Especially, it was found that SEE values of M-H method at $700^{\circ}C$ were lower than that of L-M and O-S-D methods.

• 한국재료학회지
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• 제25권6호
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• pp.293-299
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• 2015

In this study, nitrogen ions were implanted into STS 316L austenitic stainless steel by plasma immersion ion implantation (PIII) to improve the corrosion resistance. The implantation of nitrogen ions was performed with bias voltages of -5, -10, -15, and -20 kV. The implantation time was 240 min and the implantation temperature was kept at room temperature. With nitrogen implantation, the corrosion resistance of 316 L improved in comparison with that of the bare steel. The effects of nitrogen ion implantation on the electrochemical corrosion behavior of the specimen were investigated by the potentiodynamic polarization test, which was conducted in a 0.5 M $H_2SO_4$ solution at $70^{\circ}C$. The phase evolution and texture caused by the nitrogen ion implantation were analyzed by an X-ray diffractometer. It was demonstrated that the samples implanted at lower bias voltages, i.e., 5 kV and 10 kV, showed an expanded austenite phase, ${\gamma}_N$, and strong (111) texture morphology. Those samples exhibited a better corrosion resistance.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2005년도 추계학술대회 논문집
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• pp.818-823
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• 2005

Creep damage is one of the mosl important characteristics for the stability of high temperature structures such as huge energy converting facilities. Creep failure of Type 316LN stainless steel is highly correlated to generation and growth of the voids. In this paper, in order to investigate the correlation of creep rupture time and ultrasonic parameters (group velocity, angular velocity), creep-damaged Type 316LN specimens and measurements for the ultrasonic parameters were made. However, bi-directional measurements were applied along the load direction and the perpendicular direction to the load line by means of the contact type probe of which the central frequencies are 10MHz, 15MHz and 20MHz. Analyzing the angular velocities of the ultrasonic signals obtained from the load direction, it was confirmed that the angular velocities were declined as the creep time passed when 15MHz and 20MHz probes were used. Also, the group velocities were declined for all three frequencies as the creep time increased. Thus, positive feasibility for the creep damage evaluation by means of the angular and group velocities was confirmed. Moreover, result of analysis for the ultrasonic signal which was obtained from the perpendicular direction upon the angular and group velocities indicated little variation for both of the angular and group velocities. Therefore, the creep damage is likely to represent anisotropic itself.

• 한국표면공학회지
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• 제46권5호
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• pp.192-196
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• 2013

Stainless steels (AISI 316L) are carburized by Inductively coupled plasma using $CH_4$ and Ar gas. The ${\gamma}_c$ phase(S-phase) is formed on the surface of stainless steel after carburizing process. The XRD peak of carburized samples is shifted to lower diffracting angle due to lattice expansion. Overall, the thickness of ${\gamma}_c$ phase showed a linear dependence with respect to increasing temperature due to the faster rate of diffusion of carbon. However, at temperatures above 500, the thickness data deviated from the linear trend. It is expected that the deviation was caused from atomic diffusion as well as other reactions that occurred at high temperatures. The interfacial contact resistance (ICR) and corrosion resistance are measured in a simulated proton exchange membrane fuel cell (PEMFC) environment. The ICR value of the carburized samples decreased from 130 $m{\Omega}cm^2$ (AISI 316L) to about 20 $m{\Omega}cm^2$. The sample carburized at 200 showed the best corrosion current density (6 ${\mu}Acm^{-2}$).

• 한국분말재료학회지
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• 제29권1호
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• pp.1-7
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• 2022

This study investigates the effect of process stopping and restarting on the microstructure and local nanoindentation properties of 316L stainless steel manufactured via selective laser melting (SLM). We find that stopping the SLM process midway, exposing the substrate to air having an oxygen concentration of 22% or more for 12 h, and subsequently restarting the process, makes little difference to the density of the restarted area (~ 99.8%) as compared to the previously melted area of the substrate below. While the microstructure and pore distribution near the stop/restart area changes, this modified process does not induce the development of unusual features, such as an inhomogeneous microstructure or irregular pore distribution in the substrate. An analysis of the stiffness and hardness values of the nano-indented steel also reveals very little change at the joint of the stop/restart area. Further, we discuss the possible and effective follow-up actions of stopping and subsequently restarting the SLM process.