• 제목/요약/키워드: 12-step method

검색결과 684건 처리시간 0.026초

Application of Polyurethane Foam Loaded with a Schiff Base Ligand for Determination of Trace Amounts of Copper in Water Samples by Flame Atomic Absorption Spectroscopy

  • Moftakhar, Mahdieh Koorehpazan;Yaftian, Mohammad Reza;Nahaei, Samaneh;Zamani, Abbas Ali
    • 대한화학회지
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    • 제58권3호
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    • pp.283-288
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    • 2014
  • A column solid phase extraction procedure based on modified polyurethane foam (PUF) by a newly synthesized Schiff base ionophore, named 2,2'-{iminobis[propane-3,1-diylnitrilo(1E)prop-1-yl-1-ylidene]}diphenol, was developed for preconcentration step of trace amounts determination of copper ions in water samples by atomic absorption flame spectroscopy. The influence of parameters on the adsorption process such as sample pH, amount of modified PUF packed in the column, type and volume of stripping reagent and its flow rate were investigated and optimized. Under optimum experimental conditions, the calibration graph was linear in a relatively wide range ($0.005-210{\mu}g/ml$) with a limit of detection $0.002{\mu}g/ml$ of copper. The proposed method allows achieving to a concentration factor of >133. The capacity of a column (1.6 cm i.d.) packed by 6 g of PUF modified by 12 mg of the Schiff base was found to be $247.7({\pm}2.1){\mu}g$ of copper. It was found that the adsorption process was highly selective towards copper ions with respect to some associated metal ions. The presented procedure was successfully applied for determination of copper in some water samples.

A Study on the Positive Rates of HBsAg and Anti-HBs from Old People's Home and Casual Ward in Daegu, Korea

  • Shin, Hyun Gyu
    • 대한임상검사과학회지
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    • 제43권4호
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    • pp.145-149
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    • 2011
  • Serum hepatitis is still recognized as a major public health problem in many countries. The most common etiologies are acute viral hepatitis A and B, and hepatitis B virus (HBV) was known as the pathogen of serum hepatitis. since the HBV causes chronic hepatitis. HBV infection is hyperendemic in Korea. It is known that 8% and 1% of the Korean population is chronic carriers of HBV. The total number of 487 serum specimen (old people's home 190, causal ward-Daegu hope village 297) were collected at the laboratory of Department of Clinical Pathology of Daegu medical center. The laboratory tested the specimen to detect for hepatitis B surface antigen (HBsAg) and anti-HBs using reverse passive hemag-glutination (RPHA) and passive hemagglutination (PHA) method between April, 2011 and June, 2011. In one-step test, HBsAg and anti-HBs of Humasis were used. The positive rate for HBsAg was 6.80% (33/487), and the rate in male was 6.93% (19/274) higher than that of female 6.57% (14/213). In the positive rate of HBsAg by age group, the highest positive rate group was in the group of 40-49 years in male (12.0%), and 50-59 years in female (17.65 %). The overall positive rate for anti-HBs was 42.70% (208/487), showing the higher positive rate of 43.80% in male (120/274) than that of 41.30% (88/213) in female. The highest positive rate of anti-HBs in age group was the 40-49 years group in male (52.00%) and the group of under 29 in female (66.67%).

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지적기준점 성과계산을 위한 GPS 소프트웨어 개발 (GPS Software Development for Calculation of Cadastral Control Points)

  • 우인제;이종기;김병국;이민석
    • Spatial Information Research
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    • 제12권1호
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    • pp.101-110
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    • 2004
  • GPS 관측기법을 지적측량에 도입하기 위하여 GPS를 이용한 새로운 지적측량 모형(Model)을 정립하는 연구와 관련 기술들을 개발하는 연구가 활발히 진행되고 있다. 이와 같은 추세에 발맞추어 GPS 자료처리 및 기준점 성과산출과 관련하여 국내·외 측량 관련 상용 GPS 자료처리 소프트웨어의 현황 및 성능을 파악하고, 자료처리 알고리즘을 분석하여, 우리 실정에 적합한 GPS 자료처리 소프트웨어를 개발하는 것을 본 연구의 목적으로 한다. 본 연구에서는 국내ㆍ외의 전문 업체, 기관(대학)이 보유하고 있는 상용 소프트웨어 현황 분석 및 자료처리 방법에 따른 오차 발생을 연구하여 기선해석, 망 조정, 좌표변환 등에 관련된 전문 소프트웨어 기능을 비교 분석하여 자료처리 산출성과의 정확도를 향상시키는 방향을 모색한다. 또한 기존 GPS 자료처리 소프트웨어에 적용된 알고리즘을 분석하고 지적측량성과 산출에 최적인 알고리즘을 연구하여 새로운 지적기준점 성과 산출을 위한 지적측량 성과계산 소프트웨어를 개발한다.

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의류생산 정보의 커뮤니케이션 (A Study on the Communication of Clothing Manufacturing Information)

  • 허은영;조진숙
    • 복식
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    • 제38권
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    • pp.289-304
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    • 1998
  • In Korean clothing industry, most of the manufactures produce garments by subcon-tractors partially or entirely. It is very often that the design part is remote from production part and there is miscommunication between these two parts resulting dissatisfaction to both. Therefore it is very important to communicate the manufacturing information clearly and quickly to produce garments exactly the design part intended. Also to automate the clothing out how to produce and use the information objectively and efficiently. As a first step of moving to automation, the purpose of the research is to find out how manufacturing information and data are communicated in clothing manufacturing at present. In order to follow the information flow of a cer-tain manufacturer, the case study method was used. The case study samples were 12 clothing firms of 13 brands. The results and suggestions are as follows :- 1. A manufacturing information is communicated through paper documents such as“Production Order”, sample and patterns. At present, a production order sheet is the most efficient communication media, which comprises most of the information being communicated. 2. A manufacturing information comprises control information on the product, design in-formation, pattern information, cutting information, material information, sewing information, production schedule information, quality control information, costing information and information about the subcontractors. 3. A manufacturing is not quite objective except pattern information and cutting information which is presented by CAD systems. The communication of design information and sewing information should be somehow more objective. 4. There is not much information from a subcontractor. Considering that a subcontractor is the other partener of the communication, more information from the subcontractor is required for both benefit. 5. A designer produce most of the manufacturing information, but the information is communicated through a production manager to the subcontractor. The difference between the information maker and information communicator can cause any miscommunication. In future automated manufacturing, it will be possible for the designer to communicate to the manufacturer directly from the early stage of designing.

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황화 암모늄을 이용한 Al2O3/HfO2 다층 게이트 절연막 트랜지스터 전기적 및 계면적 특성 향상 연구 (Improvement of the carrier transport property and interfacial behavior in InGaAs quantum well Metal-Oxide-Semiconductor Field-Effect-Transistors with sulfur passivation)

  • 김준규;김대현
    • 센서학회지
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    • 제29권4호
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    • pp.266-269
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    • 2020
  • In this study, we investigated the effect of a sulfur passivation (S-passivation) process step on the electrical properties of surface-channel In0.7Ga0.3As quantum-well (QW) metal-oxide-semiconductor field-effect transistors (MOSFETs) with S/D regrowth contacts. We fabricated long-channel In0.7Ga0.3As QW MOSFETs with and without (NH4)2S treatment and then deposited 1/4 nm of Al2O3/HfO2 through atomic layer deposition. The devices with S-passivation exhibited lower values of subthreshold swing (74 mV/decade) and drain-induced barrier lowering (19 mV/V) than the devices without S-passivation. A conductance method was applied, and a low value of interface trap density Dit (2.83×1012 cm-2eV-1) was obtained for the devices with S-passivation. Based on these results, interface traps between InGaAs and high-κ are other defect sources that need to be considered in future studies to improve III-V microsensor sensing platforms.

Ceramic 재질을 이용한 자동차용 대형 디젤 엔진 Valve Lifter 연구 I. Brazing Process에 의한 Ceramic-Metal 접합체 개발 (Studies of Valve Lifter for Automotive Heavy Duty Diesel Engine by Ceramic Materials I. Developmet of Ceramic-Metal Joint by Brazing Method)

  • 윤호욱;한인섭;임연수;정윤중
    • 한국세라믹학회지
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    • 제35권2호
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    • pp.163-171
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    • 1998
  • Continuously contacting with camshaft the face of Valve Lifter made of cast iron brings about abnormal wear such as unfairwear or earlywear because it is heavily loaded in the valve train systems as the engine gets more powered. This abnormal wear becomes a defet namely over-clearance when the valve is lifting so that the fuel gas imperfectly combusted by unsuitable open or close aaction of the engine valve in the combustion chamber. The imperfect combustion in the end results in the major cause of air pollution and combustion chamber. The imperfectly combusted by unsuitable open or close action of the engine valve in the combustion chamber. The imperfect combustion in the end results in the major causes of air pollution and decrease of the engine output. Consequently to prevent this wear this study was to develop the valve lifter which is joined by brazing process with SCM435H and a tip by manufacturing the face as a superhardened which is joined by brazing process with SCM435H and a tip by manufacturing the face as a superhardened ceramics alloy which has high wear resistance. Having the excellent surface hardness with Hv1100-1200 the sintered body developed with superhardened alloy(WC) can endure the severe face loading in the valve train system. We experienced with various brazing alloys and obtained the excellent joining strength to the joint had 150MPa shear strength. Interface analysis and microstructure in a joint were examined through SEM & EDS Optical microscope. Also 2,500 hours high speed(3,000-4,000 rpm) and continuous (1step 12hr) engine dynamo testing was carried out to casting valve liter and ceramics-metal joint valve lifter so that the abnormal wears were compared and evaluated.

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멀티미디어 인터넷망의 최적화 전송을 위한 라벨링망 응용 정책설정 고찰 (Labeling network applicaion study policy settings for optimized transmission of multimedia internet)

  • 구현실;황성규
    • 한국정보통신학회논문지
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    • 제19권8호
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    • pp.1780-1784
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    • 2015
  • 현재의 IP 라우팅은 Layer 3 라우팅 정보를 이용하여 Forwarding시 Destination Address만을 참조하며 Destination-Based Routing Lookup은 모든 Hop에서 필요하다. 따라서 모든 라우터는 Full Internet 라우팅 정보, 약 12만 여개의 라우트 정보를 필요로 할 수 있으며 라우터는 이러한 폭주에 따라 트래픽 부하를 분산 할 수 있는 환경 구성이 필요하다. 본 연구에서는 인터넷 기존망의 고유 특징인 Best Effect 환경에서 대용량 멀티미디어 데이터 전송의 QoS 보장과 하드웨어적 고속 스위칭을 위해 Labeling을 이용하여 packet을 forwarding하는 환경 구성이 필요하다. 데이터 전송을 고성능화하기 위해서 라벨링망의 여러 단계의 정책보다는 프로세스 등 자원 효율화와 단순화 정책이 효과적인지 연구를 통해 알아보며 그 방안으로 일명 lock-up 라벨링망 Header Format으로 고정시켜 단순화된 정책으로 보다 QoS에 효과적인 정책을 적용하는 방법을 고찰한다.

후두결핵의 임상양상과 진단 (Clinical Characteristics and Diagnosis of Laryngeal Tuberculosis)

  • 조현진;소윤경;손영익
    • 대한후두음성언어의학회지
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    • 제19권1호
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    • pp.43-46
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    • 2008
  • Background and Objectives : Clinical suspicion and appropriate diagnostic procedures are essential for the timely management of extrapulmonary type of mycobacterial disease. In the hope of suggesting a suitable guideline for the early diagnosis of laryngeal tuberculosis, the authors reviewed their clinical pathways and the characteristics of patients with laryngeal tuberculosis who were managed in the recent 10 years at a single tertiary referral hospital, Samsung Medical Center. Subjects and Method : Retrospective chart review was performed for the 25 adult patients with laryngeal tuberculosis. Among 25 cases, 12 were pathologically confirmed by laryngeal biopsy and the other 13 were clinically diagnosed by cumulative clinical information; definite laryngitis on laryngoscopy, positive AFB (acid fast bacillus) smear/culture or active pulmonary tuberculosis on chest X-ray, and substantial response to anti-tuberculosis medication. Results : Chest X-ray revealed active pulmonary tuberculosis in 72% of patients (N=18/25). Sputum AFB smear/culture was positive in 95% of all tested patients (N=21/22) and in 100% of the tested patients who have stable or no evidence of pulmonary tuberculosis (N=5/5). All patients except one who had coexisting laryngeal malignancy showed considerable improvement in their subjective symptoms and laryngeal findings within the first 2 months of anti-tuberculosis medications and they achieved complete response on subsequent sputum studies, chest X-ray and laryngeal findings after $7.0{\pm}2.3$ months of the medications. Conclusion : We suggest that chest X-ray and sputum AFB smear/culture to be the first step of work-up for the patients having laryngeal tuberculosis in suspicion since laryngeal tuberculosis is largely associated with active pulmonary tuberculosis and/or sputum AFB study offers high yield even in case of primary laryngeal tuberculosis. However laryngeal biopsy must be considered in case showing unsatisfactory response to the anti-tuberculosis medication for more than 2 months.

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Polychlorobiphenyl (PCB) 토양오염복원: PCB 제거 토양미생물들의 군집과 기능을 효과적으로 분석하는 신 genomics 방법개발에 관한 연구

  • 박준홍
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2005년도 총회 및 춘계학술발표회
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    • pp.28-30
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    • 2005
  • Because of high population diversity in soil microbial communities, it is difficult to accurately assess the capability of biodegradation of toxicant by microbes in soil and sediment. Identifying biodegradative microorganisms is an important step in designing and analyzing soil bioremediation. To remove non-important noise information, it is necessary to selectively enrich genomes of biodegradative microorganisms fromnon-biodegradative populations. For this purpose, a stable isotope probing (SIP) technique was applied in selectively harvesting the genomes of biphenyl-utilizing bacteria from soil microbial communities. Since many biphenyl-using microorganisms are responsible for aerobic PCB degradation In soil and sediments, biphenyl-utilizing bacteria were chosen as the target organisms. In soil microcosms, 13C-biphenyl was added as a selective carbon source for biphenyl users, According to $13C-CO_2$ analysis by GC-MS, 13C-biphenyl mineralization was detected after a 7-day of incubation. The heavy portion of DNA(13C-DNA) was separated from the light portion of DNA (12C-DNA) using equilibrium density gradient ultracentrifuge. Bacterial community structure in the 13C-DNAsample was analyzed by t-RFLP (terminal restriction fragment length polymorphism) method. The t-RFLP result demonstates that the use of SIP efficiently and selectively enriched the genomes of biphenyl degrading bacteria from non-degradative microbes. Furthermore, the bacterial diversity of biphenyl degrading populations was small enough for environmental genomes tools (metagenomics and DNA microarrays) to be used to detect functional (biphenyl degradation) genes from soil microbial communities, which may provide a significant progress in assessing microbial capability of PCB bioremediation in soil and groundwater.

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FoLT-PCR에 의한 유전자형 (HumTH01, HumTPOX, HumCSF1PO & Amelogenin) 분석 (Quadruplex Genotype Analysis at HumTH01, HumTPOX, HumCSF1PO and Amelogenin Loci by FoLT-PCR)

  • 이양한;임시근;강필원;최동호;윤송노;한면수
    • 분석과학
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    • 제12권3호
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    • pp.260-264
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    • 1999
  • 법적시료(Forensic Evidences)로 사용되는 혈흔, 정액반, 타액반 및 모발을 DNA의 분리과정 없이 FoLT (Formamide Low Temperature) PCR법으로 DNA의 특정부위를 분석하고자 하였다. FoLT PCR법으로 3종류의 STR(Short Tandem Repeat) 좌위와 성별을 확인하는 Amelogenin gene을 PCR법으로 동시에 분석하기 위하여 formamide농도와 annealing온도를 검토한 바 최적의 formamide농도는 8%(v/v)이었고 annealing온도는 $48^{\circ}C$이었다. 그리고 1% Triton X-100을 이용하여 시료를 세척한 경우에 증폭 효율이 증가하였다. 따라서 FoLT-PCR법을 이용한 경우 DNA를 분리하기 위한 전처리없이 소량의 시료를 기존의 PCR법보다 빠른 시간내에 한번의 PCR 및 전기영동으로 HumTH01, HumTPOX, HumCSF1PO 및 Amelogenin을 동시에 분석할 수 있었다.

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