• Title/Summary/Keyword: 현장 검출장비

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A Study on the Sediment Transport using Radioisotope Tracer (방사성동위원소 추적자를 이용한 표사이동 추적실험)

  • Choi Byung-Jong;Jung Sung-Hee;Kim Jong-Bum;Lee Jong-Sup
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.16 no.3
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    • pp.162-170
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    • 2004
  • On the basis of the radiotracer technology and the related equipments which have been developed for its industrial application through the nuclear long-term research project, a radiotracer study on sediment transport was carried out as a part of the development of the radiotracer technology for a coastal environment. The crystalline material doped with iridium having a similar composition and specific gravity as those of the bedload sand collected from the research area was produced by the oxide-route method. A radioisotope container was specially designed to inject the radiotracer from 1 m above the sea bedload without radioactive contamination during the transport from the nuclear reactor at KAERI. The position data from the DGPS and the radiation measurement data were collected concurrently and stored by means of the application software programmed with the LabVIEW of the National Instrument. The position data was reprocessed to represent the real position of the radiation probe under water and not that of the DGPS antenna on board. The time dependency of the spatial distribution of the sediment was studied in the area through three tracking measurements after the iridium glass was injected. This trial application showed the potential of the radiotracer technology as an important role for maintaining and developing the coastal environment in the future.

담자균 균사체 발효음료의 기능성 검토

  • 박찬성;최미애
    • Proceedings of the Korean Society of Postharvest Science and Technology of Agricultural Products Conference
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    • 2003.10a
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    • pp.148.1-148
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    • 2003
  • 버섯은 균사체와 자실체를 가진 고등균류로서 옛날부터 식용은 물론 약용으로 많이 사용되어 왔으며 부작용이 없는 저칼로리 식품으로서, 영양적인 측면과 의약품으로서의 효능을 가진 식품으로 인식되어 소비량이 날로 증가하는 추세이다. 버섯은 항균자용, 항암작용, 면역증강작용, 혈압강하 효과 및 혈중 콜레스테롤합성 억제효과 등의 다양한 생리활성을 나타내고 있어 국내에서도 버섯의 균사체 배양이 활기를 띄고 있다. 본 연구에서는 5종류의 버섯(아가리쿠스, 상황, 노루궁뎅이, 운지, 동충하초)의 균사체 배양원액을 10%, 30%, 50%, 100% 함유한 음료로서 전자공여능, 아질산염소거능, MDA cell과 A549 cell에 대한 암세포 증식억제 작용을 조사하였다. 5종류의 버섯 균사체 음료의 전자공여능은 발효원액을 30% 함유한 경우에 72∼89%였으며 100% 원액의 경우는 87∼93%의 탁월한 항산화능을 나타내었다. 균사체 음료의 아질산염 소거능은 노루궁뎅이버섯이 가장 높아서 균사체 원액은 73%, 112 희석액은 51%였으며 다음은 동충하초의 균사체 원액이 52%를 나타내었고 나머지 3종류의 버섯 균사체는 28∼36%의 아질산염소거능을 나타내었다. 균사체 발효음료 원액은 MBA cell에 대하여 5종류의 버섯 모두에서 82∼85%의 높은 암세포 증식억제작용을 나타내었고 동충하초는 1/2 희석액에서도 80%이상의 증식억제활성을 나타내었다. 균사체 발효음료 원액의 A549 cell에 대한 증식억제능은 동충하초 발효원액이 68%, 상황 발효원액이 50%로서 MDA cell에 대한 증식억제효과 보다는 효능이 낮은 편이었다. 전체적으로 5종류의 버섯 균사체 발효음료는 항산화작용, 아질산염소거능, 항암활성이 우수한 기능성 음료로 활용될 수 있을 것으로 생각된다.적으로 평가하는데 적합하나 아직 국내에선 X-선을 이용한 가공용 감자의 내부 결함특성에 대한 연구는 이뤄지지 않고 있다. 이에 본 연구에서는 가공용 감자의 내부결함 특성중 하나인 내부동공의 X-선에 의한 특성을 본 연구소에 있는 X-선 발생장비로 측정해 보고 비파괴적인 방법으로 실시간 가능성을 시험하였다. 감자는 수원 농산물 도매시장에서 2003년산 가공용 감자 (품종:선농)를 구매하여 사용하였다. 감자내 내부동공은 35 ∼ 40 kV와 5.25 mA값으로 발생된 X-선에 의해 잘 검출되는 것으로 나타나, 현장에서 충분히 활용가능 할 것으로 판단되었다. 금후, 실시간으로 내부동공을 검출할 수 있는 시스템을 개발할 계획이다.정한 결과 메탄올에서는 5% 농도차이가 그 추출효율에 유의적인 영향을 주지 않는 것으로 나타났다. 에탄올에서는 40%에서 가장 높은 함량이 측정되었고 아세톤에서는 50%에서 측정되었다. 따라서 시료의 상태와 상관없이 배 과피의 페놀성물질 추출용매로는 40∼70%의 함수 아세톤이 적합한 것으로 사료된다.en delicious는 상온에서60일 동안 보관하였을 경우, 사과표피의 색도 변화를 현저히 지연시킴을 확인하였다. 또한 control과 비교하여 성공적으로 사과에 코팅하였으며, 상온에서 보관하여을 때 사과의 품질을 30일 이상 연장하는 효과를 관찰하였다. 이들 결과로부터 대두단백질 필름이 과일 등의 포장제로서 이용할 가능성을 확인하였다.로 [-wh] 겹의문사는 복수 의미를 지닐 수 없 다. 그러면 단수 의미는 어떻게 생성되는가\ulcorner 본 논문에서는 표면적 형태에도 불구하고 [-wh]의미의 겹의문사는 병렬적 관계의 합성어가 아니라 내부구조를 지니지 않은 단순한 단어(minimal $X^{0}$ elements

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The Study on Analysis Method and Performance Evaluation of Portable GC/MS (휴대용 GC/MS 성능검사 및 분석방법 연구)

  • Park, Yuonshin;Noh, Hyeran;Yang, Heeseon;Seok, Gwanseol
    • Journal of the Society of Disaster Information
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    • v.9 no.3
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    • pp.249-258
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    • 2013
  • Recieved Mar. 06, 2013 Revised Mar. 29, 2013 Accepted Sep. 11, 2013In this study, we evaluated the method performance and the optimum sample injection method of the portable GC/MS(HAPSITE) which were designed to operate on scene of chemical accidents. Chemicals used for performance test were vinyl chloride(VC), methyl chloride(MC), benzene(Bz), toluene(Tol). CRM(Certified Reference Material) Manufactured by KRISS(Korea Research Institute of Standards and Science) was used as the standard gas. The results showed that 1) Among three sample injection methods(Cylinder, Silico canister, and Bag), bag was identified as the most appropriate sample injection method. Bag material and capacity did not significantly affect the results. The most ideal reproducibility occurred at the 2-minute point of the purge time in the loop and tenax methods. 2) Performance evaluation of HAPSITE was conducted. Evaluation items were reproducibility, linearity, method detection limit, etc. Tenax concentration method was appropriate for larger molecules and Carbopack concentration method was suitable for smaller molecules.

Field Application of Phased Array Ultrasonic Testing for Structural Weld Overlay on Dissimilar Welds of Pressurizer Nozzles (가압기 노즐 이종금속 용접부의 구조적 오버레이 용접부에 대한 위상배열 초음파기법의 현장 적용)

  • Kim, Jin-Hoi;Kim, Yongsik
    • Journal of the Korean Society for Nondestructive Testing
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    • v.35 no.4
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    • pp.268-274
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    • 2015
  • Weld overlay was first used in power plants in the US in the early 1980s as an interim method of repairing the welds of flawed piping joints. Weld overlaid piping joints in nuclear power plants must be examined periodically using ultrasonic examination technology. Portable phased array ultrasonic technology has recently become available. Currently, the application of preemptive weld overlays as a mitigation technique and/as a method to improve the examination surface condition for more complex configurations is becoming more common. These complex geometries may require several focused conventional transducers for adequate inspection of the overlay, the original weld, and the base material. Alternatively, Phased array ultrasonic probes can be used to generate several inspection angles simultaneously at various focal depths to provide better and faster coverage than that possible by conventional methods. Thus, this technology can increase the speed of examinations, save costs, and reduce radiation exposure. In this paper, we explain the general sequence of the inspection of weld overlay and the results of signal analysis for some PAUT (phased array ultrasonic testing) signals detected in on-site inspections.

A Preliminary Study on the Fire Safety Testing Method for Fire-resistance Paints Using an X-ray Analysis Method (X-선 분석법을 이용한 내화도료의 화재안전성 평가 방법에 관한 기초연구)

  • Shim, Ji-Hun;Cho, Nam-Wook;Kim, Kang-Woo
    • Fire Science and Engineering
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    • v.28 no.5
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    • pp.58-63
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    • 2014
  • Fire-resistance paints are supposed to become intumescent and diminish heat transfer along the steel frames in case of a fire. If unsatisfactory fire-resistance paints which do not satisfy their standard specification are used, it may result in a severe disaster. Because satisfactory fire-resistance paints are hardly discriminated from the unsatisfactory ones by a simple visual inspection, more reliable and convenient onsite evaluation methods are necessary. Here we report the preliminary study result on the fire safety testing method for fire-resistance paints using an X-ray analysis method. It was found that the existence and quantity of effective constituents in fire-resistance paints can be detected by the X-ray analysis method. X-ray fluorescence (XRF) analyses showed that P and Cl elements are much more enriched in fire-resistance paints, compared to normal paints. X-ray diffraction (XRD) analyses showed that ammonium polyphosphate is present as the main crystalline material in fire-resistance paints, but absent in normal paints. The X-ray analysis method is expected to be used for the onsite inspection of fire-resistance paints with the upcoming availability of portable XRF and XRD instruments.

The Basic Study on the Method of Acoustic Emission Signal Processing for the Failure Detection in the NPP Structures (원전 구조물 결함 탐지를 위한 음향방출 신호 처리 방안에 대한 기초 연구)

  • Kim, Jong-Hyun;Korea Aerospace University, Jae-Seong;Lee, Jung;Kwag, No-Gwon;Lee, Bo-Young
    • Journal of the Korean Society for Nondestructive Testing
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    • v.29 no.5
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    • pp.485-492
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    • 2009
  • The thermal fatigue crack(TFC) is one of the life-limiting mechanisms at the nuclear power plant operating conditions. In order to evaluate the structural integrity, various non-destructive test methods such as radiographic test, ultrasonic test and eddy current are used in the industrial field. However, these methods have restrictions that defect detection is possible after the crack growth. For this reason, acoustic emission testing(AET) is becoming one of powerful inspection methods, because AET has an advantage that possible to monitor the structure continuously. Generally, every mechanism that affects the integrity of the structure or equipment is a source of acoustic emission signal. Therefore the noise filtering is one of the major works to the almost AET researchers. In this study, acoustic emission signal was collected from the pipes which were in the successive thermal fatigue cycles. The data were filtered based on the results from previous experiments. Through the data analysis, the signal characteristics to distinguish the effective signal from the noises for the TFC were proven as the waveform difference. The experiment results provide preliminary information for the acoustic emission technique to the continuous monitoring of the structure failure detection.

Improvement of Microwave Water Surface Current Meter for Oblique Angle Measurements (편각측정을 위한 위한 전자파표면유속계의 성능개편각측정을 성능개선)

  • Kim, Young-Sung;Kim, Woo-Gu;Yang, Jae-Rheen;Koh, Deuk-Koo
    • Proceedings of the Korea Water Resources Association Conference
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    • 2008.05a
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    • pp.1789-1793
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    • 2008
  • 전자파표면유속계는 홍수유속측정을 위하여 개발된 기기로 평 갈수기에는 유속측정이 불가하여 프로펠러 유속계를 이용하고 있다. 현재 보급된 전자파표면유속계는 하천의 흐름방향에 나란하게 설치하였을 때에만 유속을 측정할 수 있는 기기의 구조상의 한계성 때문에 교량이 없는 지점에서는 유속측정이 불가하여 유량산정을 할 수가 없다. 또한 편각측정이 불가능하여 기기를 각 측선마다 이동 설치하여야 하기 때문에 유속측정시 효율성 떨어진다. 이에 홍수시 유량측정의 효율성을 증대시키고 전자파표면유속계의 활용도를 높이고자 편각측정이 가능하도록 전자파표면유속계의 성능을 개선하는 것이 본 연구의 주된 목적이다. 전자파표면 유속계에서의 편각 측정은 하천의 유속방향을 기준으로 정면에서 측정하면 수평 편각이 0도가 되며 좌우로 안테나를 회전하여 움직인 각도가 측정 편각으로 결정된다. 현장에서 전자파표면유속계의 사용시 편의성을 높이고 유량측정을 효율적으로 하기 위해서는 가급적 편각을 크게 해서 측정을 해야 하지만, 편각이 증가하면 전자파의 물리적 특성 때문에 반사된 신호의 수신 크기가 감소하여 측정이 불가능하게 된다. 이러한 문제를 해결하기 위해서는 유속 측정시 전자파 출력을 기존의 시스템보다 높게 물표면에 발사하여야 하며 안테나를 포함한 RF 모듈의 수신감도 및 지향성이 개선되어야 한다. 이에 편각측정이 가능하도록 이러한 사항에 주안점을 두어 새로운 시스템을 구성하였다. 수신감도 향상을 위해서는 물표면에 반사되어 돌아오는 신호를 가장 먼저 수신하는 안테나의 특성이 중요하며 그 다음 수신용 증폭기, IF 증폭기 순으로 개선이 필요하다. 본 연구에서는 안테나의 형태를 기존 파라볼릭 안테나에서 위상 배열 평면안테나로 변경하였으며, 이에 따른 이점으로는 송수신부를 분리하여 하나의 평면에 두 개의 안테나를 구성할 수 있다는 사항이다. 즉 외형적으로는 하나의 안테나로 보이지만 두 개의 안테나가 하나로 구성된 것이다. 송수신부를 분리하는 형태는 기존 파라볼릭 안테나에선 불가능한 구조로 변경에 따른 수신감도 향상은 수치적으로 10dB 이상 개선하였다. 송수신부 분리가 수신감도에 영향을 미치는 이유는 물표면으로 발사된 송신 신호의 일부가 수신단으로 유입되는 현상으로 누설되는 송신 신호를 최대한 차단하는 분리도가 수신 신호 검출에 직접적인 양향을 주기 때문에다. 평면 안테나를 적용하면 기존 파라볼릭 안테나에서 사용하던 써큘레이터라는 부품을 삭제할 수 있으며, 안테나의 구조적인 분리를 통해서 수신감도를 개선할 수 있었다. 안테나의 지향성은 발사하는 전자파의 빔폭 성능과 일치하며 각도 단위로 표시한다. 각도 값이 작을수록 전자파의 에너지가 한 곳에 집중된다고 말할 수 있다. 즉 빔폭이 크면 측정시 반사면적이 커져 정확한 지점의 유속을 측정하기 어려운 문제가 발생한다. 본 연구를 통해 빔폭은 기존 안테나 대비2도를 개선하였으며 25%의 개선 효과를 얻었다. 또한 수신감도 및 지향성 개선과 더불어 전자파의 출력을 기존 장비 대비하여 1.6배를 증가하여 편각측정을 위한 전자파표면 유속계의 성능을 개선하였다.

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A Practical Method to Quantify Very Low Fluxes of Nitrous Oxide from a Rice Paddy (벼논에서 미량 아산화질소 플럭스의 정량을 위한 실용적 방법)

  • Okjung, Ju;Namgoo, Kang;Hoseup, Soh;Jung-Soo, Park
    • Korean Journal of Agricultural and Forest Meteorology
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    • v.24 no.4
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    • pp.285-294
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    • 2022
  • In order to accurately calculate greenhouse gas emissions in the agricultural field, Korea has been developing national-specific emission factors through direct measurement of gas fluxes using the closed-chamber method. In the rice paddy, only national-specific emission factors for methane (CH4) have been developed. It is thus necessary to develop those for nitrous oxide (N2O) affected by the application of nitrogen fertilizer. However, since the concentration of N2O emission from rice cultivation is very low, the QA/QC methods such as method detection and practical quantification limits are important. In this study, N2O emission from a rice paddy was evaluated affected by the amount of nitrogen fertilizer, by taking into account both method detection and practical quantification limits for N2O concentration. The N2O emission from a rice paddy soils affected by the nitrogen fertilizer application was estimated in the following order. The method detection limit (MDL) of N2O concentration was calculated at 95% confidence level based on the pooled standard deviation of concentration data sets using a standard gas with 98 nmol mol-1 N2O 10 times for 3 days. The practical quantification limit (PQL) of the N2O concentration is estimated by multiplying 10 to the pooled standard deviation. For the N2O flux data measured during the rice cultivation period in 2021, the MDL and PQL of N2O concentration were 18 nmol mol-1 and 87 nmol mol-1, respectively. The measured values above the PQL were merely about 12% of the total data. The cumulative N2O emission estimated based on the MDL and PQL was higher than the cumulative emission without nitrogen fertilizer application. This research would contribute to improving the reliability in quantification of the N2O flux data for accurate estimates of greenhouse gas emissions and uncertainties.

A standardized procedure on building spectral library for hazardous chemicals mixed in river flow using hyperspectral image (초분광 영상을 활용한 하천수 혼합 유해화학물질 표준 분광라이브러리 구축 방안)

  • Gwon, Yeonghwa;Kim, Dongsu;You, Hojun
    • Journal of Korea Water Resources Association
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    • v.53 no.10
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    • pp.845-859
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    • 2020
  • Climate change and recent heat waves have drawn public attention toward other environmental issues, such as water pollution in the form of algal blooms, chemical leaks, and oil spills. Water pollution by the leakage of chemicals may severely affect human health as well as contaminate the air, water, and soil and cause discoloration or death of crops that come in contact with these chemicals. Chemicals that may spill into water streams are often colorless and water-soluble, which makes it difficult to determine whether the water is polluted using the naked eye. When a chemical spill occurs, it is usually detected through a simple contact detection device by installing sensors at locations where leakage is likely to occur. The drawback with the approach using contact detection sensors is that it relies heavily on the skill of field workers. Moreover, these sensors are installed at a limited number of locations, so spill detection is not possible in areas where they are not installed. Recently hyperspectral images have been used to identify land cover and vegetation and to determine water quality by analyzing the inherent spectral characteristics of these materials. While hyperspectral sensors can potentially be used to detect chemical substances, there is currently a lack of research on the detection of chemicals in water streams using hyperspectral sensors. Therefore, this study utilized remote sensing techniques and the latest sensor technology to overcome the limitations of contact detection technology in detecting the leakage of hazardous chemical into aquatic systems. In this study, we aimed to determine whether 18 types of hazardous chemicals could be individually classified using hyperspectral image. To this end, we obtained hyperspectral images of each chemical to establish a spectral library. We expect that future studies will expand the spectral library database for hazardous chemicals and that verification of its application in water streams will be conducted so that it can be applied to real-time monitoring to facilitate rapid detection and response when a chemical spill has occurred.

Improvement of analytical methods for arsenic in soil using ICP-AES (ICP-AES를 이용한 토양 시료 중 비소 분석 방법 개선)

  • Lee, Hong-gil;Kim, Ji In;Kim, Rog-young;Ko, Hyungwook;Kim, Tae Seung;Yoon, Jeong Ki
    • Analytical Science and Technology
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    • v.28 no.6
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    • pp.409-416
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    • 2015
  • ICP-AES has been used in many laboratories due to the advantages of wide calibration range and multi-element analysis, but it may give erroneous results and suffer from spectral interference due to the large number of emission lines associated with each element. In this study, certified reference materials (CRMs) and field samples were analyzed by ICP-AES and HG-AAS according to the official Korean testing method for soil pollution to investigate analytical problems. The applicability of HG-ICP-AES was also tested as an alternative method. HG-AAS showed good accuracies (90.8~106.3%) in all CRMs, while ICP-AES deviated from the desired range in CRMs with low arsenic and high Fe/Al. The accuracy in CRM030 was estimated as below 39% at the wavelength of 193.696 nm by ICP-AES. Significant partial overlaps and sloping background interferences were observed near to 193.696 nm with the presence of 50 mg/L Fe and Al. Most CRMs were quantified with few or no interferences of Fe and Al at 188.980 nm. ICP-AES properly assessed low and high level arsenic for field samples, at 188.980 nm and 193.696 nm, respectively. The importance of the choice of measurement wavelengths corresponding to relative arsenic level should be noted. Because interferences were affected by the sample matrix, operation conditions and instrument figures, the analysts were required to consider spectral interferences and compare the analytical performance of the recommended wavelengths. HG-ICP-AES was evaluated as a suitable alternative method for ICP-AES due to improvement of the detection limit, wide calibration ranges, and reduced spectral interferences by HG.