• Composites Research
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• v.16 no.3
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• pp.25-31
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• 2003

In this work the effect of surface treated SiC on thermal stability and mechanical interfacial properties of carbon fiber/epoxy resin composites. The surface properties of the SiC were determined by acid/base values and contact angles. The thermal stabilities of carbon fiber/epoxy resin composites were investigated by TGA. The mechanical interfacial properties of the composites were studied in ILSS, critical stress intensity factor ($\textrm{K}_{IC}$), and critical strain energy release rate($\textrm{G}_{IC}$) measurements. As a result, the acidically treated SiC(A-SiC) had higher acid value than untreated SiC(V-SiC) or basically treated SiC(B-SiC). According to the contact angle measurements, it was observed that chemical treatments led to an increase of surface free energy of the SiC surfaces, mainly due to the increase of the specific(polar) component. The mechanical interfacial properties of the composites including ILSS, $\textrm{K}_{IC}$, and $\textrm{G}_{IC}$ had been improved in the specimens treated by chemical solutions. These results were explained that good wetting played an important role in improving the degree of adhesion at interfaces between SiC and epoxy resin matrix.

• Korean Journal of Materials Research
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• v.4 no.7
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• pp.817-822
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• 1994

The reinforcing effect of C-shape carbon fiber was investigated as comparing to typical round-shape fiber with similar properties. The results show that C-shape fiber reinforced materials have better in almost all aspects of mechanical properties, or 218% in flexural strength, 223% flexural modulus, 157% interlamina shear strength, 227% impact strength, 184% transverse flexural strength and so on. Also in damping characteristics considerably concerned with fatigue life, friction/wear coefficient of a material, C-CF/EP had about 185% greater. In this research, we present the potential of non-circular fiber reinforcing materials by C-shape carbon fiber.

• Composites Research
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• v.13 no.4
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• pp.54-66
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• 2000

Interfacial and microfailure properties of carbon fiber/epoxy matrix composites were evaluated using both tensile fragmentation and compressive Broutman tests with an aid of acoustic emission (AE) monitoring. A polymeric maleic anhydride coupling agent and a monomeric amino-silane coupling agent were used via the electrodeposition (ED) and the dipping applications, respectively. Both coupling agents exhibited significant improvements in interfacial shear strength (IFSS) compared to the untreated case under tensile and compressive tests. The typical microfailure modes including fiber break of cone-shape, matrix cracking, and partial interlayer failure were observed during tensile test, whereas the diagonal slippage in fiber ends was observed under compressive test. For both loading types, fiber breaks occurred around just before and after yielding point. In both the untreated and treated cases AE amplitudes were separately distributed for the tensile testing, whereas they were closely distributed for the compressive tests. It is because of the difference in failure energies of carbon fiber between tensile and compressive loading. The maximum AE voltage for the waveform of carbon or basalt fiber breakages under tensile tests exhibited much larger than those under compressive tests, which can provide the difference in the failure energy of the individual failure processes.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2004.10a
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• pp.189-192
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• 2004

In this study, mode II interlaminar fracture phenomena of carbon fabric/epoxy composite for tilting train were investigated. The end notched flexural specimen containing an artificial crack with the thickness of 12.5fl11l was used. The mode II interlaminar fracture toughness was evaluated through a three point bending test and the fractured surfaces were examined through a scanning electron microscope. The experimental results obtained in this study would be applicable in the design and structural analysis of the composite structures.

• Composites Research
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• v.13 no.5
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• pp.44-49
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• 2000

Although the net-shape molding of composites is generally recommended, molded composites frequently requires cutting or grinding due to the dimensional inaccuracy for precision machine elements. The surface roughness and cutting force were also measured to investigate the surface grinding characteristics of the composites using the vitrified bonded wheel (WA, GC). The experiments were performed dry grinding conditions with respect to cutting speed, feed speed, depth of cut of the stacking sequence $[O]_{nT.}$ From the experimental investigation, the optimal conditions both the vitrified bonded wheel WA and GC for the surface grinding are suggested.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2000.11a
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• pp.119-123
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• 2000

The characteristics of fatigue life distribution for Carbon/epoxy composite laminates was investigated under tension-tension loading(R=0.1). The statistical nature of the fatigue life of the composite materials was analyzed by Weibull, normal, lognormal distributions As a result, it was observed that the correlation between the experimental results and the theoretical predictions for the fatigue life is good. The distribution of the static ultimate strength has the characteristic of lognormal distribution and distribution of the fatigue life has characteristics of the weibull distribution.

• Composites Research
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• v.12 no.2
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• pp.36-45
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• 1999

Since carbon fiber epoxy composite materials have excellent properties for structures due to their high specific strength, high modulus, high damping and low thermal expansion, the hollow shafts made of carbon fiber epoxy composites have been widely used for power transmission shafts for motor vehicles, spindles of machine tools and rollers for film manufacturing. However, the molded composite shafts are not usually accurate enough for mechanical machine elements, which require turning or grinding of composite hollow shafts. In this paper, the grinding characteristics of composite hollow shafts, which are flexible in the radial and circumferential directions, were investiaged experimentally and analytically with respect to the stacking angle, thickness and outer diameter.

• Composites Research
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• v.21 no.2
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• pp.25-30
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• 2008

A hemispherical microbond specimen adhered onto single carbon fiber has been proposed for evaluating the interfacial shear strength between epoxy and carbon fiber. Hemispherical microbond specimens showed low interfacial shear strength data and its small standard deviation as compared with the droplet one, which seemed to be caused by the reduction of the meniscus effects and of the stress concentration in the region contacting with the tip of pin hole. In comparison with the droplet specimen the hemispherical specimen showed the shear stress distribution similar to the cylindrical one in that low stress concentration arose around the contacting region. Average interfacial shear strength obtained by the hemispherical ones represented a good correlation with the hardness of the epoxy matrix.

• Composites Research
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• v.12 no.3
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• pp.84-90
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• 1999

High alumina cement(HAC) and polyvinyl alcohol(PVA) based macro-defect-free(MDF) cement composites were reinforced using short carbon fibers, 3mm in length, 1-4% in weight fraction and insoluble polymers such as polyurethane, epoxy, phenol resin, in order to increase mechanical properties and water stability. The specimens were manufactured by the low heat-press(warmpress) method. In addition, the interface and the cross-linking reaction of cement and polymers was also studied by the SEM and TEM. Flexural strength of HAC/PVA based MDF cementitious composites was proportionally decreased with increasing fiber contents due to the undensified structure around fibers. The flexural strength of insoluble polymer added specimen was decreased with increasing fiber contents, while water stability was dramatically improved. Epoxy resin added specimen showed the highest strength with increasing fiber contents, compared with other specimens. The water stability of fiber content 4% added specimen immersed in water presented about 95%, 87% at 3 and 7 days immersed in water, respectively. The interfacial adhesive strength of fiber-matrix was very much improved due to cross linking reaction of polymer and metal ions of cement. Tensile strength of insoluble polymers added composites as linearly increased with increasing the fiber contents. The epoxy resin added specimen also showed highest tensile strength. The 4% fiber added specimen presented 30~80% higher strength than controlled specimen.

• Composites Research
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• v.12 no.6
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• pp.1-7
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• 1999

The change of the coefficients of thermal expansion(CTE) of Carbon/Epoxy was investigated for the temperature variation and a prediction model for the change of CTE was proposed. Elastic properties and CTEs in the principal material directions were measured in the range of room temperature to cure temperature and characterized as functions of temperature. By applying the characterized properties to the classical lamination theory, a computational method to predict the change of CTEs of a general laminate for temperature variation was proposed. the coefficients of thermal expansion of laminates with various stacking sequences were measured and compared with those predicted. Good agreements between the predicted results and the experimental data show that the c hanges of CTEs of a general laminate for temperature variation can be predicted well by using the proposed method.