• Title/Summary/Keyword: 측정 불확도 평가

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2,500 L/s 급 복합분자펌프의 특성평가 database 구축 및 표준화 기술 개발

  • Kim, Wan-Jung;Go, Mun-Gyu;Jeong, Wan-Seop;Im, Jong-Yeon
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.08a
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    • pp.167-167
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    • 2011
  • 한국표준과학연구원에서는 국제표준화기구에서 제정한 국제규격(ISO, PNEUROP, DIN, JIS, AVS 등)에 기반을 둔 터보분자펌프의 특성평가시스템을 자체적으로 설계/제작 하였고, 터보분자펌프 1,000 L/s 급의 Database를 구축하였다. 이것을 토대로 특성평가시스템의 신뢰성 확인과 Feedback을 통한 시제품 개발 및 평가지원을 위해 터보분자펌프 2,500L/s 급의 Database를 구축한다. 터보분자펌프의 배기성능을 나타내는 가장 중요한 항목인 배기속도는 분자류 영역에 따라 상이한 가스($N_2$, He)를 사용하여 Throughput method와 Orifice method 두 가지 방법을 병행하여 측정한다. 측정함에 있어서 측정게이지, 유량계 및 Orifice conductance의 불확도에 의하여 배기 속도에 많은 측정오차를 포함하고 있다. 측정 오차를 줄이기 위하여 1% 이상의 안정성과 4%의 오차만을 허용하는 자전 회전자게이지(SRG)와 $10^{-3}$ mbar-L/s 영역까지의 유량 주입범위를 가지는 불확도 ${\pm}$3%의 정적형 유량시스템(CVFM)을 사용하였다. Orifice method의 경우 고진공영역으로 진입할수록 커질 수밖에 없는 배기속도 측정 불확도를 최소화하기 위해 검증된 유량을 이용한 Conductance 값을 제시하여 두 방법에서 얻은 배기속도의 불연속적인 문제를 해결한다. 본 연구에서는 2,500 L/s 급 터보분자펌프는 무거운 기체 $N_2$와 가벼운 기체 He을 사용하여 압축비의 변화와 분자류 영역에 따른 배기속도 변화를 연구하고, 2,500 L/s 급 터보분자펌프의 측정능력을 검증한다. 차후에 배기속도뿐만 아니라 소비전력, 소음, 진동, 온도 등의 특성평가의 전반적인 사항을 평가하여 터보분자펌프 2,500 L/s 급의 database를 완비해간다. 터보분자펌프 특성평가시스템을 사용한 1,000 L/s 급과 2,500 L/s 급 특성 Data를 비교, 분석하여 신뢰성 파악 및 표준화 방안을 개발하고, 고진공펌프 개발 주체와의 feedback 지원 기능의 infra를 구축한다.

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Uncertainty Evaluation of Color Measurement on Light Sources and Display Devices (광원 및 디스플레이 기기의 색특성 측정의 불확도 평가)

  • Park, Seong-Chong;Lee, Dong-Hoon;Kim, Yong-Wan;Park, Seung-Nam
    • Korean Journal of Optics and Photonics
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    • v.20 no.2
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    • pp.110-117
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    • 2009
  • This work introduces the uncertainty evaluation formulation on color measurement of light sources and display devices, such as CIE 1931 (x, y) chromaticity, CIE 1960 (u, v) chromaticity, correlated color temperature, and distribution temperature. All the mentioned quantities are reduced from spectral data in the visible range, for which uncertainties are strongly correlated between different wavelengths. Using matrix algebra we have formulated the uncertainty propagation from the SI- traceable spectral irradiance standard to the individual color related measurement quantities taking the correlation between wavelengths into account. As a result, we have demonstrated uncertainty evaluation examples of 3 types of light sources: CIE illuminant A, LED white light, and LCD white light. This method can be applied to any other quantities based on spectral measurement such as solar irradiance, material color measurement, etc.

Design of Simple Direct Comparison Measurement System from 10 MHz to 1 GHz for Thermistor Mounts Calibration (서미스터 마운트 교정을 위한 10 MHz에서 1 GHz 주파수 대역의 단순 직접 비교 측정시스템 설계)

  • Cha, Yun-Bae;Jang, Young-Guen;Kim, Boo-Il
    • The Journal of the Korea institute of electronic communication sciences
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    • v.15 no.3
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    • pp.405-412
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    • 2020
  • The thermistor mount is used for precise RF power measurement because the calibration factor is constant according to the change of power. The calibration factor of the standard mount can be measured with an uncertainty less than 0.5 % from the 10 MHz to 1 GHz by direct comparison with the transfer standard using the DC substitution method. Recently, as the supply of precision power meter based on DC substitution method allows simple and fast measurement, a simple direct comparison measurement system with the same level uncertainty was designed and the minimum required specifications of components through analysis of mismatch error was proposed. The uncertainty was evaluated for system validation, and the results show that uncertainties have been well maintained within 0.5 % in the measurement frequencies.

Uncertainty evaluation of dioxin analysis in blood samples (혈액 시료 중 다이옥신의 농도 분석 결과에 대한 불확도 평가)

  • Mun, Su-Jung;Kim, Byung-Hoon;Woo, Jin-Chun;Chang, Yoon-Seok
    • Analytical Science and Technology
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    • v.16 no.6
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    • pp.475-482
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    • 2003
  • Uncertainty of final measurement results considering main uncertainty sources being in dioxin analysis of a blood sample was estimated. 'The Guide to the Expression of Uncertainty in Measurement' was suggested for accomplishment of this study. After uncertainties for the 11 compounds detected in this experiment of the 17 target compounds of dioxin and furan were calculated considering the uncertainty sources of each step, uncertainty for the total dioxin concentration was estimated by combining these values. The concentration of dioxin in blood sample was expressed as $0.0746{\pm}0.0074pg$ I-TEQ/g weight or $20.68{\pm}2.04pg$ I-TEQ/g lipid, including the uncertainty values obtained in this way. The former expression indicates the conversion concentration into the sample weight and the latter one indicates the conversion concentration into the lipid weight. The quality of measured analytical results could be assured quantitatively by estimating uncertainty of measurement results and showing the range of measurand.

A Study on the Treatment of Uncertainty in Linear Regression Method for Chemical Analysis (회귀식 사용에 따른 화학 분석 과정의 불확도 처리 연구)

  • Woo, Jin-Chun;Suh, JungKee;Lim, MyungChul;Park, MinSu
    • Analytical Science and Technology
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    • v.16 no.3
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    • pp.185-190
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    • 2003
  • We applied modified least square method (MLS) and ordinary least square method (OLS) to 1st order equation for the comparison of the uncertainties calculated by these methods. The uncertainty calculated by OLS covered statistically safe interval because it was over-estimated in many cases of measurement and concentration level. But, if the uncertainty of the concentration as a reference value was comparably large (about 5% of the relative standard deviation of random scattering from the regression line and about 7% of relative standard uncertainty of reference values), then uncertainty calculated by OLS was seriously under-estimated at high concentration level. It was revealed that the calculated uncertainty didn't cover statistically safe interval at the stated confidence level. It was found that the method, MLS, described in the previously article would be valid for this calculation of uncertainty.

Development of an Performance Evaluation Method for Vehicle Detector Speed Measurement Applying Uncertainty in Measurement (측정불확도를 적용한 차량검지기 속도측정 성능평가방법 개발)

  • Lee, Hwan-Pil;Kim, Yong-Man;Kang, Dong-Yun
    • International Journal of Highway Engineering
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    • v.14 no.2
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    • pp.165-174
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    • 2012
  • In this study, a method for evaluating the performance of speed measurements was developed to assess the qualities of a vehicle detector. The evaluation method considers measurement errors that are reflected in a reference speed. For this, the concept of uncertainty in measurement was applied to the development method. Other factors such as precedent study, statistical processing techniques, and speed measurement performance method of traffic enforcement equipment and vehicle detection systems were also reviewed. Through this process, the problems of the existing evaluation methods were derived and developed for the new performance evaluation method. Vehicle detectors that are installed in the field were evaluated using the traditional assessment methods and the developed method. As a result, for traditional assessment methods, it was found that evaluation criteria are acceptable, while developed method's criteria are not acceptable. This means that traditional assessment methods do not sufficiently consider errors in measurement, so it has potential to over-estimate for performance of evaluation equipment. On the other hand, it was represented that the developed method should include variable factor such as errors in measurement and more precise compared to traditional assessment methods.

Uncertainty Analysis of 1 GHz Band Impulse Spectrum Amplitude (1 GHz 대역 임펄스의 스펙트럼 진폭 불확도 평가)

  • Lee, Dong-Joon;Lee, Joo-Gwang;Kwon, Jae-Yong;Kang, Tae-Weon
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.23 no.12
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    • pp.1365-1372
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    • 2012
  • This paper presents a methodology to accurately evaluate the spectral components of impulse signals which are delivered from an impulse generator through the measurement system. The complicated terms for uncertainty measurement of impulse spectrum amplitude and their analysis methods and experimental results are discussed. The expanded uncertainty of the impulse spectrum measurement is 0.015, which is believed to be the best domestic measurement capability and comparable to those of world class.

Development of a Candidate Equipment for Ozone SRP and its Uncertainty Evaluation (오존 SRP 후보 기기의 제작과 측정 불확도 평가)

  • 정규백;이진홍;우진춘
    • Proceedings of the Korea Air Pollution Research Association Conference
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    • 1999.10a
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    • pp.113-114
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    • 1999
  • 일차 오존 표준 분광기(SRP)를 제작하여 오존 측정의 정확성을 확보하고, 이것을 국가 표준으로 이용하여 현장 분석기를 차례로 교정하는 체계(그림 1 참조)를 구축하기 위하여, 먼저 자외선 흡광 광도법을 근간으로 하여 오존 SRP 후보 기기를 제작하였다.(중략)

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A Study on the Effects of Cross-sectional Dimension Change of Brake Pad Specimen on the Uncertainty of the Compressive Strength (제동 패드의 압축강도시편의 단면치수변화가 압축강도 불확도에 미치는 영향 분석)

  • Park, Soo Hong;Park, Jin Kyu;Kim, Si Wan;Park, Chan Kyoung
    • Journal of the Korean Society for Railway
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    • v.17 no.4
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    • pp.223-227
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    • 2014
  • The brake pad is one of the basic brake elements of a railway vehicle. It accomplishes braking action by friction between a pad and a brake disc. Because the brake pad must endure specified high pressure, the compressive strength is managed as the main performance factor. The standards for measuring the compressive strength of brake pads are KRS, KRCS, and KRT. These standards specify the size of the test piece for measuring compressive strength as $20mm{\times}10mm{\times}15mm$ ($W{\times}D{\times}H$). To reduce the uncertainty of the compressive strength, factors of uncertainty were analyzed. The results show that changing the dimensions of the cross section was useful to reduce the uncertainty. The uncertainty due to the new cross-sectional dimension shows the effectiveness of reducing uncertainty.