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A Study on Flash Points and Fire Points of Acids Using Closed Cup and Open-cup Apparatus (밀폐식과 개방식 장치를 이용한 Acid류의 인화점과 연소점에 관한 연구)

  • Ha, Dong-Myeong;Han, Jong-Geun;Lee, Sung-Jin
    • Fire Science and Engineering
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    • v.20 no.3 s.63
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    • pp.29-34
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    • 2006
  • The flash and fire point are the most important combustible properties used to determine the potential for the fire and explosion hazards of flammable material. The flash point is defined as the lowest temperature at which a flammable liquid gives off sufficient vapor to form an ignitable mixture with air near its surface or within a vessel. The fire point is the temperature of the flammable liquid at which there will be flaming combustion, sustained 5 seconds in response to the pilot flame. In this study, the flash points and fire points were measured to present raw data of the flammable risk assessment for acids, using Pensky-Martens Closed Cup(C.C.) apparatus (ASTM-D93) and Tag Open-cup (O.C.) apparatus(ASTM D 1310-86). The measured fire points were compared with the estimated values based on 1.11 times stoichiometric concentration. The values calculated by the proposed equation were in good agreement with measured values.

Continuous PTFE Coating Process on Basalt Sewing Thread (현무암 재봉사의 연속식 테프론 코팅 공정)

  • Lee, Soo
    • Journal of the Korean Applied Science and Technology
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    • v.31 no.2
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    • pp.183-189
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    • 2014
  • On the basis of our previous research results concerning a batch Teflon coating process on the surface of basalt fiber which has superior fire-resistance and chemical resistance, we have tried to set up suitable operating conditions for continuous polytetrafluoroethylene(PTFE) coating process. The basalt fiber was continuously pre-treated with 7.5 wt%(6.5% of DPU) of triethoxytrifluoropropylsilane(TMTFPS) and then coated with 20 wt% of PTFE dispersions containing 0.25 wt% of penetrating agent sodium bis(2-ethylhexyl)sulfo succinate (DOS-Na) to get the highest tensile and loop strengths. After dipping process, the PTFE coated basalt fiber was dried under 2 m drying chamber at $120^{\circ}C$ with 12 m/min of winding speed and consequently sintered under 2 m sintering chamber at $380^{\circ}C$ for 40 s. Conclusively, PTFE coated basalt fiber whose tensile and loop strengths were to $3.4g_f/D$ and $2.3g_f/D$, respectively, applicable to high temperature sewing thread could be continuously prepared with our pilot scale process under optimum conditions.

A Study on Insulation·Fire Proof Materials Using Silica Aerogels (실리카 에어로젤을 이용한 단열·내화재 개발에 관한 연구)

  • Cho, Myung Ho;Hong, Sungchul
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.16 no.10
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    • pp.6816-6822
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    • 2015
  • In this study, silica aerogel-glass wool composites were developed for improvement of thermal conductivity and overcoming the water adsorption of glass wool boards. Silica aerogel-glass wool composites were prepared by glass wool and silica aerogel with liquid binder. Mixtures with binder were composed of CMC (carboxymethyl cellulose) and silica aerogel for glass wool board. Silica aerogel-glass wool composite boards were had $0.065g/cm^3$ density by impregnation silica aerogel where from origin glass wool board at $0.048g/cm^3$ density. Thermal conductivity of silica aerogel-glass wool composites were 0.0315 W/mK (up to 7.4% thermal resistance) and fire penetration time came to 362 seconds (up to 2.7 times stronger than origin glass wool board). In addition, hydrophobic aerogel characteristics prevented the adsorption of water onto silica aerogel-glass wool composite boards that was good for lightweight.

Preparation of Barley Leaf Powder Tea and Its Quality Characteristics (보리잎 분말차의 제조와 그 품질특성)

  • Kim, Dong-Chung;Kim, Dong-Won;Lee, Sung-Dong;In, Man-Jin
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.35 no.6
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    • pp.734-737
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    • 2006
  • This study was carried out to establish the manufacturing process of barley leaf powder tea. The optimal manufacturing process among many trials was determined with sensory evaluation. Finally established process and operation conditions were as follows: pretreatment (cutting and washing), steaming ($100^{\circ}C$, 30 sec), primary drying and roasting ($130^{\circ}C$, 40 min), rolling (RT, 25 min), middle drying and roasting ($60^{\circ}C$, 30 min), final drying and roasting ($55^{\circ}C$, 25 min), drying ($60^{\circ}C$, 20 min), roasting ($85^{\circ}C$, 20 min), and powdering (120 mesh). The barley leaf powder tea produced by this process mainly consisted of dietary fiber (33.8%), amino acids (12.9%), minerals (4.7%) and ${\beta}-carotene$ (6.9 mg%).

Behavioral Characteristics Following Lesions of the Nucleus Accumbens Septi in Rats (측좌각의 부위별 파괴가 행동에 미치는 영향)

  • Lee, Soon-Chul
    • The Korean Journal of Pharmacology
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    • v.21 no.2
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    • pp.111-118
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    • 1985
  • Caudal, rostral and both areas of the nucleus accumbens septi (NAB) were lesioned each in separate animal group by applying DC of 3.0 mA for 15 sec. in order to examine if any regional differences in the NAB with regard to the manifestation of locomotor activity, The r-NAB and cr-NAB-lesioned rats were significantly increased in locomotor activity but not in the c-NAB-lesioned rats and the effect following the NAB lesion was immediately produced and returned to control levels in about 7 days postoperatively. On the other hand, the locomotor stimulation produced by methamphetamine was significantly attenuated in all NAB-lesioned rats but also stereotyped behavior was significantly elicited simultaneously. These results thus suggested that NAB may be attributed to the inhibitory role in the locomotor activity, of which intensity differs from rostral site and caudal site, and stereotyped behavior may be shown higher sensitivity of the denervated striatal dopamine function.

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뇌로의 약물송달(2) -혈액-뇌관문(BBB)의 Osmotic Opening법에 의한 뇌로의 약물송달

  • 황만용;박경호;손영택;이민화
    • Proceedings of the Korean Society of Applied Pharmacology
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    • 1993.04a
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    • pp.177-177
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    • 1993
  • 뇌모세혈관내피세포로 구성된 혈액-뇌관문(BBB)은 tight junction으로 구성되어 있을뿐만 아니라 fenestra가 없는 등 BBB가 가진 특성으로 인해 물질 수송에 장벽역할을 하기 때문에 주로 중추신경계 질환시의 약물요법에 많은 제한이 따른다. 따라서 뇌로의 효율적인 약물 송달방법에 대해 많은 연구가 진행중에 있는데 본 연구에서는 BBB의 hyperosmotic opening법을 이용하여 뇌로 잘 수송되지 않는 약물의 뇌송달 방법에 대해 연구하고자 하였다. 먼저 수용성으로 인해 BBB 에 잘 통과하지 않는 물질로 신장 및 뇌영상 촬영시 사용되는 방사성 의약품이 Tc-DTPA를 이용하여, hyperosmotic opening법에 의한 뇌투과 증가정도를 검토하였으며, 실험방법이 확립됨에 따라 뇌암의 항암요법을 위해 뇌로의 투과가 적은 항암제(5-Fluorouracil, 5-FU)의 뇌송달에 대해 본 방법을 적용하여 검토하였다. 실험동물로는 S.D.계 웅성 랫트를 사용하였으며, 실험방법은 다음과 같이 하였다. 랫트의 좌측 외경동맥(left external carotid artery)에 혈류의 역방향으로 혈관 분지점에서 1-2mm 전까지 PE-50 catheter를 삽입하고, 1.6 molal L-(+)- arabinose 고장액(1580mOsm)을 0.12ml/sec의 일정한 속도로 30초간 infusion함으로 BBB를 opening 한 다음, 5분 후에 Tc-DTPA를 대퇴 정맥으로 주사하여 0, 10, 30초, 1, 1.5, 2, 3, 4, 5, 7 및 10분 간격으로 대퇴동맥에 설치한 카테타로부터 혈액을 채취하고 마지막 혈액을 취한 후 즉시 단두하여 뇌를 적출하였다. 채취한 뇌를 액체질소에 담근 후 tissue Tek으로 고정하고 autoradiography를 하기 위한 slice와 농도측정을 위해 필요한 부위를 취한 후 감마카운터로 Tc-DTPA의 brain각 부위별 및 혈장농도를 측정하였다. 뇌조직중 혈액부피의 측정은 Tc-albumin를 이용하여 구하였다. 같은 방법으로 5-FU에 대한 실험도 행하였고, 이때 각 혈장 및 조직중의 5-FU함량은 HPLC로 하였다.

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Submerged Type Water Purification System using Hollow Fiber Microfiltration Membrane (중공사 정밀여과막을 이용한 상수처리용 일체형 시스템 개발)

  • Jeong, Gyu-Yeong;Kim, Hyeong-Su;Im, Jong-Seong
    • Journal of Korea Water Resources Association
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    • v.32 no.3
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    • pp.311-319
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    • 1999
  • Membrane separation process is considered as an alternative of conventional water purification system using coagulationㆍsedimentation+sand filtration. In this study, it was examined that the application possibility of Hollowfiber Microfiltration membrane for water purification process. A $20m^3/day$ scale pilot plant was used for studying the possibility of long-term operation and the stability of water quality under the optimum conditions, 0.03m/h permeate flux, filtration for 10 minutes, pause for 2 minutes(including air-scrubbing for 30 seconds), obtained by lab-scale experiment. As a result, it was proved stability of pilot plant over one year and filtrate quality(Turbidity. SS etc). Therefore, it was proved that membrane separation process using Hollowfiber Microfiltration membrane can be applied for water purification system

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The Study of Formation of Ti-silicide deposited with Composite Target [II] (Composite Target으로 증착된 Ti-silicide의 현성에 관한 연구[II])

  • Choi, Jin-Seog;Paek, Su-Hyon;Song, Young-Sik;Sim, Tae-Un;Lee, Jong-Gil
    • Korean Journal of Materials Research
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    • v.1 no.4
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    • pp.191-197
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    • 1991
  • The surface roughnesses of titanium silicide films and the diffusion behaviours of dopants in single crystal and polycrystalline silicon substrates durng titanium silicide formation by rapid thermal annealing(RTA) of sputter deposited Ti-filicide film from the composite $TiSi_{2.6}$ target were investigated by the secondary ion mass spectrometry(SIMS), a four-point probe, X-ray diffraction, and surface roughness measurements. The as-deposited films were amorphous but film prepared on single silicon substrate crystallized to the orthorhombic $TiSi_2$(C54 structure) upon rapid thermal annealing(RTA) at $800^{\circ}C$ for 20sec. There was no significant out-diffusion of dopants from both single crystal and polycrystalline silicon substrate into titanum silicide layers during annealing. Most of the implanted dopants piled up near the titanium silicide/silicon interface. The surface roughnesses of titanium silicide films were in the range between 16 and 22nm.

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Variations in electrical properties and interface reactions of $Ta_{2}O_{5}-Si$ by RTA post annealing (RTA 후속 열처리에 의한 $Ta_{2}O_{5}-Si$ 계면 반응과 전기적 특성 변화)

  • Jeon, Seok-Ryong;Lee, Jeong-Yeop;Han, Seong-Uk;Park, Jong-Wan
    • Korean Journal of Materials Research
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    • v.5 no.3
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    • pp.357-363
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    • 1995
  • PECVD(Plasma-enhanced Chemical Vapor Deposition)법을 이용하여 증착한 $Ta_{2}$O_{5}$ 박막의 전기적 특성과 미세구조에 미치는 RTA(Rapid Thermal annealing) 후속 고온 열처리의 영향을 조사하였다. $Ta_{2}$O_{5}$ 박막의 미세구조와 interface 거동을 관찰하기 위하여XRD(X-ray Diffractometer), TEM(Transmission Electron Microscope), AES(Auger Electron Spectroscope) 분석을 실시하였으며, 전기적 특성을 관찰하기 위하여 I-V, C-V 측정을 하였다. $600^{\circ}C$에서 60초간 열처리를 실시하였을 경우 가장 우수한 유전 특성 및 누설 전류 특성을 보였으며, 유전 상수는 26이었고 누설 전류는 5 $\times$ $10^{-11}$A/$cm^{2}$이었다. $600^{\circ}C$ 이상의 온도에서 행한 열처리에 의하여 박막의 누설 전류와 유전 특성은 복합적으로 영향을 받았음을 알 수 있었다. 이는 $600^{\circ}C$의 열처리에서 이루어지고있는 박막의 결함감소와 고밀화 현상과 함께 80$0^{\circ}C$ 이상의 열처리에서 발생하는 조밀육방정 결정 구조를 가지는 $\delta$-$Ta_{2}$O_{5}$의 결정화에 기인함을 알 수 있었다. 또한 TEM과 AES분석 결과로부터 이들 박막의 누설 전류와 유전상수의 변화는 열처리에 의하여 일어나는 Ta-O-Si transition층의 생성과 성장에 기인함을 알 수 있었다. 따라서 $Ta_{2}$O_{5}$ 박막의 전기적 특성의 변화는 RTA 후속 열처리에 따른 계면 반응과 결정화 그리고 박막의 조밀화에 그 영향이 있음을 알 수 있었다.

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Effects of Some Organic Acids on Shelf Life and Textural Properties of Cooked Noodle (유기산이 숙면의 저장성 및 물성에 미치는 영향)

  • Cha, Wook-Jin;Kim, Kong-Hwan
    • Applied Biological Chemistry
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    • v.41 no.2
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    • pp.166-174
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    • 1998
  • The effects of some organic acids on the shelf life of cooked noodle and the change in textural properties were studied. Organic acids used were vinegar, lactic, citric and malic acid. The pH of noodle was adjusted to $4.7{\pm}0.25$ by dipping it in each solution for 30 seconds. Total microbial count and turbidity of the treated samples were measured storage for 4 days at $15^{\circ}C$. The total count was high in order of control, malic, citric, lactic acid and vinegar. High turbidity was observed in order of control, lactic, malic, citric acid and vinegar. Hardness, adhesiveness, cohesivenes and springiness were measured for 30 days at $35^{\circ}C$ using Rheometer along with concurrent sensory evaluation. The acid treated samples showed higher values in hardness and cohesiveness than control but lower in adhesiveness and springiness. After 30 days storage, the malic or citric acid treated sample led to a somewhat higher gumminess than control. Based on the sensory evaluation the malic acid treated noodle significantly exhibited the highest score followed by citric, lactic acid, control and vinegar.

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