• Title/Summary/Keyword: 접착식

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COMPARATIVE ENAMEL BOND STRENGTH BETWEEN LIGHT-AND DUAL-CURED COMPOSITES BONDED BY SELF-ETCHING ADHESIVES (자가 산부식 접착제로 접착된 광중합과 이원중합 복합레진의 법랑질 결합강도 비교)

  • Cho, Young-Gon;Yoo, Sang-Hoon
    • Restorative Dentistry and Endodontics
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    • v.32 no.1
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    • pp.1-8
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    • 2007
  • This study compared the microshear bond strength (${\mu}SBS$) of light-cured and dual-cured composites to enamel bonded with three self-etching adhesives. Crown segments of extracted human molars were cut mesiodistally, and 1 mm thickness of specimen was made. They were assigned to three groups by used adhesives: Xeno group (Xeno III), Adper group (Adper Prompt L-Pop), and AQ group (AQ Bond). Each adhesive was applied to cut enamel surface as per manufacturer's instruction. Light-cured (Filtek Z 250) or dual-cured composite (Luxacore) was bonded to enamel of each specimen using Tygon tube. After storage in distilled water for 24 hours, the bonded specimens were subjected to ${\mu}SBS$ testing with a crosshead speed of 1 mm/minute. The mean ${\mu}SBS$ (n = 20 for each group) was statistically compared using two-way ANOVA, Tukey HSD, and t test at the 0.05 probability level, The results of this study were as follows ; 1. The ${\mu}SBS$ of light-cured composite was significantly higher than that of dual-cured composite when same adhesive was applied to enamel. 2. For Z 250, the ${\mu}SBS$ of AQ group ($9.95{\pm}2.51 MPa$) to enamel was significantly higher than that of Adper soup ($6.74{\pm}1.80 MPa$), but not significantly different with Xeno group ($7.73{\pm}2.01 MPa$). 3. For Luxacore, the ${\mu}SBS$ of Xeno group ($5.19{\pm}1.32\;MPa$) to enamel was significantly higher than that of Adper group ($3.41{\pm}1.19\;MPa$), but not significantly different with AQ group ($4.50{\pm}0.96\;MPa$).

Effects of Item Packaging Methods on the Quality Characteristics of Yukwa during Storage (단위포장 방법에 따른 유과의 저장 중 품질 특성)

  • Jang, Min Jun;Lee, Keun Taik
    • Food Science and Preservation
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    • v.20 no.2
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    • pp.158-165
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    • 2013
  • This study aimed at investigating the quality changes of Yukwa during storage using the various item packaging methods present in the domestic market. The samples consisted of a self-adhesive-oriented polypropylene (OPP) film pouch (P1), a heat-sealed OPP film pouch (P2), and a polystyrene (PS) tray with a polyethylene terephthalate (PET) lid (P3). These were stored at $25^{\circ}C$ up to eight weeks. Throughout the storage period, the acid values of all the study samples remained under the Korean hygiene regulation limit of 2.0 mg KOH/g. The P2 samples showed both the slowest decrease in water content and the slowest increase in hardness value during storage. Sensory evaluation also showed that the P2 samples were the only ones that maintained their market value of 5.0 throughout the eight-week assessment period.

Mechanical Properties of Polypropylene/Talc Composites Prepared via Solid-State Extrusion (고상 압출된 폴리프로필렌/탈크 복합재료의 기계적 물성)

  • Lee, Jaechoon;Ha, Chang-Sik
    • Journal of Adhesion and Interface
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    • v.17 no.4
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    • pp.131-135
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    • 2016
  • We investigated the specific gravity and mechanical property changes of solid-state extruded polypropylene (PP)/talc composites before and after orientation. The specific gravity of the composites increases with increasing the filler contents. The specific gravity of the oriented specimen containing filler in PP matrix is found to be much smaller than that of pre-specimen due to the formation of more micro-voids. It was found that the tensile properties of the composites are increased up to the talc content of 10 wt%, but after the contents exceeding 10 wt%, the tensile properties are decreased. For oriented specimens, the tensile strength of the composites showed monotonously decrease with increasing talc contents. When the contents of talc is 10 wt%, the theoretical values according to Halpin-Tsai equation are close to the experimental values but over 20 wt% of talc contents, the deviation of the experimental values from the theoretical prediction becomes higher. The maximum flexural strength and modulus were observed for PP/talc composites when the talc contents was 10 wt% for both pre-specimen and oriented specimen.

Study on the Experimental Aging Estimation Technique for HTPB based Solid Propellant Considering Post Curing Effect (후경화를 고려한 HTPB 고체 추진제의 실험적 노화평가 기법 연구)

  • Jung, Gyoo Dong;Park, Jae Beom;Kim, Shinhoe
    • Journal of the Korean Society of Propulsion Engineers
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    • v.23 no.3
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    • pp.51-57
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    • 2019
  • Post curing effects are estimated by specimen tests. Propellant specimen accelerated aging tests are performed when post curing is estimated to be complete and the coefficients of Arrhenius aging equations are acquired. Simulated motors with cylindrical grain are designed and fabricated to confirm the application. Accelerated aging tests are conducted, and aged properties are measured and estimated for the inner bore, center and bond parts of the grain. The measured aging ratios of the modulus are compared with the ones predicted by the equations. As the results, the accelerated aging equations predict well the propellant aging trends; however, some differences are observed at the bond part. Therefore, the specimen extraction part must be carefully chosen to suit the test purpose when a rocket motor grain is used for the aging test.

Comparison of adhesive strength of resinous teeth splinting materials according to enamel surface treatment (법랑질 표면 처리방법에 따른 레진계 치아 고정재료의 접착강도 비교)

  • Lee, Ye-Rim;Kim, Soo-Yeon;Kim, Jin-Woo;Park, Se-Hee;Cho, Kyung-Mo
    • Journal of Dental Rehabilitation and Applied Science
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    • v.35 no.2
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    • pp.72-80
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    • 2019
  • Purpose: The purpose of this study is to compare and analyze the shear bond strength and fracture pattern in different enamel tooth surface treatments for resin splinting materials. Materials and Methods: G-FIX and LightFix were used as tooth splinting materials. Twenty bovine mandibular incisors were used for the preparation of the specimens. The exposed enamel surface was separated into four parts. Each tooth was treated with 37% phosphoric acid, 37% phosphoric acid + adhesive resin, 37% phosphoric acid + G-premio bond, and G-premio bond for each fraction. Shear bond strength was measured using a universal testing machine. After measuring the shear bond strength, the fractured surface of the specimen was magnified with a microscope to observe the fracture pattern. Two-way ANOVA was used to verify the interaction between the material and the surface treatment method. One-way ANOVA was used for comparison between the surface treatment methods of each material and post-hoc test was conducted with Scheffe's test. An independent t-test was conducted to compare shear bond strengths between materials in each surface treatment method. All statistics were conducted at 95% significance level. Results: G-FIX, a tooth splinting resin, showed similar shear bonding strength when additional adhesive resins were used when material was applied after only acid etching, and LightFix showed the highest shear bonding strength when additional adhesive resins were used after the acid etching. In addition, both G-FIX and LightFix showed the lowest shear bond strength when only self-etching adhesive was applied without additional acid etching. Verification of interactions observed interconnection between resins and surface treatment methods. Most of the mixed failure was observed in all counties. Conclusion: When using G-FIX and LightFix, which are tooth-splinting materials, it is considered that sufficient adhesion will be achieved even after applying only acid etching as instructed by the manufacturer.

THE EFFECT OF THERMOCYCLING ON THE DURABILITY OF DENTIN ADHESIVE SYSTEMS (열순환이 상아질 접착제의 결합 내구성에 미치는 영향)

  • Moon, Young-Hoon;Kim, Jong-Ryul;Choi, Kyung-Kyu;Park, Sang-Jin
    • Restorative Dentistry and Endodontics
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    • v.32 no.3
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    • pp.222-235
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    • 2007
  • The objectives of this study was to evaluate the effect of thermocycling on the ${\mu}TBS$ (microtensile bond strength) to dentin with four different adhesive systems to examine the bonding durability. Freshly extracted $3^{rd}$ molar teeth were exposed occlusal dentin surfaces, and randomly distributed into 8 adhesive groups 3-steps total-etching (Scotchbond Multi-Purpose Plus; SM, All Bond-2; AB), 2-steps total-etching (Single Bond; SB, One Step plus; OS), 2-steps self-etching (Clearfil SE Bond; SE, AdheSE AD) and single-step self-etching systems (Promp L-Pop; PL, Xeno III; XE) Each adhesive system in 8 adhesives groups was applied on prepared dentin surface as an instruction and resin composite (Z250) was placed incrementally and light-cured. The bonded specimens were sectioned with low-speed diamond saw to obtain $1\times1mm$ sticks after 24 hours of storage at $37^{\circ}C$ distilled water and proceeded thermocycling at the pre-determined cycles of 0, 1,000 and 2,000. The ${\mu}TBS$ test was carried out with EZ-tester at 1mm/min. The results of bond strength test were statistically analyzed using one-way ANOVA/ Duncan's test at the a < 0.05 confidence level. Also, the fracture mode of debonded surface and the interface were examined under SEM. The results of this study were as follows ; 1. 3-step total etching adhesives showed stable, but bond strength of 2-step adhesives were decreased as thermocycling stress. 2. SE showed the highest bond strength, but single step adhesives (PL, XE) had the lowest value both before and after thermocycling. 3 Most of adhesives showed adhesive failure. The total-etching systems were prone to adhesive failure and the single-step systems were mixed failure after thermocycling. Within limited results of this study, the bond strength of adhesive system was material specific and the bonding durability was affected by the bonding step/ procedure of adhesive Simplified bonding procedures do not necessarily imply improved bonding performance.

Effect of Different Types of Bonding Agent and Application Methods on Shear Bond Strength of Orthodontic Bracket (Bonding agent의 종류 및 적용 방법에 따른 교정용 브라켓의 전단결합강도에 관한 연구)

  • Lee, Jaehee;Kim, Jongsoo
    • Journal of the korean academy of Pediatric Dentistry
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    • v.44 no.4
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    • pp.419-426
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    • 2017
  • Attachment of the orthodontic bracket conducted during the window opening procedure can result in failure due to various adverse conditions such as blood or saliva contamination, or other wet conditions. For the success of the bracket attachment, reduction of total operation time is crucial. The purpose of this literature is to evaluate the differences between the final resultant shear bond strength of the conventional method of using phosphoric acid and self-etching primer, and that of the operation time-reduced method in which the curing step is omitted subsequent to the primer application. A total of 40 human maxillary incisors were prepared. Group I(control group) and II were etched with 37% phosphoric acid and Group III and IV were conditioned with self-etching primer. Attachment of the group I and III was conducted by manufacturer's instructions. The operation time of Group II and IV was reduced by eliminating the curing step after the primer application. The resultant shear bond strength of each group was measured and an adhesive remnant index (ARI) was recorded. The mean shear bond strength of group I, II, III, and IV were 14.16 MPa, 8.33 MPa, 8.29 MPa, and 6.48 MPa respectively. Significant differences could only be found between the control group and the experimental groups (p < 0.05). The ARI indicated no significant difference among all groups.

INFLUENCE OF MULTIPLE ADHESIVE COATINGS ON THE SHEAR BONDING STRENGTH OF COMPOSITE RESIN (접착제의 다층적용이 복합레진의 전단결합강도에 미치는 영향)

  • Park, Heon-Dong;Lee, Chang-Seop;Lee, Sang-Ho;Lee, Nan-Young
    • Journal of the korean academy of Pediatric Dentistry
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    • v.33 no.3
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    • pp.377-387
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    • 2006
  • The objective of this study was to evaluate the influence of multiple adhesive coatings on the thickness of hybrid and adhesive layer and shear bond strength(SBS) of self-etch adhesives and self-etch primer adhesives. The buccal or lingual crown dentin of extracted human molars was used. Self-etch adhesives or self-etch primer adhesives were applied 1, 2 and 3 times on the dentin before light curing. In another group adhesives were reapplied after light curing first layer. Treated surfaces were prepared to measure the thickness of hybrid and adhesive layer with SEM, and shear bond strength to dentin using an Instron machine. The following results were obtained : 1. The adhesive layers increased with the number of coatings(p<0.05) with all adhesives. Adpor Prompt L-Pop and Xeno III were significantly thinner than self-etch primer adhesives (p<0.05). 2. The thickness of hybrid layers increased with the number of coatings (p<0.05). 3. The shear bonding strength of Unifil Bond and Clearfill SE Bond were higher than Scotchbond Multipurpose Plus and Adpor Prompt L-Pop (p<0.05), and similar with Xeno III. 4. The shear bond strength increased significantly with the number of coatings in Adpor Prompt L-Pop(p<0.05), but decreased at 3 times in AdheSE Bond(p>0.05). 5. In Adpor Prompt L-Pop and Xeno III, the shear bond strength decreased when adhesives were reapplied after curing the first adhesive layer.

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A study on the modeling of axis-direction belt movement in the 3 cylinders-belt system (3 cylinders-belt system에서의 축방향 belt운동 modeling에 관한 연구)

  • Heo, Yu;Hong, Seung-Kwan
    • Proceedings of the Korean Fiber Society Conference
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    • 2002.04a
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    • pp.69-72
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    • 2002
  • 섬유산업은 fiber로부터 시작하여 yarn, fabric을 거쳐 최종 섬유제품인 clothing을 생산하는 긴 stream을 가지고 있으며, 이와 같이 여러 단계의 공정을 거치는 가운데 섬유물은 새로운 형태를 가지게 되며 부가가치가 형성된다. 특히 garments manufacturing 공정에는 fusing press기가 사용되는데 이 방식은 같은 각속도와 지름을 가진 cylinder로 구동되는 두 개의 상하 벨트구동기구와 내부에 열전식 heather로 구성되어 상하 벨트의 내부로 원단과 심지를 통과시키며 열을 가함으로써 원단과 심지를 접착시킨다. (중략)

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차분법에 의한 복합 박판에서의 비선형 응력 해석

  • 현혜정;김치경
    • Proceedings of the Korean Institute of Industrial Safety Conference
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    • 2000.11a
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    • pp.429-434
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    • 2000
  • 본 연구에서는 등분포하중을 받는 laminated 박판의 거동해석을 제시하였다. 접착한 두 박판의 비선형 지배방정식을 Von Karman 식을 이용하여 유도하고 박판의 거동을 차분법을 이용하여 수치해석 한다. Interlayer에서의 전단변형을 고려하여 지배방정식에 포함시켜 하중 증분법(load incremental method)으로 기하학 비선형 해석을 수행한다. 하중 증분법에 따른 반복법을 도입하여 비선형 방정식을 해석했다. 해석방법의 타당성을 입증하기 위하여 해석결과들을 기존의 문헌의 결과와 비교, 검토함으로써 본 논문에서 제시한 이론 및 해석방법의 타당성을 입증한다. 차분법의 하중 증분법 알고리즘을 개발하여 예제문제에 대한 수치해석 결과들을 논하였다.(중략)

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