• Korean Journal of Materials Research
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• v.5 no.4
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• pp.405-411
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• 1995

급냉응고된 Al-3.51wt%Li-0.34wt%Zr 합금의 시효거동을 시차주사열량계(DSC)에 의한 열분석 방법으로 조사하였다. DSC에 의한 비열측정 결과 $\delta$’의 석출에 의한 발열반응과 $\delta$, $\beta$ 및 복합석출상의 석출에 의한 발열반응을 확인하였으며 $\delta$’ 및 $\delta$의 재고용에 의한 2개의 흡열반응을 확인하였다. 7$0^{\circ}C$ 저온시효시 $\delta$’의 석출에 의한 발열반응 이전에 흡열반응이 나타났으며 이것은 $\delta$’ 석출 이전에 $\delta$’ 전구생성물이 형성되었음을 의미한다. DSC 곡선상에 나타난 발열과 흡열곡선을 해석하여 얻은 $\delta$’상 석출과 재고용의 활성화에너지값은 각각 83KJ/mol과 98KJ/mol로서 Al-Li 2원계 및 Al-Li-Mg에 비해 높은 값을 나타내엇으며, 시효에 의한 강화가 일어나 DSC에 의한 비열변화 조사결과 나타난 $\delta$’상 석출 완료 시효조건점 (21$0^{\circ}C$, 1시간)에서 최고경도값(Hv 160)을 나타내었다.

• Journal of the Society of Disaster Information
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• v.10 no.1
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• pp.71-83
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• 2014

This study carried out an experiment in order to compare thermal characteristics after collecting dust generated in the process of disposing of waste tire, plywood flour in the process of manufacturing plywood, salicylic acid dust in the process of manufacturing functional soap, and dust in the process of manufacturing wheat powder, which has potential fire and explosion hazard. According to the results of experiment, the analysis showed that all samples subject to the experiment were in the condition where heat flux decreased and temperature decreased as the quantity of added talc was increased. This shows that decomposition rate decreased, and hazard decreased. However, in all of samples subject to the experiment, as heating rate increased, endothermic onset temperature moved to the low-temperature part, and the amount of absorbed heat was largely increased. This showed that the decomposition hazard of sample increased as heating rate increased, according to the analysis. Besides, TGA experiment results showed that thermal stability was secured because total weight loss decreased as the amount of talc was increased for all samples subject to the experiment regarding the ratio of weight loss. It is expected that the continuous research and supplementation of dust explosion mechanism in the future will contribute to the establishment of measures for the effective dust explosion prevention.

• Journal of Korean Society of Steel Construction
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• v.12 no.6
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• pp.759-767
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• 2000

In this study, the time dependent internal stress changes of a Concrete Filled Steel Tube(CFT) column during a fire test were quantitatively analyzed. The strain ratio of a CFT column on the different loads was measured by tensile strength tests in terms of yield strength, tensile strength average extensibility and elasticity modulus. To understand the internal material properties change of concrete in CFT column damaged due to a fire, the compressive strength and elastic modulus tests were measured on a core sample from the center of the steel tube after the fire test. The elastic modulus test measured the strain from the stress. To determine the fire temperature of the test material, a differential thermal analysis was done. From the tested result, the gained data were conducted and an analysis method was suggested. The purpose of this work is to suggest a basic data for structure regulation enactments of the internal fire design of CFT.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2023.05a
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• pp.317-318
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• 2023

This study is part of the carbonation degree DB accumulation through quantitative analysis of carbonation depth, Ca(OH)₂ and CO₂ according to the type of finish and years of use of old concrete structures in order to predict the amount of CO₂ that can be absorbed through carbonation of concrete. To this end, the depth of carbonation of the concrete core specimen is measured using an indicator, and the dry amount of water combined with CO₂ in the sample is measured using a differential thermal gravimetric analyzer for samples in the carbonation area and non-carbonated area classified by the indicator, and the absorption compared to the weight of the sample. The amount of absorbed CO₂ was calculated. In addition, the degree of carbonation was calculated through quantitative comparison of Ca(OH)₂ in the carbonation section and non-carbonation section. In the future, we will continue to add the survey and analysis data of dismantled structures and use them as basic data for estimating the amount of carbon dioxide that can be absorbed according to the exposure conditions and years of use by concrete mix.

• The Korean Journal of Applied Statistics
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• v.37 no.3
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• pp.297-309
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• 2024

This paper evaluates the performance of the neural network autoregressive model combined with an exponential smoothing model, called the NNARX+ETS model. The combined model utilizes the components of ETS as exogenous variables for NNARX, to forecast time series data using artificial neural networks. The main idea is to enhance the performance of NNAR using only lags of the original time series data, by combining traditional time series analysis methods with the neural networks through NNARX. We employ two real data for performance evaluation and compare the NNARX+ETS with NNAR and traditional time series analysis methods such as ETS and ARIMA (autoregressive integrated moving average) models.

• Journal of Sericultural and Entomological Science
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• v.44 no.2
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• pp.82-86
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• 2002

Silk sericin powder was prepared by mechanical treatment from culled-cocoon extract of Bombyx mori silkworm. The physical and structural characteristics of sericin powder were investigated by instrumental analysis. The solubility of sericin powder was decreased nearly half of sericin lyophilized. Amino acid analysis showed that arginine content was decreased from 3.72% to 0.03∼0.07%. XRD showed that molecules of sericin were somewhat regularly arranged by mechanical treatment. On the other hand, FT-IR showed the molecular vibration of silk sericin was not induced by mechanical treatment. Thermal properties also did not changed.

• Journal of the Korea institute for structural maintenance and inspection
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• v.17 no.2
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• pp.94-100
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• 2013

In this paper, Machinery analysis was conducted, in order to predict highest exposure temperatures and the analyze fire damage in the case of fire on reinforced concrete structure. After analyzing differential thermal of reference materials in accordance with temperature of concrete reference core specimen, it turned out that powerful endothermic peak came resulting from evaporation of capillary water and get water untill $200^{\circ}C$, another endothermic peak came resulting from decomposition of calcium hydroxide at $520^{\circ}C$, and then mass of reference materials remarkably decreased due to endothermic reaction. Another powerful endothermic reaction came after decomposition of calcite at $720^{\circ}C$. After analyzing X-ray diffraction of reference materials in accordance with temperature of concrete reference core specimen, it turned out that calcium hydroxide existed until the temperature of $400^{\circ}C$, but CH almost disappeared and CaO appeared from $600^{\circ}C$. The production increased in proportion to the temperature. This is because that calcium hydroxide and calcite are decomposed and CaO is produced when the temperature of concrete increases with fire. It is estimated that calcium hydroxide and calcite are utterly decomposed and peak disappears, and peak of CaO is remarkably formed instead, at the temperature of $700-800^{\circ}C$.

• Journal of the Korean Society of Propulsion Engineers
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• v.19 no.5
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• pp.15-21
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• 2015

The thermal decomposition characteristics of the ZPP(Zirconium/Potassium perchlorate), widely used as a primary charge of initiators, were investigated by differential scanning calorimetry(DSC). The DSC results with different heating rates were elaborated with AKTS-Thermokinetics software for the determination of the kinetic parameters of the thermal decomposition of ZPP. There was good agreement between the experimental and the simulation curves, based on the determined kinetic parameters, which indicates the validity of the kinetic description of the thermal decomposition process of ZPP.

• Electrical & Electronic Materials
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• v.9 no.5
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• pp.450-454
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• 1996

Maxwell-Displacement-Current(MDC) measuring technique has been applied to the study of monolayers of Dilauroylphosphatidylcholine (L-.alpha.-DLPC) and Dimyristoylphosphatidylcholine (L-.alpha.-DMPC). The displacement current was generated from monolayers on a water surface by monolayer compression. Displacement current was generated when the area per molecule was about 250.angs.$^{2}$, 280.angs.$^{2}$. Displacement current was generated in the gas state, gas/liquid state, and liquid state in the course of monolayer compression. The orientational change of molecules in monolayers was discussed on the basis of the MDCs obtained. Finally, we measured differential thermal analysis of sample.

• Journal of Sericultural and Entomological Science
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• v.46 no.1
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• pp.28-31
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• 2004

Bombyx mori silk fibroin/hyaluronic acid blend films were prepared by mixing aqueous solution of B. mori silk fibroin and hyaluronic acid. According to the FTIR spectra, no interaction between silk fibroin and hyaluronic acid was found. The conformation of silk fibroin in blend films was changed from random coil to $\beta$-sheet structure by treatment of EDC ethanol solution. Thermal degradation peak of silk fibroin and hyaluronic acid was also not altered by blending each other. The average swelling ratio of silk fibroin/hyaluronic acid blend films was 70. Therefore, silk fibroin/hyaluronic acid blend films might be one of possible wound dressing materials.