• Proceedings of the Korean Vacuum Society Conference
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• 2015.08a
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• pp.176.2-176.2
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• 2015

기존의 트라이볼로지 분석 기법은 macro 영역에서 시료의 강도 및 탄성 등의 물성을 분석하는 정도였으나 Nano-Indenter 분석 기법은 macro 영역보다 더 미세한 nano 영역에서의 시료 물성 분석을 가능하게 해주었다. 따라서 본 연구에서는 시료들의 결정 배양 방향에 따른 Nano-Indenter 압입 각도 차이에 대한 nano 영역에서의 연구를 진행하였다. Si 기판 외에 본 연구에 사용 된 HfN 및 Zr 박막의 시료들은 rf magnetron sputter를 이용하여 약 100 nm 두께로 증착하였다. 각각 시료들에 대한 결정성 확인을 위해 XRD 분석을 실시하였다. 이후 Nano-Indenter를 이용하여 압입 인가력 대비 압입 깊이를 측정하였다. 이 과정에서 Nano-Indenter 압입 각도를 $0^{\circ}$와 $90^{\circ}$로 변화함에 따라 압입 인가력 - 압입 깊이 그래프의 차이를 확인하였고 이를 기준점으로 부터 $10{\mu}m$ 이격시켜 16회 반복 측정과 Weilbull distribution을 통해 신뢰도를 향상시켰다. 측정 결과 Zirconium(Zr) 박막의 경우 21.53 GPa과 22.18 GPa 측정되었으나 Si 기판은 17.46 GPa 16.33 GPa으로, 그리고 HfN 박막의 경우 25.18 GPa과 27.75 GPa으로 상대적으로 큰 차이를 확인하였다. Si 기판과 HfN의 측정결과 Weibull distribution는 75.02와 70.23인 반면 Zr 박막은 30.94로 상대적으로 불균일한 특성을 확인하였다. 이 결과들로부터 각각의 박막 결정 배양 방향에 따른 분석의 한가지 방법으로 Nano-Indenter 분석 기법을 사용할 수 있는 가능성을 확인하였다.

• Journal of the Korean GEO-environmental Society
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• v.16 no.11
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• pp.29-37
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• 2015

Non-excavation method is needed to secure the stability of existing structures during construction. Therefore, prediction of ground settlement is essential. Causes of settlement when using steel pipe indentation method are leading pipe-steel pipe gap, excessive excavation and soil-steel pipe friction etc. Also they are similar to the causes of settlement when using Shield TBM during construction. In this study, ground settlement during steel pipe indentation is predicted by the Gap Parameter Method and Volume Loss Method which are kinds of Shield TBM prediction Method. and compared with those of prediction methods by conducting field test. As a result, Volume Loss Prediction Method is the most similar to the field tests. However, It is needed to additional studies, such as decision of the factors and adaptability for total settlement predictions of non-excavation method.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.31 no.9
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• pp.26-31
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• 2003

Aging aircraft accumulates widespread fatigue damage commonly referred to as multiple site damage(MSO). For ductile material such as 2024-T3 aluminum, MSO may lower the service life below that which is predicted by conventional fracture mechanics. The present paper is concerned with the fatigue life extension by pre-indentation technique for thin 2024-T3 aluminum plate to decelerate the crack propagation rate in the panels with MSO. The panel with fastener holes can be simply modelled by Hole/Slot type Middle-Tension specimen. Results of fatigue testing show significantly improving failure cycles from 10 to 40 times. This retardation effect is decreased by increasing the loading level in the constant amplitude loading. In the sense of retardation mechanism, the crack propagation rate is gradually attenuated by entering the indentation mark and maintains at the lowest value for a long period after the edge of crack passes the center of indentation area.

• Journal of the Korean Ceramic Society
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• v.33 no.3
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• pp.339-347
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• 1996

Mechanical properties(flexural strength hardness fracture toughness) of alumina ceramics were evaluated. Alumina products of four companies were selected and three of those were made in Korea and one of those was made in Japan. The large differences according to manufacturing companies had resulted from flexural strength and weibull modulus which had a wide ranges of 300 to 400 MPa and 5 to 15 respectively. Critical indenstation load which could be neglected the effect of elastic recovery was about 9.8N and Vickers' hardness were about 15 GPa. Fracture toughnesses were evaluated by IF and ISB method. It was more preferable to the average at one indentation load that fracture toughness were obtained from the slope of the relationship between indentation load and crack length in IF method and between indentation load and fracture load in ISB method and fracture toughness was about 4 MPa·m1/2.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.36 no.2
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• pp.117-123
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• 2012

This paper discusses two different techniques used to measure the mechanical properties of thin films: the bulge test and the nanoindentation test. In the bulge test, a uniform pressure is applied to one side of the film. Measurement of the membrane deflection as a function of the applied pressure allows one to determine the mechanical properties such as Young's modulus, and the residual stress. A nanoindentation test is performed by pushing an indenter tip into the specimen and then withdrawing it, and then recording the indentation force as a function of the indenter position. A modified King's model is used to estimate the mechanical properties of the thin film in order to avoid the effects of the substrate layers. A combination of both the bulge test and the nanoindentation test can determine both Young's modulus and Poisson's ratio simultaneously.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.32 no.1
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• pp.35-42
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• 2008

Instrumented sharp indentation test is a well-directed method to measure hardness and elastic modulus. The sharp indenter such as Berkovich and conical indenters have a geometrical self-similarity in theory, but the self-similarity ceases to work in practice due to inevitable indenter tip-blunting. In this study we analyzed the load-depth curves of conical indenter with finite tip-radius via finite element method. Using the numerical regression data obtained from Kick's law, we first confirmed that loading curvature is significantly affected by tip radius as well as material properties. We then established a new method to evaluate Young's modulus, which successfully provides the value of elastic modulus with an average error of less than 2%, regardless of tip-radius and material properties of both indenter and specimen.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.37 no.10
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• pp.1229-1237
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• 2013

In this study, the theory of spherical indentation based on incremental plasticity is extended to an indentation method for evaluating creep properties. Through finite element analysis (FEA), the point where the elastic strain effect is negligible and the creep strain gradient constant is taken as the optimum point for obtaining the equivalent strain rate and stress. Based on FE results for spherical indentation with various values of creep exponent and creep coefficient, we derive by regression an equation to calculate creep properties using two normalized variables. Finally a program is generated to calculate creep exponent and creep coefficient. With this method, we obtain from the load-depth curve creep exponents with an average error of less than 1.5 % and creep coefficients with an average error of less than 1.0 %.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.10 no.4
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• pp.330-336
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• 2000

Effects of microstructure and indentation stress on fracture behavior of glass-infiltrated alumina composite for dental restorative application were investigated by the Hertzian and Vickers indentation method. Indentation stress-strain curve of glass-infiltrated alumina has showed the quasi-plastic behavior - deviation from linearity at high stress and the classical Hertzian cone crack, which could be confirmed the subsurface damage micrographs using bonded-interface specimen technique. The indentation stress-strain curves for the starting preforms are strongly dependent on porosity and microstructure of the preforms. On the other hand, the curves for the infiltrated composites are relatively insensitive to these factors. The failure of composite is originated at quasi-plastic deformation region. Damage and fracture behavior due to Hertzian stress field is theoretically examined, so that the indentation stress field plays a great role in material degradation. After Hertzian indentation annealing processing changes fracture behavior of alumina composite, so that stress field in material is healed through annealing.

• Journal of the Korean Society for Nondestructive Testing
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• v.26 no.5
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• pp.306-314
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• 2006

Instrumented indentation technique is a new way to evaluate nondestructive such mechanical properties as flow properties, residual stress and fracture toughness by analyzing indentation load-depth curves. This study evaluated quantitatively the flow properties of steels and residual stress of weldments. First, flow properties can be evaluated by defining a representative stress and strain from analysis of deformation behavior beneath the rigid spherical indenter and the parameters obtained from instrumented indentation tests. For estimating residual stress, the deviatoric-stress part of the residual stress affects the indentation load-depth curve, so that by analyzing the difference between the residual-stress-induced indentation curve and residual-stress-free curve, the quantitative residual stress of the target region can be evaluated. The algorithm for flow property evaluation was verified by comparison with uniaxial tensile test and the residual stress evaluation model was compared to mechanical cutting and ED-XRD results.

• Proceedings of the Korean Reliability Society Conference
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• 2011.06a
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• pp.125-130
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• 2011

발전 설비는 기대 수명동안의 안정성을 확보하기 위하여 해당 규격에 부합하도록 설계하여 건설된다. 하지만 가동 중 다양한 복합 환경에 노출됨에 따라 구조물을 이루고 있는 재료의 열화 현상이 가속화되어 예기치 못한 파손이 발생할 수 있다. 기계적 물성은 재료의 기계적 거동을 나타내는 주요 척도가 되며 이는 신뢰성 및 안전과 직결된다. 하지만 기존의 역학물성을 측정하는 대부분의 시험법들은 특정 크기의 시편을 요구하고 파괴적인 시험법이기 때문에 가동 중 시설물에 적용하기가 불가능하였다. 이러한 한계점을 극복하고자 비파괴적이고 정량적인 시험이 가능한 연속압입시험법이 최근 각광받는 시험법으로서 많은 연구자들에 의해 연구되고 있다. 이 시험법은 시험 대상물의 형상에 제약을 받지 않으며 시험 절차가 매우 간단하다는 장점을 가진다. 또한 대상의 국소 부위에 시험할 수 있어 취약 부위 판별이 가능하다. 본 연구에서는 대표응력-대표변형률 기법을 통하여 인장물성을 평가하고, 압입 하중 차이를 이용하여 소재에 존재하는 잔류응력을 평가하는 기법을 소개한다. 또한, 연속압입시험을 이용하여 실제 발전소 파이프의 취약부위로 알려진 용접부에 대하여 인장물성 및 잔류응력을 측정함으로써 실제 산업체의 신뢰성 평가가 적용할 수 있음을 확인하였다.