• Journal of the Society of Cosmetic Scientists of Korea
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• v.47 no.1
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• pp.57-63
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• 2021

In this study, isoscoparin was selected as an indicator component to develop Silene seoulensis extract as a functional cosmetic material, and we developed an analysis method using high performance liquid chromatography (HPLC) for quality control. HPLC was performed on a Unison US-C18 with a gradient elution of 0.05% (v/v) trifluoroacetic acid (TFA) and methanol at a flow rate of 1.0 mL/min at 35 ℃, and the detection wavelength was 330 nm. The HPLC method was performed in accordance with the international conference on harmonization (ICH) guideline (version 4, 2005) of analytical procedures with respect to specificity, precision, accuracy, and linearity. The limits of detection and quantitation were 0.02 and 0.07 mg/mL respectively. Calibration curves showed good linearity (R2 > 0.99988), and the precision of analysis was satisfied (less than 0.46%). In addition, the recovery rate was in the range of 99.10 to 101.61%, it was shown to be accurate. This result indicated that the established HPLC method is very useful for the determination of marker compounds in Silene seoulensis extracts.

• Journal of the Korea institute for structural maintenance and inspection
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• v.26 no.2
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• pp.76-83
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• 2022

Since the 3D printing mortar is exposed to the atmosphere immediately after printing, moisture is largely evaporated from the surface of the layer. The evaporation of moisture on the surface of the layer greatly causes drying shrinkage and increases the risk of cracking and damage to the structure due to drying shrinkage. This study experimentally evaluated the shrinkage behavior of the initial age using the mortar used for 3D printing. The change in shrinkage was evaluated by comparing the shrinkage of the specimen cured by the sealing method and the atmospheric exposure method. In addition, compared with the case where type 1 cement was used 100%, the shrinkage amount was evaluated when 20% of fly ash was replaced and 10% of silica fume was used. In particular, the effect of three chemical admixtures applied using 3D printing on shrinkage was evaluated experimentally. When fly ash and silica fume were used, the shrinkage amount increased by 60 - 110% compared to the case when type 1 cement was used. The application of viscosity modifiers and shrinkage reducers reduced the shrinkage by at least 18% and at most 70% depending on the curing conditions. The temperature of the specimen temporarily decreased to 15 ℃ at the beginning of curing, and the correlation between the internal temperature of the specimen and the shrinkage behavior was observed.

• Journal of the Korean Society of Marine Environment & Safety
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• v.28 no.4
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• pp.639-647
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• 2022

The use of flames is essential in cutting, bending, and welding steel during a ship's construction process. While acetylene fuel is commonly used in steel cutting and the manufacturing process in shipyards, the use of propane as an alternative fuel has recently been increasing, due to the lower risk of explosion and propane's relatively low calorific value. However, propane fuel has a relatively slow processing speed and high slag generation frequency, thereby resulting in poor quality. Propylene is another alternative fuel, which has an excellent calorific value. It is expected to gain wider use because of its potential to improve the quality, productivity, and efficiency of steel processing. In this study, the combustion characteristics of propane and propylene fuel during steel plate processing were analyzed and compared. The reduction of greenhouse gases and other harmful gases when using propylene flame was experimentally verified by analyzing the gases emitted during the process. Heat distribution and tensile tests were also performed to investigate the effects of heat input, according to processing fuel used, on the mechanical strength of the marine steel. The results showed that when propylene was used, the temperature was more evenly distributed than when propane fuel was used. Moreover, the mechanical tests showed that when using propylene, there was no decrease in tensile strength, but the strain showed a tendency to decrease. Based on the study results, it is recommended that propylene be used in steel processing and the cutting process in actual shipyards in the future. Additionally, more analysis and supplementary research should be conducted on problems that may occur.

• Journal of Soil and Groundwater Environment
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• v.27 no.3
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• pp.11-21
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• 2022

The purpose of this study was to evaluate the influences of digestion temperature on the extraction of heavy metals from soil using the standard method established by Korean Ministry of Environment (KMES). A total of 7 heavy metals (As, Cd, Cr, Cu, Ni, Pb and Zn) in soil samples were extracted at varying digestion temperatures [(66 ± 2.0)℃, (73 ± 1.9)℃, (80 ± 1.3)℃, (85 ± 1.7)℃, (92 ± 2.0)℃, (98 ± 1.7)℃]. As, Cd, Cu, Pb and Zn concentrations remained relatively constant over the temperature range, but Ni and Cr concentrations greatly varied with the digestion temperature. The extent of variation in extraction efficiencies as compared to the concentration obtained at 66℃ was in following order; Ni (7.09% ~ 35.42%) > Cr (4.79% ~ 25.40%) > Zn (3.99% ~ 17.52%) > Cu (2.22% ~ 19.34%) > As (3.54% ~ 8.26%) > Cd (-5.08% ~ 1.08%) > Pb (-4.71% ~ -1.70%). The accuracy for certified reference materials at the digestion temperature of 80 and 85℃ was 98.7% ~ 105.8%. Therefore, digestion temperature of 80℃ ~ 85℃ is suggested to obtain reliable and reproducible data when the standard method by Korean Ministry of Environment is employed to analyze multiple heavy metal components in soil samples.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.42 no.5
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• pp.607-616
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• 2022

Corrosion and degradation of reinforced structures due to abnormal climates and natural disasters further accelerate the aging of structures. Coping with the decrease in structure performance, many old structures are being repaired and reinforced with low-weight and high-strength materials such as glass fiber composite material (GFRP). To further contribute, this paper focus on a more economical and eco-friendly material, basalt fiber composite (BFRP), which provide a more effective lateral constraint effect for seismic reinforcement. The main variables considered in this study are the curing temperature during the manufacturing of BFRP and the material characteristics of the target concrete member. The lateral constraint reinforcement effect was investigated through the evaluation of the performance of normal concrete and those with improved durability through fiber reinforcement. The reinforcement effect was 3.15 times for normal concrete and 3.72 times for fiber reinforced concrete, and the difference in reinforcement effect due to the improvement of the durability characteristics of the compression member was not significant. Lastly, the performance of the BFRP was compared with the results of the GFRP reinforcement from the previous study. The effect of the BFRP reinforcement was 1.18 times better than that of the GFRP reinforcement.

• Resources Recycling
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• v.30 no.2
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• pp.39-45
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• 2021

Spent photovoltaic module is one of the important resource of silver, while related research concerning silver recovery remains limited. In our previous research, HNO3 was utilized to dissolve Ag(I) and Al(III) from the spent silicon solar cells. In order to recover Ag(I) from the leachate of a silicon solar cell, the present study made use of a nitrate solution containing Ag(I) and Al(III), which was subjected to a solvent extraction process with 5,8-diethyl-7-hydroxydodecan-6-oxime (LIX63). Ag(I) was selectively extracted with LIX63 over Al(III) from the nitrate leach solution. Subsequently, quantitative stripping of Ag(I) from the loaded LIX63 was performed by using 20% ammonia water. The McCabe-Thiele plots for the extraction and stripping isotherms of Ag(I) were also constructed. Extraction and stripping simulation tests confirmed an Ag(I) extraction and stripping efficiency of >99.99% and 98.9%, respectively with high purity Ag (99.998%) and Al (99.99%) solution. A process flow sheet for Ag(I) recovery from the nitrate leach solution was proposed.

• Tunnel and Underground Space
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• v.32 no.6
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• pp.568-585
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• 2022

In the present study, we proposed a numerical method for simulating thermally induced fracture slip using a grain-based distinct element model (GBDEM). As a part of DECOVALEX-2023, the thermo-mechanical loading test on a saw-cut rock fracture conducted at the Korea Institute of Civil Engineering and Building Technology was simulated. In the numerical model, the rock sample including a saw-cut fracture was represented as a group of random Voronoi polyhedra. Then, the coupled thermo-mechanical behavior of grains and their interfaces was calculated using 3DEC. The key concerns focused on the temperature evolution, thermally induced principal stress increment, and fracture normal and shear displacements under thermo-mechanical loading. The comparisons between laboratory experimental results and the numerical results revealed that the numerical model reasonably captured the heat transfer and heat loss characteristics of the rock specimen, the horizontal stress increment due to constrained displacement, and the progressive shear failure of the fracture. However, the onset of the fracture slip and the magnitudes of stress increment and fracture displacement showed discrepancies between the numerical and experimental results. We expect the numerical model to be enhanced by continuing collaboration and interaction with other research teams of DECOVALEX-2023 Task G and validated in further study.

• Journal of the Korean Institute of Gas
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• v.26 no.6
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• pp.37-44
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• 2022

In this study, two low-swirl nozzles with the same SN (Swirl Number) but different mass ratio (m) of the core part and the swirler part were designed to perform an atmospheric pressure combustion test. For each nozzle, a combustion test was conducted according to the adiabatic flame temperature, and the flame structure, emissions, and combustion instability mode were identified. Although the flame structure was significantly different, the CO emission was similar, and the NOx emission was also more related to combustion dynamics than the flame structure. Combustion dynamics and NOx emission were identified while adjusting the convection delay time by changing the position of the fuel injection nozzle. It was confirmed that when the convection delay time is in the region of (3+4n)/4T±1/4T (n=0,1,2,...), the combustion instability is strong, and in the opposite case, the combustion instability is very weak.

• Journal of Mushroom
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• v.20 no.4
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• pp.263-269
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• 2022

This study investigated the culture characteristics of Cryptoporus volvatus, whichis grow naturally in Korea, to determine the suitable environmental conditions for its cultivation. The physiological characteristics of the mycelia were assessed according to the cultivation conditions, to determine the optimal conditions for artificial cultivation. The visual characteristics of the hyphae of Cryptoporus volvatus KACC52303 included an irregular and uneven surface and a fuzzy or cotton-like texture. Under the microscope, its microstructure showed pre-chlamydospore formation, but no clamps were seen. The appropriate culture temperature was found to be a medium/high temperature of approximately 25-30℃, and the optimal pH was found to have a wide range from weakly acidic (pH 4) to neutral (pH 7). In the optimal nutrient source experiment, hyphal growth was shown to be fair in a mixed medium with 2.5% dextrin as the carbon source and 0.1% yeast extract as the organic nitrogen source. Among the various amino acids, organic acids, and inorganic salts tested, the fastest hyphal growth was observed in the presence of leucine, acetic acid or gluconic acid, and KCl or KH₂PO₄, respectively. The column test showed that the best mycelial growth occurred in a mixed medium of 80% pine sawdust, 10% rice bran, and 10% corncob sawdust.

• Journal of the Korean Wood Science and Technology
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• v.32 no.5
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• pp.75-85
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• 2004

The natural dyes from Gardenia jasminoides, Carthamus tinctorius L., Rhus javanica, Lithospermum erythrorhizon, Caesalpinia sappan L., and Castanea crenata were extracted under different pH in distilled water, As the pH in distilled water went from acid to alkali, the much deeper colors in the same color tone were generated from the individual plant species. Before dyeing, wood species were treated by different mordants including AI, Cu, Cr and Fe for color-fixing between wood and the natural dyes. Each mordant could develop independent color on the surface of the woods. The wood species dyed by the natural dyes created deep-tone colors according to higher pH and temperature of the dyeing solution, leading to deeper penetration of the dyes into the wood tissues. Finally through the computer modelling of natural-dyed wood furniture, it was confirmed that the colored furniture can adequately be compatible with the current interior spaces of diverse colors.