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Beam-Type Bend Specimen for Interlaminar Fracture Toughness of Laminated Composite under Mixed-Mode Defmrmations (보 형태의 굽힘시편을 이용한 적층복합재료의 혼합모우드 층간파괴인성 평가)

  • 윤성호;홍창선
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.13 no.5
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    • pp.911-920
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    • 1989
  • It this study, beam-type bend specimen is used to evaluate the interlaminar fracture toughness of laminated composite under mixed-mode deformations. The specimen is loaded under three-point bending and hence produced mixed-mode deformations in the vicinity of the crack tip according to the variation of the thickness ratio on delamination plane. Total energy release rate is obtained by elementary beam theory considering the effect of shear deformation. The partitioning of total value into mode-I and mode-II components is also performed. The mixed-mode interlaminar fracture toughness is evaluated by experiments on specimens with several thickness ratios of delamination plane. As the part of delamination plane is thicker, the effect of shear deformation on total energy release rate is increased. Beam-type bend specimen men may be applied to obtain informations on the mixed-mode interlaminar fracture behavior of laminated composites.

Temperature and Frequency Dependences of Ultrasonic Properties in Commercial MC Nylon Polymers (상용 MC Nylon계 고분자 재료에서 초음파 특성의 온도 및 주파수 의존성)

  • Kim, Myung Deok;Kim, Yong Tae;Lee, Kang Il
    • Journal of the Korean Society for Nondestructive Testing
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    • v.32 no.5
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    • pp.509-517
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    • 2012
  • In the present study, temperature and frequency dependences of ultrasonic properties such as attenuation coefficient and phase velocity was investigated for six kinds of commercial MC-Nylon polymer samples. The ultrasonic properties of the samples were measured by using a pulse transmission method in water over a broadband frequency range of 2 to 8 MHz. Water temperature was varied from 10 to $60^{\circ}C$ with the $10^{\circ}C$ interval. The attenuation coefficients of the samples increased with the frequency and the exponent n of frequency dependence ranged within 1.16 to 1.44, slightly deviating from the linear dependence (n=1). The phase velocities of the samples exhibited negative dispersion, i.e., decreasing velocity with increasing frequency, except for ivory sample at $60^{\circ}C$. The frequency-dependent phase velocities of the samples showed the decreasing tendency with increasing temperature.

Study on the Experimental Aging Estimation Technique for HTPB based Solid Propellant Considering Post Curing Effect (후경화를 고려한 HTPB 고체 추진제의 실험적 노화평가 기법 연구)

  • Jung, Gyoo Dong;Park, Jae Beom;Kim, Shinhoe
    • Journal of the Korean Society of Propulsion Engineers
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    • v.23 no.3
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    • pp.51-57
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    • 2019
  • Post curing effects are estimated by specimen tests. Propellant specimen accelerated aging tests are performed when post curing is estimated to be complete and the coefficients of Arrhenius aging equations are acquired. Simulated motors with cylindrical grain are designed and fabricated to confirm the application. Accelerated aging tests are conducted, and aged properties are measured and estimated for the inner bore, center and bond parts of the grain. The measured aging ratios of the modulus are compared with the ones predicted by the equations. As the results, the accelerated aging equations predict well the propellant aging trends; however, some differences are observed at the bond part. Therefore, the specimen extraction part must be carefully chosen to suit the test purpose when a rocket motor grain is used for the aging test.

Development of Low-Cost High-Performance Antibacterial Tempered Glass (저비용 고기능성 항균강화유리 개발을 위한 연구)

  • Kim, Jun-Sub
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.22 no.1
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    • pp.562-567
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    • 2021
  • To develop an antibacterial tempered glass for applications to various building facilities and household products, the antibacterial activity of domestic materials was investigated, and a tempered glass sample was produced with silver, copper, and zinc, having an antibacterial activity of 99% or more at a specific concentration. The measured antibacterial activity of the samples, in which silver, copper, and zinc were dispersed in ethylene glycol + glycerol, was more than 99%. Measurements of the thickness of the coated metal material by washing using a surface analyzer showed that the thickness decreased by less than 1% in various types of detergents, including water, but only approximately 10% in the alkaline detergents. To check the human safety of the samples, a cytotoxicity test was performed through an MTT assay; the samples showed no cytotoxicity. Finally, a Live/Dead kit or film adhesion method showed that the antibacterial activity of the prototype was more than 99%. Therefore, the high-functional antibacterial effect of tempered glass was developed using domestic materials and may be used in various products in the future.

Evaluation of Weathering Durability of Waterborne Preservative Treated Wood by Accelerated Weathering (수용성 방부처리재의 기상열화 저항성 평가)

  • Lee, Myung-Jae;Lee, Dong-Heub;Kim, Gyu-Hyeok
    • Journal of the Korean Wood Science and Technology
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    • v.31 no.4
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    • pp.44-49
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    • 2003
  • This study was carried out to evaluate the weathering durability of waterborne preservative (AAC, ACQ, CCA, CuAz) treated Japanese red pine (Pinus densiflora S. et Z.) sapwood samples by accelerated weathering, and to find out the factor of stability. When considered the color changes, weight losses, surface degradation, and microstructure changes due to weathering, ACQ-, CCA-, and CuAz-treated samples were durable against weathering; the weathering durability of AAC-treated samples was poor and similar to untreated controls. The lignin content in aqueous extracts collected from ACQ-, CCA-, and CuAz-treated samples during weathering was lower than that from untreated and AAC-treated ones. From these findings, we might concluded that weathering durability of ACQ-, CCA-, and CuAz-treated samples was enhanced by the fixation of preservative component(s) onto the lignin structure, which is very susceptible to weathering.

Weathering of Prunus sargentii Specimens Modified with Acetic Anhydride and Formaldehyde Vapor (무수초산 및 포름알데하이드 기상처리 산벚나무의 야외폭로 및 촉진열화)

  • Kang, Ho-Yang;Kim, Su-Won;Park, Sang-Jin
    • Journal of the Korean Wood Science and Technology
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    • v.31 no.5
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    • pp.57-64
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    • 2003
  • Small cherry specimens modified with acetic anhydride and formaldehyde vapor phase were weathered by outdoor exposure and accelerated conditioning in a climate chamber. The effects of the chemical modification were evaluated by measuring their weight percentage gains (WPG), hygroscopicity and color differences before and after weathering. The average WPGs of the 72 hour acetylated and formaldehyde-treated specimens were 8.1 and 15.7%, respectively. After outdoor exposure for more than 2 months, the acetylated specimens lost weights by only 1.5%, but the formaldehyde-treated did much more than the formers. It was revealed that acetylation reduced the hygroscopicity and discoloration of wood while formaldehyde treatment didn't. Moreover the longer is the formaldehyde treatment time the more degraded after weathering. It was concluded that the vapor-phase acetylation could be applied for improving the dimensional stability of old wooden blocks.

Evaluation of the Effect of Nickel Powder on the Piezoresistivity Behavior of Carbon-Fiber/Rubber Composites (탄소섬유/고무 복합재료의 압저항과 니켈입자의 영향)

  • Lim, Dong-Jin
    • Composites Research
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    • v.34 no.6
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    • pp.412-420
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    • 2021
  • In this study, we measure the initial electrical conductivity of SCF/rubber specimens and SCF/rubber specimens with nickel particles respectively. The corresponding electrical conductivity with compressive strain on the specimens is also measured. Through this experiment, we observed the effects of the volume fraction of carbon fiber, nickel particles and external strain on the electrical conductivity. Experiments show that even a small difference in the volume fraction of SCF plays a major role in the change of the electrical conductivity and that the piezoresistivity increases due to fiber reorientation respond to external strain. In addition, the nickel particles contribute to improving the electrical conductivity in specimens with carbon fibers above the threshold volume fraction. It was confirmed that there is an effect of offsetting the increment in the piezoresistivity caused by the reorientation of carbon fibers according to external strain.

Mechanical Properties of 3D Printed Composite Material on Various Thermal Environment (다양한 온도 환경에 따른 3D 프린트 복합재료의 기계적 물성 평가)

  • Sang-Hun Kang;Do-Hyeon Kim;Hyoung-Seock Seo
    • Composites Research
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    • v.36 no.3
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    • pp.193-198
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    • 2023
  • Currently, there are many discussions about composite materials and 3D printed composite material to weight reduction of ships. A test was conducted to confirm the applicability of the 3D printed composite material to ships and offshore structures by linking the 3D printing technology with excellent productivity and the composite material with corrosion resistance and lightweight characteristics in salt water environments. In order to apply the 3D printed composite material used in this paper to ships and offshore structures, the temperature environmental effects that can be exposed in the marine environment should be considered. Therefore, the tensile test was conducted with specimen of Carbon + Onyx, Carbon + Nylon, HSHT glass + Onyx, HSHT glass + Nylon material in low temperature (-50℃), room temperature (20℃), and high temperature (50℃) environments that can be exposed to the marine environment. As a result of the tensile test, the carbon + onyx specimen showed the highest tensile strength and the HSHT glass + onyx specimen showed the highest tensile strain. In addition, by analyzing the tested specimens, the failure mode of the 3D printed composite material specimens exposed to various temperature environments was analyzed.

Properties of Yttrium Manganates with MFS Structure Fabricated on Various Substates (MFS 구조로 적층된 Yttrium Manganates의 기판 변화에 따른 특성 연구)

  • 강승구
    • Journal of the Korean Ceramic Society
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    • v.40 no.2
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    • pp.206-211
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    • 2003
  • Effects of substrates and buffer layer upon the formation of crystalline phases and ferroelectricity of $YMnO_3$ thin films were investigated. The hexagonal $YMnO_3$ was easily formed on Si(100) while the mixed phases, hexagonal and orthorhombic $YMnO_3$, on $Pt(111)/TiO_2/SiO_2/Si$ substrate. When the $Y_2O_3$ buffer layer of 70 nm thick was inserted between the substrates and the $YMnO_3,$ the c-axis oriented hexagonal single phase formed on both substrates, Si(100) and $Pt(111)/TiO_2/SiO_2/Si$. The leakage current density of the hexagonal $YMnO_3$ thin films was lower than that consisting of mixed phases, hexagonal and orthorhombic. Furthermore the hexagonal $YMnO_3$ with c-axis preferred orientation showed the lowest leakage current density. The remnant polarization from a P-E hysteresis curve for the $YMnO_3$ formed on Si(100) was 0.14 without buffer layer and $0.24_{mu}C/cm^2$ for that with buffer layer. For the $Pt(111)/TiO_3/SiO_3/Si$ substrates, the specimen without $Y_2O_3$buffer layer did not show the hysteresis curve, while the buffer-layered has the remnant polarization of $1.14_{mu}C/cm^2$. It was concluded that the leakage current density and the ferroelectricity for the $YMnO_3$ thin films could be controlled by varying crystalline phases and their preferred orientation which depend on the kind of substrates and whether the $Y_2O_3$buffer layer exist or not.

Influence of resin-nanoceramic CAD/CAM block shade and thickness on the microhardness of dual-cured resin cement (레진-나노세라믹 CAD/CAM블록의 색조와 두께가 이원중합 레진시멘트의 미세경도에 미치는 영향)

  • Choi, Ga-Young;Park, Jeong-Kil;Jin, Myoung-Uk;Kwon, Yong Hoon;Son, Sung-Ae
    • Korean Journal of Dental Materials
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    • v.44 no.2
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    • pp.151-161
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    • 2017
  • The purpose of this study was to examine the effect of shade and thickness of resin-nanoceramic CAD-CAM block (RNB) on the microhardness of dual-cured resin cement, as well as to measure the number of photons transmitted through RNBs of different thicknesses and colors. One dual-cured resin cement was used to prepare resin cement specimens. Resin cement specimens were light-cured for 40 seconds through 3 shades (A1, A2, A3 in HT (high translucency) and LT (low translucency) respectively) and four thicknesses (1, 2, 3, 4 mm) of RNB specimens. Vickers microhardness measurements of resin cement specimens were performed using a Vickers hardness tester. The light transmission of RNB specimens was measured using a spectrometer (SpectroPro-500, Acton Research, Acton, MA, U.S.A.), and the translucency parameter was calculated using the CIEL*a*b* system. Data were statistically analyzed by ANOVA and Tukey's test. There was a significant decrease of microhardness of resin cement specimen with an overlay of 4 mm of RNB thickness and A3 shade in comparison to A1 and 1 mm, respectively (p<0.05). The translucency parameter values and light transmission of RNBs tested differed significantly, according to the thicknesses of the specimen (p<0.05). Light transmission is decreased with increase in the thicknesses of RNBs. Shade A1 transmitted more light than darker blocks. A decrease in microhardness of resin cement specimens was observed with increasing thickness and shade (A1 to A3) of RNBs.