• Title/Summary/Keyword: 수직분리

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Direct Bonding of Si(100)/NiSi/Si(100) Wafer Pairs Using Nickel Silicides with Silicidation Temperature (열처리 온도에 따른 니켈실리사이드 실리콘 기판쌍의 직접접합)

  • Song, O-Seong;An, Yeong-Suk;Lee, Yeong-Min;Yang, Cheol-Ung
    • Korean Journal of Materials Research
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    • v.11 no.7
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    • pp.556-561
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    • 2001
  • We prepared a new a SOS(silicon-on-silicide) wafer pair which is consisted of Si(100)/1000$\AA$-NiSi Si (100) layers. SOS can be employed in MEMS(micro- electronic-mechanical system) application due to low resistance of the NiSi layer. A thermally evaporated $1000\AA$-thick Ni/Si wafer and a clean Si wafer were pre-mated in the class 100 clean room, then annealed at $300~900^{\circ}C$ for 15hrs to induce silicidation reaction. SOS wafer pairs were investigated by a IR camera to measure bonded area and probed by a SEM(scanning electron microscope) and TEM(transmission electron microscope) to observe cross-sectional view of Si/NiSi. IR camera observation showed that the annealed SOS wafer pairs have over 52% bonded area in all temperature region except silicidation phase transition temperature. By probing cross-sectional view with SEM of magnification of 30,000, we found that $1000\AA$-thick uniform NiSi layer was formed at the center area of bonded wafers without void defects. However we observed debonded area at the edge area of wafers. Through TEM observation, we found that $10-20\AA$ thick amourphous layer formed between Si surface and NiSix near the counter part of SOS. This layer may be an oxide layer and lead to degradation of bonding. At the edge area of wafers, that amorphous layer was formed even to thickness of $1500\AA$ during annealing. Therefore, to increase bonding area of Si NiSi ∥ Si wafer pairs, we may lessen the amorphous layers.

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Evaluation of Fracture Behavior of Adhesive Layer in Fiber Metal Laminates using Cohesive Zone Models (응집영역모델을 이용한 섬유금속적층판 접착층의 모드 I, II 파괴 거동 물성평가)

  • Lee, Byoung-Eon;Park, Eu-Tteum;Ko, Dae-Cheol;Kang, Beom-Soo;Song, Woo-Jin
    • Composites Research
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    • v.29 no.2
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    • pp.45-52
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    • 2016
  • An understanding of the failure mechanisms of the adhesive layer is decisive in interpreting the performance of a particular adhesive joint because the delamination is one of the most common failure modes of the laminated composites such as the fiber metal laminates. The interface between different materials, which is the case between the metal and the composite layers in this study, can be loaded through a combination of fracture modes. All loads can be decomposed into peel stresses, perpendicular to the interface, and two in-plane shear stresses, leading to three basic fracture mode I, II and III. To determine the load causing the delamination growth, the energy release rate should be identified in corresponding criterion involving the critical energy release rate ($G_C$) of the material. The critical energy release rate based on these three modes will be $G_{IC}$, $G_{IIC}$ and $G_{IIIC}$. In this study, to evaluate the fracture behaviors in the fracture mode I and II of the adhesive layer in fiber metal laminates, the double cantilever beam and the end-notched flexure tests were performed using the reference adhesive joints. Furthermore, it is confirmed that the experimental results of the adhesive fracture toughness can be applied by the comparison with the finite element analysis using cohesive zone model.

A Novel Volumetric Method for Quantitation of Titanium Dioxide in Cosmetics (용량분석법을 이용한 화장품 중 티타늄옥사이드의 정량)

  • Kim, Young-So;Kim, Boo-Min;Park, Sang-Chul;Jeong, Hye-Jin;Chang, Ih-Seop
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.31 no.4 s.54
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    • pp.289-293
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    • 2005
  • Nowadays there are many sun protection cosmetics including organic or inorganic UV filter as an active ingredient. Chemically stable inorganic sunsEreen agents, usually metal oxides, we widely employed in high SPF products. Titanium dioxide is one of the most frequently used inorganic UV filters. It has been used as pigments for a long period of cosmetic history. With the development of micronization techniques, it becomes possible to incorporate titanium dioxide in sunscreen formulations without whitening effect and it becomes an important research topic. However, there are very few works related to quantitations of titanium dioxide in sunscreen products. In this research, we analyzed amounts of titanium dioxide in sunscreen cosmetics by adapting redof titration, reduction of Ti(IV) to Ti(III) and reoxidation to Ti(IV). After calcification of other organic ingredients of cosmetics, titanium dioxide is dissolved by hot sulfuric acid. The dissolved Ti(IV) is reduced to the Ti(III) by adding aluminum metals. The reduced Ti(III) is titrated against a standard oxidizing agent, Fe(III) (ammonium iron(III) sulfate), with potassium thiocyanate as an indicator In order to test accuracy and applicability of the proposed method, we analyzed the amounts of titanium dioxide in four types of sunscreen cosmetics, such as cream, make-up base, foundation and powder, after adding known amounts of titanium dioxide $(1{\sim}25w/w%)$. The percent recoveries of the titanium dioxide in four types of formulations were in the range between 96 and 105%. We also analyzed 7 commercial cosmetic products labeled titanium dioxide as an ingredient and compared the results with those of obtained from ICP-AES (Inductively Coupled Plasma-Atomic Emission Spectrometry), one of the most powerful atomic analysis techniques. The results showed that the titrated amounts were well coincided with the analyzed amounts of titanium dioxide by ICP-AES. Although instrumental analytical methods, ICP-MS (Inductively Coupled Plasma-Mass Spectrometry) and ICP-AES, are the best for the analysis of titanium, it is hard to adopt because of their high prices for small cosmetic companies. It was found that the volumetric method presented here gat e quantitative and reliable results with routine lab-wares and chemicals.

Delineation of internal heterogeneities of Geum River point bar deposits in Buyeo area using GPR Data (지하 투과 레이다 조사를 통한 부여 지역 금강변의 충적 대수층 내부 불균질성 파악)

  • Rhee, Chul-Woo;Kim, Hyoung-Soo;Lee, Kyung-Joo
    • Journal of the Korean Geophysical Society
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    • v.5 no.4
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    • pp.337-344
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    • 2002
  • The alluvial deposits along meandering rivers can be used as an artificial aquifer for infiltration of river waters. Internal heterogeneity of the alluvial deposits is a prerequisite information for the development of alluvial groundwater because vortical and lateral movement of alluvial ground water depends on the internal heterogeneity The internal heterogeneity due to variations in channel behavior can be delineated using GPR survey, GPR profiles for the point bar deposits near Buyeo county reveals two different stratigraphic units: the lower inclined heterogeneous strata and the upper horizontally stratified strata. The upper unit is largely indicative of vertical accumulation by overbank floods within a floodplain, whereas the lower one represents typical point bar deposits formed by lateral accretion. The stratigraphic variation in the heterogeneity shows that GPR survey is a useful and necessary investigation method for the development of alluvial ground water.

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Experimental Analysis of Terminus and Horizontal Crack Behaviors in Continuously Reinforced Concrete Pavement (연속철근 콘크리트 포장 단부 및 수평균열 거동 실험적 분석)

  • Cho, Young-Kyo;Kim, Seong-Min;An, Zuog;Han, Seung-Hwan
    • International Journal of Highway Engineering
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    • v.13 no.4
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    • pp.81-91
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    • 2011
  • This study was conducted to evaluate the necessity of the anchor lug system in continuously reinforced concrete pavement(CRCP) by comparing longitudinal displacements of CRCPs with and without anchor lugs, and to investigate the effect of horizontal cracking on CRCP performance by measuring the vertical displacements. The measurements before and after the anchor lug section was separated were conducted for 12 days in June, and for 14 days in August after the abrupt displacements according to cutting disappeared, respectively. This short term measurement results showed that when anchor lugs were installed, a daily displacement variation at any location was less than 0.1mm; therefore, longitudinal movements were negligibly small. When there were no anchor lugs, longitudinal displacements mainly occurred near the free end and the displacement variation was small; therefore, an expansion joint system seems to be employed at a CRCP terminus without installing anchor lugs. However, further studies are needed to verify the terminus behavior due to annual temperature changes. The horizontal crack width variation was ignorable and did not affect the vertical displacement of the slab. Therefore, the horizontal crack did not delaminate the slab and did not seem to reduce the structural capacity and performance of CRCP.

An Experimental Study on the Shear Behavior of Reinforced Concrete Beams Strengthened by Slit Type Steel Plates with Anchor Bolt (앵커볼트 체결 Slit형 강판 보강 RC보의 전단거동에 관한 실험적 연구)

  • Lee, Choon-Ho;Jeong, Woo-Dong;Shim, Jong-Seok
    • Journal of the Korea Concrete Institute
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    • v.22 no.5
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    • pp.703-710
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    • 2010
  • Reinforced concrete beams of existing structure often encounter insufficient shear problems for various reasons. Application of steel plates is one of widely used methods for shear strengthening of reinforced concrete beams that are insufficient of shear capacity. This study presents test results on strengthening shear deficient RC beams by external bonding of vertical and diagonal slit type steel plates with anchor bolt. Test parameters are width, interval, angle and length of slits with anchor bolt. The purpose was to evaluate the failure modes and shear capacities for RC beams strengthened by various slit type steel plates with anchor bolt. The results showed that the slit type steel plate specimens strengthened by adhesive bonding and bolting failed in shear fracture modes at maximum load. Flexural crack first occurred on the tension face of beam and then inclined cracks occurred on the shear span. Finally, slit type steel plates strengthened by adhesive bonding and fastening bolts managed to delay abrupt debonding and didn't detach fully from main body of RC beam.

INTENTIONAL REPLANTATION OF CROWN-ROOT FRACTURED TOOTH WITH OPEN APEX (의도적 재식술을 이용한 치관-치근 파절된 미성숙영구치의 치험례)

  • Ryu, Jung-A;Lee, Jae-Ho;Choi, Byung-Jai;Son, Heung-Kyu;Choi, Hyung-Jun
    • Journal of the korean academy of Pediatric Dentistry
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    • v.31 no.2
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    • pp.267-272
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    • 2004
  • This case report describes an uncommon treatment method for crown-root fractured incisor with immature root. A 7-year-old girl was referred for treatment of crown-root fractured maxillary central incisor. The fracture line extended to 1/2 of the total tooth length with incomplete root formation. The prognosis of crown-root fracture is usually poor and extraction is usually undertaken. But, in the mixed dentition, extraction of maxillary permanent incisor results in many complications, such as resorption of alveolar bone, poor esthetics, pronunciation and mastication. Conservative therapy in the permanent dentition comprises of few treatment modalities; supragingival restoration, gingivectomy, orthodontic extraction of apical fragment, surgical extrusion of apical fragment with or without rotational replantation. However, in this case, these indications are not applicable, so intentional replantation with adhesive resin system is the treatment of choice. The tooth was followed-up for 12 months. Currently, there are no symptoms. Since this modality adopts the respective advantages of both intentional replantation and adhesive treatment, it might be the treatment of choice in cases of vertical crown-root fracture.

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A Design and Performance Evaluation of Differentiated Daylight-Glazing Systems (가변 투과시스템의 광제어 특성을 고려한 통합 채광시스템의 적용성 평가에 관한 연구)

  • Kim, Gon;Kim, Jeong-Tai
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.19 no.2
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    • pp.13-22
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    • 2005
  • This research aimed to generate two points of daylighting application as follows: 1) providing daylight performance data with a variety of glazing materials for a large window and 2) designing and evaluating an experimental type of differentiated window. For this purpose, we compared the daylight and distribution performance of new defined type of window configuration to the conventional window counterpart with a variety of glazing materials. The comparison was made for a deep, south-facing perimeter zone with large window, without any interior obstruction. The conventional window is the base single homogeneous glass pane, where as the differentiated window uses of two different glazings; an upper daylight glazing with high visible transmission and lower view window with lower transmittal glass. The daylight performance data was translated into a ratio between outdoor illuminance and the interiors. The simulated analysis of the conventional window indicates that the interior light levels have been changed proportionally dependent on the transmittance of the applied glass. The comparison of daylight distribution analysis showed that the differentiated window has lots of photometric advantage by the optical function of upper daylight window. In particular, the contribution of higher daylight window into deep rear space must be stressed for daylighting application.

A Study on the Evaluation of Airborne Lidar Height Accuracy for Application of 3D Cadastral (3차원지적 적용을 위한 항공라이다의 수직 정확도 평가에 관한 연구)

  • Choi, Byoung Gil;Na, Young Woo;Lee, Kyung Sub;Lee, Jung Il
    • Journal of Korean Society for Geospatial Information Science
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    • v.22 no.2
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    • pp.33-40
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    • 2014
  • At present, Cadastral map of 2 dimensional is in the stream of changing it to 3 dimensional type supported by GPS and laser techniques. In addition, this steam can be explained at the same time with improvement of equipment of storing much information, support of equipment for imaginative 3D spatial information, and support of equipment of expressing land in 3D Cadastral. This study suggest to apply airborne lidar survey technique on cadastral map to acquire comparably and quickly detailed height of ground. For doing this, this study checked out credibility regarding accuracy of airborne lider survey. After choosing research area, this study has done the airborne lidar survey and acquire the result after surveying Cadastral Comparison Point to check out the accuracy of acquired results. In addition, this study check out the result of Cadastral Comparison Point and airborne lidar survey applied by paired sample t-test based on actual results. The result is that test statistics is 0.322 which is 5 % similar level and null hypothesis cannot be rejected, so this study found out that result of both survey ways are the same. Therefore, the result of airborne lidar survey can be utilized to build up 3D Cadastral information hereafter.

The Investigation on the Behavior of Beam-Column Joint with High and Low Strength Concerte (고강도와 보통강도 콘크리트를 사용한 보-기둥 접합부의 구조적 거동)

  • 신성우;이광수;문정일;안종문;박희민;장일영
    • Magazine of the Korea Concrete Institute
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    • v.4 no.1
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    • pp.119-126
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    • 1992
  • AC] 318-H9 Recommended that when the specified compressive strength of concrete in a column is greater than 1. 4 times that specified for a floor system, top surface of the colurrm concrete shall extend 2ftU;OOrrun) into the slab from the face of colUlml to avoid unexpected brittle failure. The purpose of this investigation is to suggest the basic information for the structural safety, The major variables are com preSSlve strength of concrete, shear confinement ratio, and loading types. The test results showed that the load capaCIty of speCImen subjected to monotOI1lC loading had more than that of specimen subjected to one way cyclic loading. The failure modes of specimens under cyclic loading were concentrated at 5-20cm apart region from beam-column joint face and ductility index are increased with increasing of shear confinement ratio. Keywords: ACI 318-89, High and Low Strength Concrete, Beam-Column Joint, Shear Confinement Ratio, Loading Type, Ductility Index, Extension Distance.