• Title/Summary/Keyword: 분쇄

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Study On the Characteristics of Milled $UO_2$ Powder Prepared by Oxidation and Reduction Process (산화ㆍ환원처리된 $UO_2$ 분말의 분쇄특성 연구)

  • Lee Jae-Won;Lee Jung-Won
    • Resources Recycling
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    • v.11 no.4
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    • pp.3-10
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    • 2002
  • The characteristics of dry and wet milled powder prepared by 1 cycle OREOX (oxidation and reduction of oxide fuels) treatment were investigated using the simulated spent fuel pellet. Sintered pellets simulating spent nuclear fuel burned in reactor were fabricated from $UO_2$ powder using as a starting material in fabrication of nuclear fuel. The 1 cycle OREOX-treated powder was prepared by only one path of oxidation md reduction of the simulated pellet. Powder having average particle size of less than 1 $\mu\textrm{m}$ could be easily obtained by dry milling, but not be achieved by wet milling. And, specific surface area of dry milled pow-der was higher than that of wet milled powder. Dry milled powder formed loose agglomerate, while wet milled powder showed the shape of irregular and angular particles. Dry milled powder provided higher green density, resulting in higher sintered density of higher than 95% TD and average grain size of larger than 8 $\mu\textrm{m}$ satisfying the standard specification of sintered pellets.

Attritor milling에 의한 $UO_2$ - 4wt% 분말의 혼합 및 혼합분말의 특성변화

  • 김시형;김한수;송근우;나상호;이영우;손동성
    • Proceedings of the Korean Nuclear Society Conference
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    • 1995.05b
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    • pp.733-738
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    • 1995
  • $UO_2$ 및 CeO$_2$ 분말을 turbular mixer에서 혼합, 또는 attritor mill에서 분쇄한 후, 각 분말의 특성변화와 이에 따른 소결특성의 변화를 관찰하였다. 혼합된 분말은 평균입자크기와 비표면적이 각각 22.9$\mu\textrm{m}$, 5.1g/㎤이었고, 2시간 분쇄된 분말은 0.5$\mu\textrm{m}$, 6.7g/㎤이었다. 혼합분말로 성형할 경우의 소결밀도는 성형압력의 증가에 관계없이 약 9.6 g/㎤로서 매우 낮았고, 2시간 분쇄된 분말은 10.35 9/㎤ 이상으로 나타나, 혼합핵연료 소결체 제조시 분쇄공정이 반드시 필요함을 나타내었다. 분쇄된 분말을 환원성분위기에서 소결할 경우에는 분쇄시간이 증가함에 따라 결정립이 8$\mu\textrm{m}$까지 증가하였는데 이것은 CeO$_2$ 분말의 미세화와 함께 Ce 성분이 균질 하게 분포되었기 때문으로 사료된다. 그러나 산화성분위기에서는 분쇄시간이 증가할 때 평균 결정립크기는 6$\mu\textrm{m}$로서 변화가 거의 없었다.

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Fine Crushing Characteristics of Concrete Wastes (콘크리트 폐기물의 분쇄 특성 연구)

  • 오중환;이효숙;정헌생
    • Resources Recycling
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    • v.5 no.2
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    • pp.52-56
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    • 1996
  • Fix crushing characteristics of construction concrete wastes wcrc rnvcstigatcd in order to scparate the natural aggregatcs. A roll crushcr and a hammcr crusher wcrc used to granulate pre-crushed concrete\ulcorner below 30 rnm The crushers pruducc finer sizes far ccmcnt concrete than for asphalt concrele, and the hammer crushing resulls in separating the aggregales from thc olhers better than thc roll crushing. The narural aggregatcs of orcr 70-90% by volume were obtained from the concretes by using a riffled shaking table.

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신형 시멘트 mill$\ldots$ COMBIDAN

  • 한국양회공업협회
    • Cement
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    • s.76
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    • pp.51-56
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    • 1979
  • F.L.Smidth는 기획적인 규모로 광범위한 시험과 운용을 한 후에 신형의 크리카 밀을 개발했다. 이 밀의 미분쇄실에서는 평균 단위중량이 5$\~$7g 밖에 안되는 최적 크기의 분쇄매체가 사용된다. 이의 사용은 특수하게 설계된 밀의 출구와 전연 새로운 원리에 바탕을 둔 매우 효율적인 스크리닝 diaphragm에 의해서 가능하게 되었다. Conbidan 밀은 개회로나 폐회로식 분쇄에서 모두 최저의 분쇄 효율을 보장하기 때문에 에너지 소비량이 상당히 절감된다. 완성시멘트에서 요구되는 입도에 따라서, 그리고 채택된 분쇄방법에 따라서 Conbidan 밀의 분쇄 효율은 (kg/kwh), 기업적인 규모로 장기에 걸쳐 시험한 결과로 나타난 바와 같이, $12\%\~27\%$가 향상된다.

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Physicochemical Characteristics of Powder from Cryogenic Grinding of Aronia, Grapefruit, Black Bean, and Germinated Brown Rice (동결분쇄에 따른 아로니아, 자몽, 서리태, 발아현미의 이화학적 특성)

  • Jeon, Hyeong-ju;Lee, Il-nam;Han, Ye-eun;Jeong, Ho-jun;Park, Ha-eun;Jung, Ju-yeong;Rhee, Jin-Kyu
    • Microbiology and Biotechnology Letters
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    • v.45 no.4
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    • pp.291-298
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    • 2017
  • We compared the ingredients present in freeze-dried ground food samples with those present in hot air-dried and ambient ground food samples to optimize processing conditions for preserving nutrients in and for improving the ingestion of different foods. The freeze-dried ground sample of black bean showed 4.57% higher retention rate than the ambient ground sample of black bean. Mineral content was also significantly different between these two samples. Moreover, the freeze-dried ground sample of black bean contained 11.54% higher content of ${\beta}$-carotene, a precursor of vitamin A, than the ambient ground sample of black bean. Total anthocyanin content was 453.49 mg in the freeze-dried ground sample of Aronia compared with 158.98 mg in the ambient ground sample of Aronia. Contents of ${\beta}$-carotene and niacin increased by 129.47% and 439.39%, respectively, in the freeze-dried ground sample of grapefruit. Retention rates of proteins, carbohydrates, and niacin were 107.74%, 103.87%, and 156.52%, respectively, in the freeze-dried ground sample of germinated brown rice. Protein digestibility increased by 120.5% and 101.14% in the freeze-dried ground samples of Aronia and black bean, respectively, but did not increase in the freeze-dried ground samples of grapefruit and germinated brown rice.

Quality Characteristics of Korean Red Ginseng Powder with Different Milling Methods (분쇄방법에 따른 고려홍삼분말의 품질특성)

  • 서창훈;이종원;도재호;김나미;양재원;장규원
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.32 no.3
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    • pp.370-374
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    • 2003
  • Cell cracking method using a non-collision was evaluated for the possibility of new red ginseng grinding technique. Based on particle size distribution analysis by 1size shaker, the ratios of 100 mesh penetrated particles were 94.9% for hammer mill (group A) and 95.6% for cell crack (group B). The ratio of 120 mesh penetrated particle of group A was higher than that in group B. The particle size distributions for 100 mesh non-penetrated Powder between 2 groups were not significantly different, and particle size distribution analysis by laser scattering analyzer showed that the particle size ranges were 0.77~128.07 ${\mu}{\textrm}{m}$ for group A and 4.24~180.07 ${\mu}{\textrm}{m}$ for group B. The Particle size distribution in group A was more broad than that in group B. The mean particle size in group B was larger than that in group A, while the standard deviation of particle size distribution in group B was less than that in group A. Structural surface characteristics, in group A, particle size distribution was broad and the distribution curve was amorphous. The structure of individual particles was similar to unequal stone which was roughly grinded and had soft cotton-like surface. In the contrary, in group B, particle size distribution was relatively narrow and also individual size particles were ubiquitously distributed. The structure of individual particles was unequal cut stone shape.

Breakage and Surface Oxidation Characteristics of Waste NdFeB Magnet for Recycling (NdFeB 자석 재활용을 위한 파분쇄 및 그에 따른 표면 산화 특성 연구)

  • Kim, Kwanho;Kim, Gahee;Lee, Hoon;Kang, Jungshin
    • Resources Recycling
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    • v.28 no.3
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    • pp.26-34
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    • 2019
  • Due to the increasing demand of rare earth magnet for various application, it is predicted that the amount of waste rare earth magnet will increase sharply. The process of waste rare earth magnet recycling is mainly consisted of leaching and separation of rare earth element contained in the magnet. However, there is no study on the breakage characteristics of the waste rare earth magnet for production of magnet powder. Therefore, in this study, effective crushing/grinding process and breakage characteristics were investigated for waste rare earth magnet. In the case of jaw crusher, the particle size of magnet was effectively reduced without rapid oxidation. In ball mill grinding test, it was found that the grinding process was not performed properly at the early stage of grinding. Moreover, waste rare earth magnet showed very low specific rate of breakage(S) and high fraction of fine particle breakage distribution(B) compared to ordinary minerals. These results can be used as a basic data for developing crushing/grinding circuit of waste rare earth magnet.

Effect of Heating Treatment of Silica Powder on Stirred Ball Milling Efficiency (규석 분말의 교반형 볼 밀 분쇄효율에 미치는 열처리의 영향)

  • 김병곤;박종력;최상근;이재장
    • Journal of the Korean Ceramic Society
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    • v.40 no.7
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    • pp.696-701
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    • 2003
  • The grinding efficiencies of silica powder in a small scale stirred ball mill were investigated by energy consumption estimate. Comparing with a non-treated silica powder and a heating treated silica powder, it was found that a silica powder cooled in room temperature after heating treatment at 600∼900$^{\circ}C$ consumed lower grinding energy than non-treated silica powder, and a silica powder quenched after heating treatment consumed lower grinding energies about 52∼62%, in case of dry grinding. Additionally, if heating treated silica powder grind in wet method, energy consumption will be decreased about 40% than in dry grinding, and the dependency of the particle size to the grinding efficiency, quenching significantly improved it.

Change in the Characteristics of Waste Activated Sludge after Pretreatment of Grinding, Freezing and Thawing (분쇄, 동결, 해동 등 전처리에 의한 하수슬러지의 성상 변화)

  • Seon, Yong-Ho
    • Journal of the Korea Organic Resources Recycling Association
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    • v.18 no.2
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    • pp.93-100
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    • 2010
  • In this study, ways to help anaerobic digestion were studied and waste activated sludge were pretreated by grinding, thawing after freezing and grinding after freezing. The volumes of grinding sludge, thawing after freezing and grinding after freezing were decreased 2.08 times, 3.37 times, 3.54 times compared to the volume of sludge respectively and the larger decline in the sludge has been grinding after freezing, thawing after freezing, and grinding. In addition, when the concentrations of SCOD, SBOD and protein were compared, the concentration of freezing sludge was higher than others and the grinding after freezing method seems to be the highest concentration. When the TS, VS removal rates were compared, thawing after freezing method seems to be higher than others method. From these results, grinding after freezing method is very effective for the pretreatment of sludge and it can be expected grinding after freezing method can be an alternative method for prohibiting ocean dumping of sludge after 2012.

Optimization of Process Variables for Grinding of Ibuprofen using Response Surface Methodology (반응표면분석법을 이용한 이부프로펜의 분쇄공정변수의 최적화)

  • Sim, Chol-Ho
    • Korean Chemical Engineering Research
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    • v.51 no.6
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    • pp.685-691
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    • 2013
  • Ibuprofen, non-steroidal anti-inflammatory drugs; NSAIDs, is a highly crystalline substance with the pharmaceutical properties of poor solubility and low bioavailability. The size reduction of ibuprofen is needed to improve the solubility. The objective of this study is to optimize the grinding condition of ibuprofen. Grinding of ibuprofen was carried out using a planetary mill. Grinding parameters were optimized using Box-Behnken experimental design method. The physical characteristics of ground ibuprofen were investigated for the particle size by particle size analyzer, for the crystal size by X-ray diffraction (XRD), and for the tensile strength by tensile/compression tester. The optimum conditions for the milling of ibuprofen were 290 rpm of the revolution number of mill, 24.6 g of the weight of sample, and 10 minutes of grinding time. The measured value of the particle size of ground ibuprofen at these optimum conditions was $13.5{\mu}m$. The results showed that the crystal size of ibuprofen was reduced by the planetary milling process. In case the relative density of the tablets formulated of ground ibuprofen was range of 0.85~0.90, the tensile strength of them was range of 1$2{\sim}14Kg_f/cm^2$.