• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2015년도 추계 학술논문 발표대회
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• pp.49-50
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• 2015

Recently, by-products from concrete industry are generated in large quantities because of urban redevelopment. Accordingly, waste concrete powder(WCP) inevitably generated in the course of crushing, screening, and separating the waste concrete also show high emission and be increasing gradually, but which is mostly buried with waste concrete aggregate. This is a basic research to increase the value added utilization rate of WCP. We have examined strength characteristic of extruding panel with WCP, depending on the curing methods. The result of study shows similar strength to the base specimen in autoclave curing condition. And in autoclave curing condition, the specimen with WCP of 20% and 30% satisfy the target strength of 14MPa.

• 한국응용과학기술학회지
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• 제24권3호
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• pp.246-252
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• 2007

$BaTiO_3$ powders were prepared by sol-gel method from different concentration of KOH aqueous solution and Ba/Ti molar ratio. Particle shape, size and crystal structure of prepared $BaTiO_3$ powders were analyzed by SEM, XRD, and FT-IR. As the result of KOH concentration changing, spherical particles were obtained by condition more than 3 M and particle size decreased as concentration increasing. Different appearance showed between dried and sintered powders against changing of Ba/Ti molar ratio. In case of dried powders, the crystallinity decreased as molar ratio increasing. On the other hand, increased as molar ratio increasing in case of sintered powders.

• 한국세라믹학회지
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• 제27권7호
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• pp.916-924
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• 1990

The preparatin of the fine TiN powders by reduction-nitridation of TiCl3-Al-N2 system was attempted in the temperature range from 350$^{\circ}$to 100$0^{\circ}C$. The formation mechanism and kinetics of TiN were examined, and the resultant TiN powder was characterized by means of XRD, PSA and SEM-EPMA methods. TiN was formed at temperatrue higher than $600^{\circ}C$. As an intermediate phase, AlTi was obtained. The apparent activation energy for the formation of TiN was approximately 4.2kcal/mole(600$^{\circ}$~90$0^{\circ}C$). The crystallite size and lattice constnat of TiN powder obtained in the temperature range from 600$^{\circ}$to 100$0^{\circ}C$ for 2h at the Al/TiCl3 molar ratio of 1.0 were 160~255A and 4.231~4.239A, respectively. According to PSA measurement, the mean particle size ranged from 14.0 to 14.8${\mu}{\textrm}{m}$.

• 대한기계학회논문집A
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• 제20권5호
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• pp.1458-1467
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• 1996

A direct differentiationmethod is presented for the shape design sensitivity analysis of axisymmeetric elastic solids. Based on the exisymmetric boundary integralequaiton formulation, a new boundary ntegral equatio for sensitivity analysis is derived by taking meterial derivative to the same integral identity that was used in the adjoint variable melthod. Numerical implementation is performed to show the applicaiton of the theoretical formulation. For a simple example with analytic solution, the sensitivities by present method are compared with analytic sensitivities. As an application to the shape optimization, an optimal shape of a gas turbine disc toinimize the weight under stress constraints is found by incorporating the sensitivity analysis algorithm in an optimizatio program.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2016년도 춘계 학술논문 발표대회
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• pp.55-56
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• 2016

In the recent concrete industry, when producing recycled aggregates, waste concrete powder is by-produced in large quantities; however, since it is not used properly but buried or discarded. This study is to apply the waste concrete powder to a cement extruding panel as filler. Flexural strength and microstructure characteristics of panel is tested in order to improve the economics of the extruding panel. As a results of this study, it was found that extruding panel replacing silica(No.8) as the waste concrete powder totally showed little difference in the strength and satisfied the target flexural strength of 14MPa, comparing with controlled panel. In addition, we can understand that rich Portlandite and Calcite contributed to develop the strength in all curing conditions from XRD pattern.

• 한국세라믹학회지
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• 제34권10호
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• pp.1009-1014
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• 1997

Ammonia gas was blown into the solution of zirconium ion to induce precipitation of supersaturated zirconium ion at gas-liquid interface with increase in pH. The influence of pH on the phase and particle size of precipitate and calcined powders has been investigated. At pH 4.5 of zirconium solution, maximum yield of 98.7% was obtained. Above pH 4.5, there was no more increase of yield. Above pH 5.5, large aggregates consisting of primary particles were observed in precipitate and calcined powders. At pH 4.5, almost aggregate-free fine spherical zirconia powders were obtained.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 1996년도 가을 학술발표회 논문집
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• pp.154-165
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• 1996

As II-anhydrite reacts with C3A(aluminate), C4AF(ferrite) at initial hydration of cement and assists the hydrolysis of C3S(calcium silicate), the production rate of ettringite(3C3A.3CaSO4.32H2O) and C-S-H gel was acclerated. It was known that compressive strength of cement concrete improved due to the effect of II-anhydrite. For the checking these effects of II-anhydrite, the fluidity and compressive strength of cementmortar admixed with II-anhydrite and pozollanic fine powders were investigated. By means of SEM analysis, the surface structure of mortar with the condition of steam curing at curing days=28 was investigated. As a result of this experiment, it was examined that II-anhydrite had an increase on the fluidity of cementpaste and compressive strength of mortar.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 1997년도 봄 학술발표회 논문집
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• pp.136-145
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• 1997

The purpose of this study is to develope of alternative adimixture for manufacture of PHC pile(compressive strength above 800kg/$\textrm{cm}^2$). For the investigation, properties of alternative admixture admixed with II-anhydrite and pozollanic fine powders(e.q., Fly-ash, Silica-Fume), the fluidity and viscosity in the cement pastes, the fluidity and compressive strength in mortars at steam curing condition, were respectively examined. Also, properties of compressive strength of concretes with exiting admixture(specimen name SM) and alterantive admixture(specimen name AP) for PHC pile, at steam and standard curing condition, were compared each other. As a result of this experimental study, it was found that specimens admixed with II-anhydrite and pozollanic fine powders had an increase on the fluidity of cement paste and mortar, and compressive strength of mortar and concrete was as good as concrete with SM.

• 한국세라믹학회지
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• 제26권2호
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• pp.179-186
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• 1989

The preparation of the fine BN powders by ammonia-nitridation of ammonia-decaborane derivate was attempted at temperature between 300 to 150$0^{\circ}C$. The formation mechanism of BN was examined and the resulant BN powder was characterized by means of IR, XRD, SEM and PSA method. In the nitridation below 80$0^{\circ}C$ bonding materials were identified with mainly BH and NH but above 80$0^{\circ}C$ with BN by IR spectra and X-ray patterns. Crystalite size, lattice constant and particle size distribution of hexagonal BN prepared at 1, 50$0^{\circ}C$ were La=470$\AA$, Lc=180$\AA$, a=2.5062$\pm$1$\AA$, c=6.8285$\pm$2$\AA$ and 2.0-5.4${\mu}{\textrm}{m}$, respectively.

• 한국세라믹학회지
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• 제28권1호
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• pp.67-73
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• 1991

Monodispersed PZT fine particles were obtained from the condition which 0.2Pb (OC3H7)2/EtOH, 0.108Zr(OC4H9)4/EtOH and 0.092 Ti (OC2H5)4/EtOH were refluxed for 5 hrs at 76$^{\circ}C$ and hydrolyzed with 0.1-0.4 H2O/EtOH. The monodispersed particle was amorphous and crystallized to the tetragonal PZT phase when heated at $600^{\circ}C$. Particle size was about 0.55${\mu}{\textrm}{m}$ in 0.3 H2O/EtOH and 0.3${\mu}{\textrm}{m}$ in other cases. Relative density of sintered body at 90$0^{\circ}C$ and 100$0^{\circ}C$ was 93.5% and 98%, respectively.