• Journal of the Korean Society of Clothing and Textiles
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• v.29 no.12 s.148
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• pp.1608-1618
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• 2005

The purpose of this investigation was to investigate the degradation products of the dye component extracted from madder dyed fabrics using the GC-MS analysis and to evaluate the change of color due to degradation treatment. Four different degradation protocols were used in this study,; refrigeration at $7^{\circ}C$ (LT), room temperature (RT), oven treatment at $100^{\circ}C$ (OV), and $H_2O_2/UV(PER)$ method. Degradation times for each thermal system were 6 hour, 24 hour, 48 hour, 1 week, 2 week, 4 week. Alizarin was detected from the control and degraded samples of both alizarin dyed and madder dyed fabrics. Benzoic acid, 2, 4-di-tert-butylphenol, phthalic anhydride were detected as the degradation products for both alizarin dyed and madder dyed fabrics. The result suggest that these products can be used as the fingerprints of GC-MS analysis for the identification of madder dye in archaeological textiles. Both alizarin dyed and madder dyed samples became less red and less yellow after degradation. In the PER degradation system madder dyed sample showed the greatest color difference even after 1 week of degradation treatment. Further research is necessary for investigating the color change in the exhumed textiles, which is caused by the dual action of dye fading and the staining of organic matters in the soil.

• Conservation Science in Museum
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• v.12
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• pp.9-17
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• 2011

This study examined non-destructive UV-Vis spectrophotometry as well as 3-D fluorescence spectrophotometry of textile that made use of red dye such as Sappan wood, madder, Safflower, Gromwell. The authors produced two textile specimen that were dyed by not only two kinds of textile (cotton and silk) but also three kinds of mordanting (no-mordanting, alumen and iron), and they investigated effects of each dye material upon investigation results. At analysis with UV-Vis spectrophotometry of dyed textile specimen, dyeing made by sappan wood, madder and gromwell had significant difference depending upon mardant regardless of kinds of textile, and safflower had no significant difference depending upon textile and mordant. At analysis with 3D-fluorescence spectrophotometry, specimen dyed with sappan wood had difference with mordants, and with madder, there were difference with textiles, and safflower had inherent fluorescence spectrum regardless of textiles and mordants, while gromwell had no fluorescence spectrum.

• Proceedings of the Korean Society of Dyers and Finishers Conference
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• 2006.04a
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• pp.290-293
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• 2006

• Korean Journal of Plant Taxonomy
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• v.40 no.2
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• pp.130-133
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• 2010

An unrecorded species of Oldenlandia brachypoda DC. is newly reported from Seogwipo-si, Jejudo, This species is distinguished from Oldenlandia diffusa, the related taxa by the surface and length of the pedicel, the number of flowerd, the shape of the calyx and capsule. The new Korean name 'je-ju-baeg-un-pul', was given considering the collect locality. The illustration, description and key of characters are provided.

• Journal of the Korean Society of Clothing and Textiles
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• v.27 no.11
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• pp.1350-1357
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• 2003

This research was aimed to establish the standard extraction and analytical procedures for examining the chromophoric substance in madder root with the ultimate goal of identifying the dyes in badly faded textiles of archaeological origin. The separation temperature of gas chromatography, pH and other extraction conditions were tested. The results were as follows: The suitable separation temperature for the GC cappillary column was 50∼305$^{\circ}C$, and methanol was a good GC solvent for both standard alizarin and madder extraction. The best extraction of madder was achieved by 90 min soaking in room temperature followed by filtration and the actual heat extraction procedure. The best pH for extracting alizarin was pH 3 and above pH 5 alizarin was not detectible. Only alizarin and no purpurin was found in the extraction of the currently used madder plant.

• Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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• 2009.04a
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• pp.175-180
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• 2009

• Korean Journal of Plant Resources
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• v.17 no.3
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• pp.297-303
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• 2004

This study was carried out to investigate into the dyeability of ramie fabrics using the extract of native plant, red-dye madder (Rubia akane Nakai) in different conditions. Surface color of ramie fabrics dyed with extracts from red-dye madder plants showed an order of descent YR. However, it was changed by the different mordants. Surface color of ramie fabrics treated with FeSO$_4$, SnCl$_4$, and tartaric acid was an order of descent Y, and that treated with the ashes of common camellia, and bean straw was an order of descent R. At higher temperatures, surface color and coloring matter concentration of ramie fabrics were as follows that values of a increased, however, values of b decreased and values of L lowered. Coloring matter concentration increased in the order of 7$0^{\circ}C$, 9$0^{\circ}C$, and 6$0^{\circ}C$, and so on. Dyeing colors on the ramie fabrics showed an order of descent Y by pH 4 and 9 in dyestuffs solutions. Coloring matter concentration in terms of K/S values, more or less, was increased at strong acids. Surface color by the concentration of dyestuffs solutions showed an order of descent YR irrelevant to the concentration of dyestuffs solutions. Coloring matter concentration was increased at higher concentrations of dyestuffs solutions. Ten minutes was sufficient for the dyeing of ramie fabrics in terms of surface color and coloring matter concentration.

• Proceedings of the Costume Culture Conference
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• 2004.04a
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• pp.44-46
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• 2004

심하게 퇴색된 출토 복식유물의 경우 유물의 고유색을 알지 못함은 물론 사용된 염료의 종류를 알지 못함으로 인하여 유물의 보존처리 및 장기간 보관과 전시에 큰 어려움을 지닌다. 이화학 분야에서는 미지시료의 기초 성분분석 방법으로서 thin layer chromatography(TLC)법이 오래 전부터 사용되었는데, 퇴색된 복식유물의 염료분석을 다룬 일부 선행연구에서는 이를 활용하여 유물의 염료를 판정하였다(Kharbade ＆ Agrawal, 1985; Schweppe, 1989). (중략)

• Journal of Fashion Business
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• v.11 no.4
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• pp.101-110
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• 2007

Since cotton fabrics with ripple finish treatment form wavy furrows on the surface or bumpy patterns, air circulation during wearing is good and the fabric is cool to the touch. The finishing principle is based on the mercerization, which utilizes the fact that cotton fibers contract in a concentrated NaOH solution. In this study, as fabric specimens, cotton fabrics with yarn counts of 40's, 60's and 80's were used. Concentrations of the NaOH solutions were 15%, 25%, and 35%. After dyeing fabrics using Rubia akane nakai, color and other properties were measured. As the concentration of the NaOH solution increased, the fabric became thicker and denser, and the number of occurrence of the prominence and depression per unit length became larger. The color of the region contracted by ripple finish became darker after dyeing, while the color of the untreated region became lighter, which enhanced the cubic effect of the ripple finish. As the count of the cotton yarn increased, the dyeability became better. As the concentration of the NaOH solution increased, the air permeability became lower.

• Journal of the Korean Society of Clothing and Textiles
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• v.26 no.9
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• pp.1301-1307
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• 2002

This paper surveys the mordanting and dyeing properties of Rubia akane Nakai appropriate extraction, dyeing and mordanting conditions of Rubia akane Nakai were determined, and the effect of mordanting method on dye uptake and color fastness of the dyed fabric was investigated. The optimum temperature to extract Rubia akane Nakai was during 1 hour in 8$0^{\circ}C$. The effective dyeing temperature and time of silk were 8$0^{\circ}C$, 1hour. The silk fabrics dyed with purpurin appeared red color, with alizarine appeared yellow-brown and with Rubia akane Nakai appeared yellow orange. K/S value of the dyeing fabrics was increased by pre-mordanting treatment. Mordant as Sn and Fe was better than anything else in K/S value. Mordanting treatment method affected color change of the dyed silk. In the case of Rubia akane Ntkai light fastness was increased by Fe and Al mordant treatment, Perspiration fastness of Rubia akane Nakai appeared more than 3 grades geneally. Fastness of abrasion and dry-cleaning appeared mon than 4～5 grades and these fastness improvement were generally effective for post-mordanting treatment.