• Title/Summary/Keyword: 광도측정

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Comparisons of sample preparation (acid digestion and microwave digestion) and measurement (inductively coupled plasma mass spectrometry and graphite furnace atomic absorption spectrometry) in the determination of bone lead (골중납 측정의 시료 전처리 (산분해법과 마이크로웨이브 분해법)와 측정 방법 (유도결합 플라즈마 질량분석법과 흑연로 원자 흡수 분광 광도법)의 비교)

  • Yoon, Chungsik;Choi, Inja;Park, Sungkyun;Kim, Rokho
    • Analytical Science and Technology
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    • v.16 no.2
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    • pp.152-158
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    • 2003
  • This study was conducted to evaluate two sample digestion procedures and instrumental determination parameters for analysis of lead in bone. Amputated human legs were treated by acid digestion or microwave dissolution prior to spectrometric analysis. Inductively coupled plasma mass spectrometry (ICP-MS) and graphite furnace atomic absorption spectrometry (GF-AAS) were used for determining bone lead levels. Recovery efficiencies using standard reference material from acid digestion measured by ICP-MS were in good agreement with those of the certified value, but in cases of acid digestion by GF-AAS and microwave digestion by both two methods, recovery underestimated and overestimated, respectively. For the bone samples, the lead concentrations obtained by ICP-MS after acid digestionwere in good agreement with those by GF-AAS (correlation coefficient = 0.983), but GF-AAS gave systematically higher values than ICP-MS. While a good agreement between two analytical methods after microwave digestion was also obtained (correlation coefficient = 0.950), bone lead concentrations from microwave were relatively higher than those from acid digestion. In conclusion, the use of the simple nitric acid digestion procedure at an ambient temperature coupled to ICP-MS seems to be efficient for the determination of lead in bone in consideration for both the convenience and validity.

Stress Effects on Photosynthesis of Greenhouse Plants as Measured by the Fluorescence Method (형광분석법에 의한 시설재배작물의 광합성 Stress 측정)

  • U, Zang-Kual;Song, Sung-Jung;Hansen, Ute
    • Korean Journal of Environmental Agriculture
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    • v.13 no.2
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    • pp.183-190
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    • 1994
  • To assess the effects of plant stress by light, temperature, NaCl and soil moisture on photosynthetic activity, the fluorescence method was used for Chinese cabbage(Brassica perkinensis Rupr.), strawberry(Fragaria grandiflora Ehrh.) and citrus tree(Citrus unshiu Marc.). With decreasing the light intensity, Fv/Fm ratios of intact leaves of Chinese cabbage and strawberry increased significantly, indicating lower photochemical efficiency in PS II system, resulting in an inverse relationship with the photosynthetic activity. Chinese cabbage and strawberry that were grown at higher temperature had higher Fv/Fm ratios and photosynthetic activities, while those given high concentration of NaCl and having low soil moisture had lower values. Chinese cabbage more resistant to salt stress and requiring more water had a greater Fv/Fm ratio than strawberry. In citrus tree, Fv/Fm ratio was lower in the non-irrigated group than the irrigated one. From these results, the fluorescence method was found to be a useful tool which can be used to assess the degree of in vivo stress induced by various environmental factors.

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Polymer Waveguide Apodized Grating for Narrow-Bandwidth High-Reflectivity Wavelength Filters (협대역 고반사 파장 필터 구현을 위한 폴리머 광도파로 에포다이즈드 격자)

  • Lee, Won-Jun;Huang, Guanghao;Shin, Jin-Soo;Oh, Min-Cheol
    • Korean Journal of Optics and Photonics
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    • v.26 no.4
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    • pp.203-208
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    • 2015
  • Wavelength filters are essential components for selecting a certain wavelength channel of a WDM optical communication system. To realize wavelength filters with narrow bandwidth and high reflectivity, an apodized grating structure with length of 15 mm and index modulation of $5{\times}10^{-4}$ was designed. The device exhibited a reflectivity of 95%, 3-dB bandwidth of 0.28 nm, and 20-dB bandwidth of 0.70 nm on an 18 mm grating length.

Polymer Waveguide Based Refractive Index Sensor Using Polarimetric Interference (편광 간섭을 이용한 광도파로 기반의 표면 굴절률 센서)

  • Son, Geun-Sik;Kwon, Soon-Woo;Kim, Woo-Kyung;Yang, Woo-Seok;Lee, Hyung-Man;Lee, Han-Young;Lee, Sung-Dong;Lee, Sang-Shin
    • Korean Journal of Optics and Photonics
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    • v.19 no.3
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    • pp.193-198
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    • 2008
  • A novel refractive index sensor, which consists of polymer channel waveguide overlaid with $TiO_2$ thin film, is demonstrated. To evaluate the fabricated sensor, we measured the polarimetric interference induced by concentration change of injected glycerol solution. Our experimental results show that thicker $TiO_2$ film improves the sensitivity of the polarimetric interferometer. For the fabricated waveguide with a 20 nm thick $TiO_2$ film, the measured index change to lead phase variation of $2{\pi}$ is $1.8{\times}10^{-3}$.

Fabrication and Characterization of an optical oxygen gas sensor formed on the planar optical waveguide prepared by ion exchang method (이온 교환법으로 제조된 평판형 광도파로의 산소광센서의 제작 및 특성평가)

  • 정채환;김재성;김원효;이병택;문종하;김진혁
    • Proceedings of the Optical Society of Korea Conference
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    • 2002.07a
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    • pp.178-179
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    • 2002
  • 최근에 화학, 임상병리, 환경 감시 등의 분야에서 산소센서의 수요가 점차 증가하고 있다. 이러한 산소 센서 중에 가장 많이 쓰이는 방식은 산화물 전극을 사용하는 amperometric 방법이지만 이 방법들은 장기간에 걸쳐 볼 때 산화물 전극의 오염, 외부 자기장의 간섭 등의 제점 때문에 산소를 측정하는데 많은 어려움이 있다. (1) 따라서 최근에는 빛과 유기염료를 통하여 산소의 농도가 증가할수록 세기가 quenching이 되는 원리를 이용한 산소센서의 연구가 이루어졌다. (중략)

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Comparison of Cold Vapor Atomic Absorption Spectrophotometry Analysis and EPA Method 101A for Measurement of Mercury in the Flue Gas (배출가스중 수은 측정을 위한 환원기화 원자흡광광도법과 EPA Method 101A의 비교 연구)

  • 김경희;최양일;박일수;홍지형;차준석;석광설;김대곤
    • Proceedings of the Korea Air Pollution Research Association Conference
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    • 1999.10a
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    • pp.92-93
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    • 1999
  • 수은은 상온에서 액체상태로 존재하는 유일한 금속으로서, 증기압이 매우 높기 때문에 가장 쉽게 휘발될 수 있는 중금속이다. 다른 중금속들은 거의 입자 상태로 변환되기 때문에 전기 집진기 등과 같은 일반적인 입자 제어시설에서 98%이상이 제거되지만, 증기압이 매우 높은 수은은 다단계 습식 스크러버, 활성탄을 사용하는 전기집진기/습식 스크러버가 결합된 특정한 방지시설에 없는 한 거의 대부분이 그대로 배출된다.(중략)

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Fabrication of a $LiNbO_3$ Single-Mode Optical Waveguide ($LiNbO_3$ 단일모드 광도파관의 제작)

  • 박동철
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.16 no.2
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    • pp.15-18
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    • 1979
  • Deposited film of a transition metal, Ti was diffused into LiNbO3 crystals to form integrated optical waveguides. By suppressing L O out -diffusion, single-mode waveguides could be constructed. Measurements on characteristics were performed by using the prise coupling technique and a He-Ne laser. ( λ = 0.6328 $\mu$m)

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Measurement of field-induced absorption changes in an electroabsorption waveguide using photocurrent (전계흡수형 도파로에서 광전류를 이용한 전계에 따른 흡수변화의 측정)

  • 강병권;박승한;최중길
    • Korean Journal of Optics and Photonics
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    • v.10 no.3
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    • pp.254-258
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    • 1999
  • We propose a simple technique to obtain field-induced absorption changes of an electroabsorption waveguide by using photocurrent generated inside a waveguide. Photocurrent proportional to the absorbed power and displaying Fabry-Perot interference fringes were observed and the field-induced absorption changes were derived from the ratio of resonant and anti resonant currents in the photocurrent spectra. The field-induced absorption change of InGaAsP waveguide for 1.5V reverse bias voltage at 1.55 $\mu\textrm{m}$ was determined to be $~157\cm^{-1}$.

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DR (Digital Radiography) 적용을 위한 Biology 초음파 특수용매를 이용한 $PbI_2$ 합성법

  • Kim, Seong-Heon;Yun, Min-Seok;O, Gyeong-Min;Kim, Yeong-Bin;Lee, Sang-Hun;Jo, Gyu-Seok;Park, Hye-Jin;Nam, Sang-Hui
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.11a
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    • pp.146-146
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    • 2009
  • 최근에 광도전체와 형광체를 기반으로 평판형 디지털 방사선 검출기의 상업적 발전가능성에 많은 관심을 가지고 있다. 본 연구는 기존의 직접변환방식에 널리 사용되었던 비정질 셀레늄 (amorphous selenium) 기반의 디지털 방사선 검출기보다 높은 전기적신호 및 동작특성을 가지는 물질층을 제작하기 위해 High Purity (99.99%)의 상용화된 $PbI_2$를 특수용매에 담가두었다가 약 1시간동안 Biology 초음파 처리한 후 농축기를 사용하여 건조된 $PbI_2$를 3Roll-milling을 사용하여 미세크기의 Powder를 얻어내었다. 합성된 $PbI_2$ Powder를 PIB(Particle-in-Binder)법을 이용하여 전도성을 가진 ITO(Indium-tin-oxide)코팅된 유리판에 제작된 필름의 상부에 Magnetron sputtering system 을 사용하여 전극을 $1cm{\times}1cm$의 크기로 증착하였다. I-V 테스트를 통하여 X선 조사시 $PbI_2$필름의 Sensitivity, Dark current, SNR(signal-to-noise ratio)을 측정하여 필름의 전기적 검출 특성을 정량적으로 평가하였고 SEM(scanning electron microscope)을 통하여 입자의 크기를 관찰하였다.

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AN ANALYSIS OF THE LIGHT AND RADIAL VELOCITY CURVES OF DO CAS (식쌍성 DO Cas의 광도곡선과 시선속도곡선의 분석)

  • 안영숙;김호일;이우백
    • Journal of Astronomy and Space Sciences
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    • v.17 no.2
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    • pp.181-188
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    • 2000
  • DO Cas is a short period (P=0.68day) eclipsing binary star and is classified as a near-contact binary by Shaw(1990). There is no published radial velocity curve for this short period binary after Mannino(1958). Hill(1991) suspected that Mannino's radial velocity curve had some serious mistake. So, we scanned the original plates used by Mannino with PDS and the spectra were employed to IRAF packages to estimate the radial velocities. The radial velocity curve and the BVR light curves made by us in 1998 were analyzed simultaneously with Wilson-Devinney code. We found that DO Cas is a contact or near-contact binary which the primary component fills its Roche lobe and we also estimated the absolute dimensions of each components of this system.

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