• Journal of the Microelectronics and Packaging Society
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• v.12 no.1 s.34
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• pp.87-93
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• 2005

Interfacial reactions between 48Sn-52In solder and $0.1{\mu}m$ Ti/3 ${\mu}m$ Cu/Au under bump metallurgies(UBM) with various Au thickness of $0.1{\~}0.7{\mu}m$ have been investigated after solder reflow at $150^{\circ}C,\;200^{\circ}C$, and $250^{\circ}C$ for 1 minute. Ball shear strength and shear energy of the Sn-52In solder bump on each UBM was also evaluated. With reflowing at $150^{\circ}C$ and $200^{\circ}C$, $Cu_6(Sn,In)_5$ and $AuIn_2$ intermetallic compounds were formed at UBW solder interface. However, UBM was consumed almost completely with reflowing at $250^{\circ}C$. While ball shear strength was not consistent with UBM/solder reactions, ball shear energy matched well with UBM/solder reactions.

• Korean Journal of Materials Research
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• v.6 no.5
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• pp.532-539
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• 1996

동과 동을 저온에서 단시간내에 접합시키는 가능성을 검토하기 위해서 직류 자기 스퍼터링을 이용한 코팅한 주석 및 주석-잡 합금층을 중간층으로 사용하였다. 접합은 대기중 200-35$0^{\circ}C$의 온도에서 수행되었고 접합온도에 도달직후 바로 냉각하였다. 접합 계면에는 액상의 주석과 고상의 동간의 반응에 의해 n-상(Cu6Sn5) 및 $\varepsilon$-상(Cu3Sn)으로 구성된 금속간화함물 층이 형성되었다. 전단강도로 측정된 접합강도는 접합온도에 따라 비례적으로 증가하지만 30$0^{\circ}C$ 이상에서 감소하였다. 접합강도는 2.8-6.2MPa 범위로 나타났으며, 중간층합금 성분에 따른 접합계면에서의 금속간화합물의 생성거동과 관련지어 설명되었다. 실험결과 실용적인 접합법으로서 저온 단시간 접합의 가능성이 확인되었다.

• Journal of the korean academy of Pediatric Dentistry
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• v.37 no.3
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• pp.298-307
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• 2010

The purpose of this study was to assess the effect on oxygen inhibition layer(OIL) for the interfacial bonding between resin composite layers, including shear bond strength, fracture modes and degree of conversion. The first layer of specimen was filled with Z-250(shade A3) and was cured for 40s. The second layer of specimen was filled with same composite(shade A1) and was cured for 40s. The first layer of specimens for each group were prepared by methods as followings. Control(curing in atmospheric air), Group1(curing against Mylar strip), Group2(scrubbed with a acetone-soaked cotton), Group3(using Tescera light cup), Group4(using Tescera heat cup), Group5(stored in disti1led water for 30days at $37^{\circ}C$), Group6 (using bonding agent). The results were as follows: 1. There was no statistically significant different shear bond strength between control and group 1(p>0.05). 2. Group 2 showed significantly lower shear bond strength than control and group 1(p<0.05). 3. The observation of the fracture surface leads to the evidence that a major difference occurs in the case of control, group1 and group 3 samples which break mainly cohesively while the other groups break in majority adhesively. 4. The results of FTIR showed that the degree of conversion was the highest in group 2 and the lowest in control group(p<0.05). It can be concluded that an OIL is not necessary for bonding with composite resin. But if a reduced critical amount of the unreacted monomer is present, it was detrimental to bonding additional layers of composite. Further study, such as the quantitative analysis of the unreacted monomer are required.

• The korean journal of orthodontics
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• v.28 no.4 s.69
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• pp.641-657
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• 1998

This study was undertaken to compare the bond strength and the fracture site of new and recycled brackets according to the base design. 252 sound premolars extracted for orthodontic treatment were collected and Type I, Type II, Type III brackets were divided into four groups by recycling method Each bracket was then bonded to an extracted premolar. Instron Universal Testing Machine(model W) was used to measure the shear bond strength, and the surface of the recycled brackets were viewed in SEM For the analysis of the results, one way ANOVA and Scheffe's multiple range test was executed using the SPSSWIN program. 1. The shear bond strength showed statistically significant difference according to the bracket base design(p<0.001). Type III bracket(round indentation base, micro-etched) showed the highest bond strength, Type I bracket(foil-mesh base) was second, and Type II bracket(grooved integral base, micro-etched) was last. 2. The effect of recycling on the bond strength was different according to bracket type. The shear bond strength of Type I, Type II brackets showed the smallist reduction when treated for 1 minute in Big Jane(p<0.05), but the shear bond strength of Type III brackets showed no statistically significant difference according to recycling method(p>0.05). 3. In Type I, Type II brackets, frequent fracture site was bracket-resin interface, but in Type III brackets, about half of the resin was retained on the tooth surface frequently. 4. The shear bond strength was highest when about half of the resin was retained on the tooth surface(p<0.05). 5. The resin remnant on the bracket base after recycling had no effect on the shear bond strength.

• Journal of Adhesion and Interface
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• v.23 no.4
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• pp.122-129
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• 2022

In this study, the hydrophilicity of the metal fiber is improved by introducing an oxygen-containing functional group to the fiber surface after treatment of the metal fiber using the oxygen plasma treatment time as an experimental variable. For the surface modification of metal fibers, changes in surface properties before and after plasma treatment were observed using SEM and x-ray photoelectron spectroscopy (XPS). In order to observe the effect of the plasma treatment time on the surface of the metal fiber, the change in contact angle of the metal fiber with respect to a polar solvent and a non-polar solvent was measured. After calculating the change in surface free energy using the measured contact angle, the contact angle and the surface free energy for metal fibers before and after oxygen plasma treatment were compared, and the correlation with the adhesion work was also considered. The microdroplet specimens were prepared to investigate the effect of surface changes of these metal fibers on the improvement of shear strength at the interface when combined with other materials and the interfacial shear strength was measured, and the correlation with the adhesion work was also identified. Therefore, the oxygen plasma treatment of the metal fiber results in an increase in the physical surface area on the fiber surface and a change in contact angle and surface energy according to the introduction of the oxygen-containing functional group on the surface. This surface hydrophilization resulted in improving the interfacial shear strength with the polymer resin.

• Proceedings of the Materials Research Society of Korea Conference
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• 2006.05a
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• pp.26.2-26.2
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• 2006

• Journal of the Korea institute for structural maintenance and inspection
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• v.25 no.6
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• pp.199-208
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• 2021

The extrudability of 3D printed concrete and its member strength can be highly influenced by water cement ratio (W/C) and printing time gap (PTG). In this study, mold cast specimens and 3D printed specimens were fabricated with variables of W/C ratio and PTG, and their shear bond strength and interlayer surface moisture content were measured and analyzed. The test results showed that the shear bond strength is greatly influenced by the amount of interlayer surface moisture. It is thus recommended that proper amount of interlayer surface moisture with respect to PTG needs to be maintained to have a required interlayer shear bond strength. In addition, further research is required to estimate the effect of many environmental factors that can influence the interlayer surface moisture content.

• Journal of Dental Rehabilitation and Applied Science
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• v.24 no.3
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• pp.231-242
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• 2008

Purpose: The purpose of this study was to investigate the bond strength of the core-veneer interface in all ceramic systems. Material and Methods: The all ceramic systems tested with their respective veneer were IPS Empress 2 with IPS Eris, IPS e.max Press with IPS e.max Ceram and IPS-e.max ZirCAD with IPS e.max Ceram. Cores (N=36, N=12/group, diameter: 10mm, thickness: 3mm) were fabricated according to the manufacturer's instruction and cleaned with ultrasonic cleaner. The veneer(diameter: 3mm, thickness: 2mm) were condensed in stainless steel mold and fired on to the core materials. After firing, they were again ultrasonically cleaned and embedded in acrylic resin. The specimens were stored in distilled water at $37^{\circ}C$ for 1 week. The specimens were placed in a mounting jig and subjected to shear force in a universal testing machine(Z020, Zwick, Germany). Load was applied at close to the core-veneer interface as possible with crosshead speed of 1.00mm/min until failure. Average shear bond strengths(MPa) were analyzed with a one-way analysis of variance and the Tukey test(${\alpha}=.05$). The failed specimens were examinated by scanning electron microscopy(JSM-6360, JEOL, Japan). The pattern of failure was classified as cohesive in core, cohesive in veneer, mixed or adhesive. Results: The mean shear bond strength($MPa{\pm}SD$) were IPS e.max Press $32.85{\pm}6.75MPa$, IPS Empress 2 $29.30{\pm}6.51MPa$, IPS e.max ZirCAD $28.10{\pm}4.28MPa$. IPS Empress 2, IPS e.max Press, IPS e.max ZirCAD were not significantly different from each others. Scanning electron microscopy examination revealed that adhesive failure did not occur in any all ceramic systems. IPS Empress 2 and IPS e.max Press exhibited cohesive failure in both the core and the veneer. IPS e.max ZirCAD exhibited cohesive failure in veneer and mixed failure.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.30 no.8
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• pp.65-70
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• 2002

The brazing of duplex stainless steels which is an essential process for rocket engine manufacturing has been investigated on bonding phenomena and shear strength. The UNS32550 was used for base metal, and the MBF-50 was used for insert metal. Brazing was carried out under the various conditions (brazing temperature : 1473K, 1498K, holding time : 0, 0.3, 0.9, 1.8 ks). There were various phases in the joint because of reaction between liquid insert metal and base metal, In the early stage, BN is formed in the bonded interlayer and base metal near the bonded layer. Cr nitride is formed in the bonded interlayer. The amount of BN and Cr nitride decrease with the increase of holding time. Superior shear strength of 550MPa is obtained by restraining the formation of nitride.

• Proceedings of the KWS Conference
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• 2010.05a
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• pp.97-97
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• 2010

최근 자동차에서 경량화의 방안으로써 높은 강성을 요구하는 고장력강 사용이 증대 되고 있다. 그러나 고장력강은 저항 점용접 시 일반 강에 비해 높은 전류를 요구하며 계면파단 및 expulsion 발생이 용이하기 때문에 가용 전류 구간이 좁은 특성을 가진다. 많은 연구자들이 hold time, tempering 등의 process를 이용하여 고장력강의 저항 점용접성을 개선하고자 하였으나 생산 공정라인에 적용하기는 어려운 실정이다. 본 연구에서는 용접 공정 변수의 변화에 따른 용접성과 전극 형상 변화을 통한 고장력강 점 용접성 향상에 대한 연구를 실시 하였다. 고장력강의 점 용접성 비교하기 위해 표준 전극(S1)과 인위적으로 가공한 전극(M1)을 사용하였으며, 실험에 사용된 판재는 두께 1.4mm의 DP590이며, 그 결과 표준전극(S1) 보다 가공 전극(M1)의 가용 전류 구간이 0.5kA 정도 넓은 것으로 확인 되었다. 두 전극을 사용한 점용접 시험편들의 인장전단강도를 비교 해보면 표준전극(S1)을 적용한 점용접 시 인장전단강도는 KS B 0850 기준에 만족하나 계면 파단이 발생 하였다. 가공 전극(M1)을 적용한 점용접 시 인장전단강도는 규격 기준에 만족하나 버튼 파단이 발생 하였다. 두 전극을 적용한 점용접부 형상 및 용접부 온도 분포에대해 저항점용접 시뮬레이션 프로그램(SORPAS)을 이용하여 실험 결과 값과 비교 분석하였고 파단모드의 변화에 대한 원인 분석을 도출 하였다.