• Journal of the Korean Society for Heat Treatment
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• v.29 no.6
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• pp.264-271
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• 2016

The effect of the oxygen content and the annealing temperature on the tensile behavior of the Ti-1.5Al-3Fe-0.25Si-(0.1~0.5)O alloy was investigated. The tensile properties were dependent on the volume fraction of the microstructure constituents, i.e. the equixed ${\alpha}$, equixed ${\beta}$ and lamellar ${\alpha}$. The results showed that the O-partitioned equixed ${\alpha}$ had a much higher strength compared to the equixed ${\beta}$. The strength of the lamellar ${\alpha}$ increased with increasing the annealing temperature because the O content of the lamellar ${\alpha}$ increased. Ti-1.5Al-3Fe-0.25Si-0.3O alloy annealed to $900^{\circ}C$ where the volume fraction of lamellar ${\alpha}$ was the highest exhibited an excellent combination of the strength (1198.5 MPa) and ductility (27.5%). The effect of the lamellar ${\alpha}$ on the ductility was discussed.

• Proceedings of the KSME Conference
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• 2000.11a
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• pp.135-140
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• 2000

The characteristics of mechanical behavior were estimated for Ti-6Al-4V alloy with four kinds of microstructure prepared with heat treatments. For this study, impact test, tensile test and fatigue crack growth test were performed, and then compared mechanical properties on the four microstructures. Furthermore, for quantitative evaluation, fractal dimensions of crack pass were obtained using the box counting method. The main results obtained are summarized as follows. (1) The microstructures exhibited equiaxed microstructure, bimodal-microstructure and lamellar microstructure by heat treatment. (2) The impact absorbed energy and elongation is superior in the bimodal-microstructure, and the hardness and tensile strength are superior in the lamellar microstructure. (3) The fatigue crack growth rate is similar to all microstructures in the low ${\Delta}K$ region. The fatigue crack growth rate of equiaxed microstructure is fastest, and that of lamellar microstructure is lowest in the high ${\Delta}K$ region. (4) The fractal dimension D of lamellar microstructure is higher then that of the equiaxed microstructure and bimodal microstructure.

• Journal of the Korean Society for Heat Treatment
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• v.34 no.5
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• pp.218-225
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• 2021

In this study, damping capacities were comparatively investigated for Mg-9%Al alloy with as-cast (AC) and fully discontinuous precipitates (DPs) microstructures, respectively. The DPs microstructure was obtained by solution treatment at 678 K for 24 h, followed by furnace cooling to RT. The AC microstructure was typically characterized by partially divorced eutectic β(Mg₁₇Al₁₂) phase particles distributed along the α-(Mg) matrix cell boundaries. The DPs microstructure showed lamellar morphology consisting of α and β thin layers with various interlamellar spacings. The DPs microstructure had better damping capacity than the AC microstructure in the strain-amplitude independent region, while in the strain-amplitude dependent region, the damping behavior was reversed. In view of the microstructural features of AC and DPs, the lower concentration of Al in the α-(Mg) phase for the DPs microstructure and the lower β phase number density for the AC microstructure would be responsible for the higher damping capacities in the strain-amplitude independent and strain-amplitude dependent regions, respectively.

• Journal of the Korean Society for Heat Treatment
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• v.27 no.3
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• pp.115-120
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• 2014

Microstructural features were comparatively investigated in AZ91 (Mg-9%Al-1%Zn) and AZ91-0.5%Sn alloys, in order to clarify the reason for the enhancement in room temperature tensile properties by the addition of small amount of Sn in Mg-Al-based alloy. In as-cast state, the Sn-containing alloy showed increased YS, UTS and elongation than the Sn-free alloy. The microstructural examination revealed that various factors including finer cell size, reduction of lamellar (${\alpha}+{\beta}$) phase and morphological change of bulky ${\beta}$ phase from partially divorced shape to fully divorced shape, are likely to be responsible for the improvement in tensile properties for the Sn-containing alloy. It is noted that two alloys showed similar tensile properties after solution treatment. This implies that microstructural evolution related to the ${\beta}$ phase plays a key role in better tensile properties in the Sn-containing alloy.

• International Journal of Precision Engineering and Manufacturing-Green Technology
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• v.5 no.5
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• pp.605-612
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• 2018

This work investigates the relationships between the static mechanical properties of Ti-6Al-4V manufactured through selective laser melting (SLM) and post-process heat treatments, namely stress relieve, annealing and hot isostatic pressing (HIP). In particular, Ti-6Al-4V parts were fabricated in three different build orientations of X, Z, and $45^{\circ}$ to investigate the multi-directional mechanical properties. The results showed that fully densified Ti-6Al-4V parts with densities of up to 99.5% were obtained with optimized SLM parameters. The microstructure of stress relieved and mill annealed samples was dominated by fine ${\alpha}^{\prime}$ martensitic needles. After HIP treatment, the martensite structure was fully transformed into ${\alpha}$ and ${\beta}$ phases (${\alpha}+{\beta}$ lamellar). Within the realm of tensile properties, the yield and ultimate strength values were found statistically similar with respect to the built orientation for a given heat treatment. However, the ductility was found orientation dependent for the HIP samples, where a lower value was observed for samples built in the X direction.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.05a
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• pp.435-438
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• 2008

High temperature deformation of Ti-6Al-4V alloy with a lamellar colony microstructure was investigated by hot compression and torsion tests. The torsion and compression tests were carried out under a wide range of temperatures and strain rates with true strain up to 2 and 0.7, respectively. The processing maps were generated on the basis of compression and torsion test data and using the principles of dynamic materials modeling (DMM). The shapes of the strain-stress curves in alpha-beta region and processing maps obtained on the two different tests have been compared with a view to evaluate the effect of the microstructure evolution on the flow softening behavior of Ti-6Al-4V alloy with a lamellar colony microstructure.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.6 no.2
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• pp.58-66
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• 1997

Ti alloys, with the advantageous tensile strength/density ratio and the chemical stability, have been used widely in the aerospace and chemical engineering industries and their usages are still expanding in various industrial areas. In the automotive industry, because of their superior merits of weight reduction and fuel saving, Ti alloys are expected to be used as various part materials including connecting rods, engine valves, springs and retainers, which are all subjected to the fatigue loads. In this study, using Ti-3A1-2.5V, the effects of temperature and microstructure change on fatigue crack propagation has been investigated. Five different microstructures were tested at the temperatures of room temperature, 20$0^{\circ}C$, 30$0^{\circ}C$ and 40$0^{\circ}C$ under the same frequency 20Hz. Some of the conclusions obtained are as follows: (1)Microstructurally, the morphology of less $\alpha$-phase and finer lamellar structure of $\alpha$ and $\beta$-Ti showed better registance to the fatigue crack propagation. (2)Fatigue crack growth rate increased with test temperature.

• Journal of the Korean Society for Heat Treatment
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• v.33 no.5
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• pp.219-225
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• 2020

The objective of this study was to investigate the tensile properties and thermal conductivities of Mg9.3%Al alloy in as-cast state and heat-treated state consisting of fully discontinuous precipitates (DPs), respectively. The fully DPs microstructure was obtained by solution treatment at 405℃ for 24 h, followed by furnace cooling to RT. The as-cast alloy showed a partially divorced eutectic β(Mg₁₇Al₁₂) phase particles formed along the α-(Mg) cell boundaries. The DPs had various apparent (α+β) interlamellar spacings, which is related to different transformation temperatures during the furnace cooling. The DPs microstructure exhibited better tensile strength than the as-cast one, resulting from the higher value of elongation in response to its more homogeneous microstructure. It is noticeable that the DPs microstructure had 12.4% higher thermal conductivity in average than the as-cast one between RT and 200℃. The XRD analyses revealed that the lower Al concentration in the α-(Mg) matrix may well be responsible for the better thermal conductivity of the DPs microstructure.

• Journal of the Korean Society for Heat Treatment
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• v.34 no.6
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• pp.302-308
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• 2021

The aim of this study was to investigate the dependence of the hardness and thermal conductivity on the volume fraction of discontinuous precipitates (DPs) in the Mg-9.3%Al alloy with (α-(Mg)+DPs) dual phase structure. In order to obtain various DPs volume fractions, the alloy was solution-treated at 688 K for 24 h and then aged at 418 K for up to 144 h. The volume fraction of DPs increased from 0% to 63% with an increase in the aging time up to 72 h, over which, continuous precipitation was observed within the α-(Mg) grains. It is noticeable that the hardness and thermal conductivity of the alloy increased linearly with the volume fraction of DPs. The improved hardness and thermal conductivity with respect to volume fraction of DPs are closely associated with the higher hardness of the DPs with fine (α+β) lamellar structure and the lower Al concentration in the α phase layer of the DPs, respectively.

• Journal of the Korean Society for Heat Treatment
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• v.32 no.6
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• pp.256-262
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• 2019

The microstructural features and texture development by both hot rolling and hot forging in ${\gamma}-TiAl$ alloy were investigated. In addition, additional heat treatment after hot forging was conducted to recognize change of the microstructure and texture evolution. The obtained microstructural features through dynamic recrystallization after hot deformed ${\gamma}-TiAl$ were quite different because two kinds of formation process were occurred depending on deformation condition. However, analyzed texture tends to be random orientation due to intermediate annealing up to ${\alpha}+{\beta}$ region during the hot deformation process. After additional heat treatment, microstructure transformed into fully lamellar microstructure and randomly oriented texture was also observed due to the same reason as before. Tensile test at room temperature demonstrated that anisotropy of mechanical properties were not appeared and transgranular fracture was occurred between interface of ${\alpha}_2/{\gamma}$. As a result, it could be suggested that microstructural features influenced much more than texture development on mechanical properties at room temperature.