• Title/Summary/Keyword: $D_{32}$

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Preparation and Physical Properties of Stretch Fabrics Using with Poly(trimethylene terephthalate) Fiber (Poly(trimethylene terephthalate) 섬유를 이용한 신축성직물의 제조 및 물성)

  • Choi, Hee
    • Fashion & Textile Research Journal
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    • v.5 no.1
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    • pp.53-58
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    • 2003
  • The stretch fabrics were made by the use of PTT[Poly(trimethylene terephthalate)] fibers and changes in their physical properties were analysed. Tenacity and elongation of D-1(PTT DTY) yarn were 3.32 g/d and 50.4%, respectively, while these of D-2(PTT+CDP DTY) yarn were 2.46 g/d and 32.1%, respectively. The tenacity of PTT-1 and PET-1 fabrics was similar, but the elongation of PTT-1 and PET-1 fabrics was 75% and 44%, respectively. Thus, the elongation of PTT-1 fabric was two times higher than those of PET-1 fabric. In addition, the elastic recovery at 20% elongation of PTT-1, PTT-2 and PET-1 fabric was 85.0%, 80.5% and 60.0%, respectively, indicating that so PTT-1 fabric showed better elastic recovery. The light, wash, and abrasion fastness of PTT-1 and PTT-2 fabrics were above Grade 3, Grade 4-5, and Grade 4-5, respectively. Therefore, there was little effect of substance on the fastness.

Development of Multi Piezo Ink-Jet Printing System Using Arbitrarily Waveform Generator (임의 전압파형발생기를 이용한 다중 피에조 잉크젯 3D 프린팅 장비 개발)

  • Kim, Jung Su;Kim, Dong Soo
    • Journal of the Korean Society for Precision Engineering
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    • v.32 no.9
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    • pp.781-786
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    • 2015
  • Recently, studies of 3D printing methods have been working in various applications. For example, the powder base method laminates the prints by using a binding or laser sintering method. However, the draw back of this method is that the post process is time consuming and does not allow for parts to be rapidly manufactured. The binding method requires the post process while the time required for the post process is longer than the manufacturing time. This paper proposes a UV curing binding method with an integrated piezo printing head system. The optimization of an arbitrary waveform generation for the control of a UV curable resin droplet was researched, in addition to developed optimized UV curing processes in multi nozzle ink jet heads.

Molecular Docking, 3D QSAR and Designing of New Quinazolinone Analogues as DHFR Inhibitors

  • Yamini, L.;Kumari, K. Meena;Vijjulatha, M.
    • Bulletin of the Korean Chemical Society
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    • v.32 no.7
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    • pp.2433-2442
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    • 2011
  • The three dimensional quantitative structure activity relationship (3D QSAR) models were developed using Comparative molecular field analysis (CoMFA), comparative molecular similarity indices analysis (CoMSIA) and docking studies. The fit of Quinazolinone antifolates inside the active site of modeled bovine dihydrofolate reductase (DHFR) was assessed. Both ligand based (LB) and receptor based (RB) QSAR models were generated, these models showed good internal and external statistical reliability that is evident from the $q^2_{loo}$, $r^2_{ncv}$ and $r^2_{pred}$. The identified key features enabled us to design new Quinazolinone analogues as DHFR inhibitors. This study is a building bridge between docking studies of homology modeled bovine DHFR protein as well as ligand and target based 3D QSAR techniques of CoMFA and CoMSIA approaches.

Development of an Isolable Active Ester, Diethyl Thiophosphoryl [(Z)-(2-Aminothiazol-4-yl)-2-(Methoxyimino)acetate (DAMA) for the Synthesis of Cefotaxime

  • Yoon, Man-Young;Lee, Hee-Bong;Shin, Hyun-Ik
    • Bulletin of the Korean Chemical Society
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    • v.32 no.2
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    • pp.407-410
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    • 2011
  • An isolable activated ester, diethyl thiophosphoryl [(Z)-(2-aminothiazol-4-yl)-2-(methoxyimino)acetate (9a, DAMA) was prepared in high purity, which was at least stable for 7 d at $25^{\circ}C$ and 6 months at $5^{\circ}C$. Its reaction with 7-ACA (4) in the presence of tributylamine in i-PrOH provided cefotaxime (1) of high purity in good yield. Preparation of DAMA and its reaction with 7-ACA (4) to 1 was performed in one-pot manner, respectively with minimal unit operations of stirring and filtration.

Evaluation of HIC/SSCC Resistance for API-X70 Pipe Manufactured by JCO Bending Process and SA Welding (JCO 밴딩과 SA용접으로 제조된 API-X70급 강관의 HIC/SSCC 저항성 평가)

  • Ryoo, Hoi-Soo;Kim, Hee Jin;Lee, Dong-Eon
    • Journal of Welding and Joining
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    • v.32 no.5
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    • pp.1-6
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    • 2014
  • This study aims at manufacturing SA welded API-X70 line-pipe with sour gas resistance. A pipe was manufactured by JCO bending process and SA welding using the API-X70 plate guaranteed HIC resistance. SA welded pipe was expanded in order to reduce the residual stress. The evaluation of a pipe for resistance to HIC and SSCC were performed by the RS D 0004 and RS D 0005 standards. For verification that a pipe has acceptable resistance to HIC, fullscale test was carried out. Results showed no cracking for the HIC and SSCC.

Gd-complexes of DTPA-bis(amide) Conjugates of Phosphonated Tranexamic Esters as MRI Contrast Agents

  • Patel, Mehul A.;Kim, Hee-Kyung;Lee, Gang-Ho;Chang, Yong-Min;Kim, Tae-Jeong
    • Bulletin of the Korean Chemical Society
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    • v.32 no.3
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    • pp.1022-1026
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    • 2011
  • The syntheses of DTPA-bis(amide) conjugates of phosphonated cyclohexane moieties (5a-d) and their Gd(III) complexes of the type $[Gd(L)(H_2O)]{\cdot}nH_2O$ (6a-d; L = 5a-d) are described. All new compounds have been characterized by microanalysis and spectroscopic techniques. High $r_1$ relaxivities of aqueous solutions of 6a-d are observed to be in the range of $10.7-18.3\;mM^{-1}sec^{-1}$, which compare much better than that of $Omniscan^{(R)}$ ($r_1=3.90\;mM^{-1}sec^{-1}$).

Bio-Inspired Micro/Nanostructures for Functional Applications: A Mini-Review

  • Young Jung;Inkyu Park
    • Journal of Sensor Science and Technology
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    • v.32 no.1
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    • pp.31-38
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    • 2023
  • Three-dimensional (3D) micro/nanostructures based on soft elastomers have received extensive attention in recent years, owing to their potential and advanced applicability. Designing and fabricating 3D micro/nanostructures are crucial for applications in diverse engineering fields, such as sensors, harvesting devices, functional surfaces, and adhesive patches. However, because of their structural complexity, fabricating soft-elastomer-based 3D micro/nanostructures with a low cost and simple process remains a challenge. Bio-inspired designs that mimic natural structures, or replicate their micro/nanostructure surfaces, have greatly benefited in terms of low-cost fabrication, scalability, and easy control of geometrical parameters. This review highlights recent advances in 3D micro/nanostructures inspired by nature for diverse potential and advanced applications, including flexible pressure sensors, energy-harvesting devices based on triboelectricity, superhydrophobic/-philic surfaces, and dry/wet adhesive patches.

Resource Allocation and Power Control for Device-to-Device Communication in LTE-Advanced Based on User Area Information (LTE-Advanced에서 단말간 직접 통신을 위한 영역 정보 기반 자원할당 및 전력 제어 기법)

  • Li, Xiang;Shin, Oh-Soon;Shin, Yoan
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.40 no.1
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    • pp.32-42
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    • 2015
  • In this paper, we considered the scenario that one cellular link and muti-D2D links share the same frequency resource which can improve the spectrum efficiency during uplink communication in LTE (Long Term Evolution)-Advanced network. In order to reduce the interference caused to the D2D users, we set DME (Discovery and Management Entity) which can send the area information to eNB(evolved Node B). We proposed a resource allocation scheme by using these assistant devices to reduce the interference that CUE (Cellular User Equipment) causes to DUE Rx (D2D UE Receiver). Basing on the area information, in order to mitigate the interference among the D2D pairs which share the same frequency resource, a power control scheme has been proposed. The simulation results prove that by using the DMEs, the proposed schemes improve the stability of D2D communication and bring the highest performance of the communication system when comparing to the other different schemes.

2D Correlation Analysis of Spin-Coated Films of Biodegradable P(HB-co-HHx)/PEG Blends

  • Kim, Min-Kyung;Ryu, Soo-Ryeon;Noda, Isao;Jung, Young-Mee
    • Bulletin of the Korean Chemical Society
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    • v.32 no.11
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    • pp.4005-4010
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    • 2011
  • We investigated thermal behavior of spin-coated films of P(HB-co-HHx)/PEG blends by using infraredreflection absorption (IRRAS) spectroscopy and 2D correlation spectroscopy. Based on 2D IRRAS correlation spectra, we could determine the sequence of spectral intensity changes with increasing temperature that PEG band changes first and then a band for crystalline component of P(HB-co-HHx) changes before a band for amorphous component. The intensities of bands for PEG and amorphous P(HB-co-HHx) were changed greatly as PEG weigh % of P(HB-co-HHx)/PEG blends increased. Transition temperatures of P(HB-co-HHx)/PEG blends were successfully determined by 2D gradient mapping method. The transition temperature of spincoated films of 98/2 and 90/10 P(HB-co-HHx)/PEG blends and 80/20 P(HB-co-HHx)/PEG blend determined by 2D gradient map are, respectively, about 137.5 and $132.5^{\circ}C$. Furthermore, P(HB-co-HHx)/PEG blends show an additional transition temperature that have been interpreted in terms of different lamellar thicknesses in spin coated films.

Electrochemical and Raman Spectroscopy Analysis for D- and L-Tryptophan-b-Cyclodextrin Inclusion Complexes

  • Jeong, Yu-Ra;Lee, So-Ra;Son, Pyeong-Soo;Choi, Seong-Ho
    • Journal of the Korean Applied Science and Technology
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    • v.32 no.3
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    • pp.451-460
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    • 2015
  • An enantioselective recognition of D- and L-tryptophan (Trp)-b-cyclodextrin (CD) inclusion complex was performed using electrochemical and FT-Raman spectroscopic analysis. From the electrochemical analysis, the selectivity coefficient ($K_{DL}$) of b-CD inclusion complexes was found higher than that of the D- and L-Trp in phosphate buffered saline (PBS, pH=7.0) solution. The percentage of enantioselectivity ($I_{%{ee}}$) for peak current of D-Trp-b-CD inclusion complexes was observed higher than that of L-Trp-b-CD inclusion complexes in PBS solution. From Raman spectroscopy, chemical shift difference (D, $cm^{-1}$) for the C=C stretch, ring vibration, and ring breathing of D-Try-b-CD inclusion complex were observed higher than that of L-Trp-b-CD inclusion complex. The electrochemical and Raman spectroscopic analyses were found very useful for chiral detection of racemic amino acid in the presence of b-CD.