• Title/Summary/Keyword: $^{11}C$ Beam

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An overview of new oxidation methods for polyacrylonitrile-based carbon fibers

  • Shin, Hye Kyoung;Park, Mira;Kim, Hak-Yong;Park, Soo-Jin
    • Carbon letters
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    • v.16 no.1
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    • pp.11-18
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    • 2015
  • The process of oxidizing polyacrylonitrile (PAN)-based carbon fibers converts them into an infusible and non-flammable state prior to carbonization. This represents one of the most important stages in determining the mechanical properties of the final carbon fibers, but the most commonly used methods, such as thermal treatment ($200^{\circ}C$ to $300^{\circ}C$), tend to waste a great deal of process time, money, and energy. There is therefore a need to develop more advanced oxidation methods for PAN precursor fibers. In this review, we assess the viability of electron beam, gamma-ray, ultra-violet, and plasma treatments with a view to advancing these areas of research and their industrial application.

Room Temperature Deposition and Heat Treatment Behavior of ATO Thin Films by Ion Beam Sputtering (이온빔 스퍼터링에 의한 ATO 박막의 실온 증착 및 열처리에 따른 특성변화)

  • 구창영;김경중;김광호;이희영
    • Journal of the Korean Ceramic Society
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    • v.37 no.11
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    • pp.1025-1032
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    • 2000
  • 산화분위기에서의 반응성 이온빔 스퍼터링법으로 Sn과 Sb 금속 타겟을 사용하여 실온에서 ATO 박막을 증착하였다. Sb 첨가량, 박막의 두께 및 열처리가 ATO 박막의 전기적 특성과 광학적 특성에 미치는 효과를 연구하고자 하였다. 제조된 ATO 박막의 두께는 약 1500$\AA$과 1000$\AA$으로 조절하였으며, Sb 농도는 10.8wt% 또는 14.9wt%임이 XPS 분석에 의하여 확인되었다. 증착한 박막의 열처리는 40$0^{\circ}C$~$600^{\circ}C$의 온도범위에서 산소 또는 forming gas(10% H$_2$-90% Ar) 분위기에서 30분간 수행하였다. 이렇게 제조된 ATO 박막은 Sb의 첨가량, 두께 및 열처리 조건에 따라 다양한 전기 비저항 값과 가시광선 대역에서의 광투과도를 나타내었다.

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Characteristics of Surface Hardened Press Die Materials by CO2 Laser Beam Irradiation (CO2 레이저 빔 조사에 의한 프레스 금형재료의 표면경화 특성)

  • Yang, Se-Young;Choi, Seong-Dae;Choi, Myeong-Soo;Jun, Jae-Mok
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.10 no.1
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    • pp.31-37
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    • 2011
  • Recently, the technology of surface treatment is being more important which affects the material cost reduction and substitution to the expensive material. The material used for the mechanical processing should have not only high intensity, but also strength toughness, wear resistance and corrosion resistance. In order to increase the durability and have better quality of the parts using such kind of tooling material, various kinds of research of the surface hardening through many kinds of heat resources is being done and practically applied. In this study, the characteristics of hardening surface zone for high strength of the press die material through laser beam irradiation are researched. In this study, it is experimentally observed by the status of the surface morphology, tensile strength, the hardness distribution of the base metal and wear condition by the surface hardness pattern by the laser beam based on the process parameters of $CO_2$ laser by using SM45C and STD11 used for press tool. Through this research, the characteristics of surface hardened zone for high strength of the thin metal by laser beam irradiation is done.

Liquid Crystal Alignment Effects on SiOx Thin Film by Electron Beam Evaporation Method (전자빔증착법을 통한 SiOx 박막의 액정 배향 효과)

  • Kang, Hyung-ku;Han, Jin-Woo;Kang, Soo-Hee;Kim, Jong-Hwan;Kim, Young-Hwan;Hwang, Jeoung-Yeon;Seo, Dae-Shik
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.18 no.11
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    • pp.1024-1027
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    • 2005
  • By using $45^{\circ}$ obliqued evaporation method with electron beam system, uniformly vertical liquid crystal (LC) alignment was achieved. And a high pretilt angles of about $2.5^{\circ}$ were measured. Also, it was verified that there are no variations of pretilt angle as a function of $SiO_x$ thin film thickness 20 nm and 50 nm. A good LC alignment states were observed at annealing temperature of $250^{\circ}C$. Consequently, the high pretilt angle and the good thermal stability of LC alignment by $45^{\circ}$ obliqued electron beam evaporation method on the $SiO_x$ thin film can be achieved.

Layer-by-layer Deposition of BSCCO Thin Films Using Ion Beam Sputtering Method (이온 빔 스퍼터법에 의한 BSCCO 박막의 순차 증착)

  • 박용필;이준웅
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.11 no.4
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    • pp.334-339
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    • 1998
  • $Bi_2Sr_2CuO_x$(Bi-2201) thin films have been fabricated by atomic layer-by-layer deposition using ion beam sputtering (IBS) method. During the deposition, 14 wt%-ozone/oxygen mixture gas of typical pressure of $5.0\times10^{-5}$ Torr is supplied with ultraviolent light irradiation for oxidation. XRD and RHEED investigations reveal that a buffer layer with compositions different from Bi-2201 is formed at the early deposition stage of less than 10 units cell and then Bi-2201 oriented along the c-axis is grown.

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Growth of Epitaxial AlN Thin Films on Sapphire Substrates by Plasma-Assisted Molecular Beam Epitaxy (플라즈마분자선에피탁시법을 이용한 사파이어 기판 위 질화알루미늄 박막의 에피탁시 성장)

  • Lee, Hyo-Sung;Han, Seok-Kyu;Lim, Dong-Seok;Shin, Eun-Jung;Lim, Se-Hwan;Hong, Soon-Ku;Jeong, Myoung-Ho;Lee, Jeong-Yong;Yao, Takafumi
    • Korean Journal of Materials Research
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    • v.21 no.11
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    • pp.634-638
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    • 2011
  • We report growth of epitaxial AlN thin films on c-plane sapphire substrates by plasma-assisted molecular beam epitaxy. To achieve two-dimensional growth the substrates were nitrided by nitrogen plasma prior to the AlN growth, which resulted in the formation of a two-dimensional single crystalline AlN layer. The formation of the two-dimensional AlN layer by the nitridation process was confirmed by the observation of streaky reflection high energy electron diffraction (RHEED) patterns. The growth of AlN thin films was performed on the nitrided AlN layer by changing the Al beam flux with the fixed nitrogen flux at 860$^{\circ}C$. The growth mode of AlN films was also affected by the beam flux. By increasing the Al beam flux, two-dimensional growth of AlN films was favored, and a very flat surface with a root mean square roughness of 0.196 nm (for the 2 ${\mu}m$ ${\times}$ 2 ${\mu}m$ area) was obtained. Interestingly, additional diffraction lines were observed for the two-dimensionally grown AlN films, which were probably caused by the Al adlayer, which was similar to a report of Ga adlayer in the two-dimensional growth of GaN. Al droplets were observed in the sample grown with a higher Al beam flux after cooling to room temperature, which resulted from the excessive Al flux.

Characteristics of Holographic Diffraction Grating Formation on $AS_{40}Se_{15}S_{35}Ge_{10}$ Thin Film with the Polarization State of Recording Beam (기록빔의 편광상태에 따른 $AS_{40}Se_{15}S_{35}Ge_{10}$ 박막에서 홀로그래피 회절격자형성 특성)

  • Park, Jeong-Il;Chung, Hong-Bay
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.55 no.9
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    • pp.423-428
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    • 2006
  • We have been carried out the two-beam interference method to form the diffraction grating on chalcogenide $AS_{40}Se_{15}S_{35}Ge_{10}$ thin films for Holography Data Storage (HDS). In the present work, we have been formed holographic diffraction gratings using He-Ne laser (632.8nm) under different Polarization state combinations (intensity polarization holography, phase polarization holography). It was obtained the diffraction grating efficiency by 11st order intensity and investigated the formed grating structure using Atomic Force Microscopy (AFM). As the results, it is shown that the diffraction efficiency of (P: P) polarized recording was maximum 2.4% and we found that its value was rather higher than that of other-polarized recordings. From the results, it is confirmed that the efficient holographic grating formation on amorphous chalcogenide $AS_{40}Se_{15}S_{35}Ge_{10}$ films depend on both the spatial variation of intensity and the polarization state of the incident field pattern.

Fabrication and Measurement of Tunable Millimeter-wave Filters (주파수 가변형 밀리미터파 필터의 제작 및 측정)

  • Park, Jae-Hyoung;Kim, Hong-Teuk;Kwon, Young-Woo;Kim, Yong-Kweon
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.49 no.11
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    • pp.627-634
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    • 2000
  • In this paper, new micromachined tunble bandpass filters for multi-band millimeter-wave telecommunication systems are proposed. Two types of mm-wave tunable filters are fabricated using micromachning technology and the responses of the filters are measured. One is two-pole lumped elements filter and the other two-pole resonators filter. Frequency tunability of the filter is achieved by changing the gap between a common CPW ground plate and the movable cantilever beam connected to the transmission line with the controllable renge of 2.5${\mu}m$. The deflection of cantilever beam is measured with the applied DC voltage. With the applied bias voltage from 0 to 50 V, the fabricated filters show 0.6 GHz(2.3%) at 26.6 GHz, and 0.8 GHz(2.5%) at 32 GHz center frequency shift for the lumped elements and resonators filter, respectively. The life time of the fabricated gold cantilever structure are tested.

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Active Vibration Control of a Composite Beam Using Piezoelectric Films (압전필름을 이용한 복합재료 외팔보의 능동진동제어)

  • Kim, S.H.;Choi, S.B.;Cheong, C.C.
    • Journal of the Korean Society for Precision Engineering
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    • v.11 no.1
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    • pp.54-62
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    • 1994
  • This paper presents active control methodologies to suppress structural deflections of a composite beam using a distributed piezoelectric-film actuator and sensor. Three types of different controllers are employed to achieve vibration suppression. The controllers are established depending upon the information on the velocity components of the structrue and on the deflection magnitudes as well. They are constant-amplitude controller(CAC), constant-gain mcontroller(CGC), and constant-amplitude-gain controller(CAGC). For the minimization of the residual vibration (chattering in a settled phase), which is the practical shortcoming of the conventional CAC dur to time delay phenomenon of the hardware system, a new control algoritym CAGCis designed by selecting switching constants in an optimal manner with respect to the initial tip deflection and the applied voltage. The experimental investigations of the transient and forced vibration control for the first vibrational mode are undertaken in order to compare the suppression efficiency of each control algorithm. Moreover, simultaneous controllability of various vibrational modes through the proposed scheme is also experimentally verified by pressenting both the transfer function and the phase.

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The Development of a 100 Mpa Class Ultra-high Strength Centrifugal Molded Square Beam Design and Manufacturing Technology (100MPa급 초고강도 원심성형 각형보의 설계 및 제작기술 개발 )

  • Doo-Sung Lee;Sung-Jin Kim;Jeong-Hoi Kim
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.27 no.4
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    • pp.11-22
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    • 2023
  • In this study, a structural concrete square beam was developed using the centrifugal molding technique. In order to secure the bending stiffness of the cross section, the hollow rate of the cross section was set to 10% or less. Instead of using the current poor mixture of concrete, a special formwork for producing a centrifugal square beam was manufactured, and a concrete mixing ratio with a high slump (150-200) and a design strength of 100 MPa or more was developed and applied. The produced centrifugally formed rectangular beams were subjected to performance tests according to the standard bending and shear test standards for centrifugally formed members. The static load test results for the four specimens exceeded both the nominal bending strength and nominal shear strength, which are design values through structural design, proving the structural reliability of the ultra-high-strength centrifugally formed square beam.