• Journal of the Korean Ceramic Society
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• v.26 no.1
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• pp.123-131
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• 1989

Hydroxyapatite powders were syntehsized by the reaction of Ca(NO3)2.4H2O and (NH4)2HPO4 in aqueous solution. The effect of the Ca/P mole ratio in the starting solution on the sintering of the powders and its microstructure was studied. When the Ca/P mole ratio in the starting solution was 1.69, the relative density of the sintered bodies was more than 95%. The sinterability was decreased as the Ca/P mole ratio in the starting solution was increased (Ca/P mole ratio >1.67). Hydroxyapatite sintered bodies obtained from the Ca/P mole ratio=1.69 had very excellent bending strength. The best bending strength was obtained at 110$0^{\circ}C$ and its value was 1220kg/$\textrm{cm}^2$. The average grain size was 0.277${\mu}{\textrm}{m}$. Most of sintered bodies were almost shown 100% hydroxyapatite phase. However, in case of the Ca/P mole ratio=1.64 hydroxyapatite was decomposed to $\alpha$-whitlockite above 120$0^{\circ}C$.

• Steel and Composite Structures
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• v.32 no.1
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• pp.127-139
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• 2019

Bridges, offshore oil platforms and other infrastructures usually require at some point in their service life rehabilitation for reasons such as aging and corrosion. This study explores the application of adhesively bonded CFRP patches in repair of corroded circular hollow sectional (CHS) steel beams. An experimental program involving three-point bending tests was conducted on intact, corroded, and repaired CHS beams. Meso-scale finite element (FE) models of the tested beams were developed and validated by the experimental results. A parametric study using the validated FE models was performed to examine the effects of different CFRP patch parameters, including patch dimensions, number of plies and stacking sequence, on efficiency of the repair system. Results indicates that the corrosion reduced elastic stiffness and flexural strength of the undamaged beam by 8.9 and 15.1%, respectively, and composite repair recovered 10.7 and 18.9% of those, respectively, compared to undamaged beam. These findings demonstrated the ability of CFRP patch repair to restore full bending capacity of the corroded CHS steel beam. The parametric study revealed that strength and stiffness of the repaired CHS beam can be enhanced by changing the fiber orientations of wet composite patch without increasing the quantity of repair materials.

• Journal of Korea Technical Association of The Pulp and Paper Industry
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• v.41 no.1
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• pp.17-23
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• 2009

The influence of different forming elements on the local paper structure and the related paper properties was investigated in this study. Specifically, a conventional papermaking foil system and a velocity induced drainage (VID) system were compared. The study involved the analysis of the product samples obtained from the commercial machine trials. The paper samples produced with VID forming systems showed better formation. The deterministic patter in the local structural profile map of the Foil samples indicated the structure of foil samples was more supple after forming process and then easier to be marked by various fabrics such as wet pressing fabric. The higher bulk was observed in the VID samples, which resulted in higher scattering coefficient, lower ZDT strength, and higher bending stiffness.

• Journal of the Korean Wood Science and Technology
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• v.25 no.1
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• pp.50-55
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• 1997

This study was carried out to utilize old newspaper(ONP) and paper sludge more effectively, and also to elucidate the influences of pressing conditions on the medium density fiberboard(MDF) properties. MDFs were made from ONP and low grade of paper sludge by wet process with change of pressing time, temperature and pressure. MDFs of ONP were more affected by pressing conditions, especially pressing pressure, but temperature and pressing time were also important. According to mixing paper sludge to ONP tensile and bending strength of MDF were decreased, but density and dimensional stability were improved. These results indicated that some physical properties of MDF can be improved by paper sludge and it is possible to use it in MDF.

• Journal of the Korean Wood Science and Technology
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• v.12 no.4
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• pp.12-18
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• 1984

Soaking treated in 20% aqueous solutions of $(NH_4)_2SO_4$, $NH_4H_2PO_4$, $(NH_4)_2HPO_4$, $Na_2B_4O_7-H_3BO_3$(60:40) and Minalith, the mixed salts for 9 hrs. the wet 3.5mm meranti (Parashorea spp.) plywoods were press-dried at 90, 120 and $150^{\circ}C$ and put to static bending test to examine the influence of redrying temperature on the strength of fire-retardant treated plywoods ill flexure. While water-soaking treatment (control) showed serious reduction in Stress at proportional limit, MOE, MOR, Work per unit volume at $150^{\circ}C$, all the fire-retardant treatments maintained bending strength even at $150^{\circ}C$ and showed rather increased values in case of some chemicals. In view of drying rate and maintenance of strength, the most pertinent platen temperature was $150^{\circ}C$ and Borax-Boric acid was the predominant fire-retardant in this study.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.16 no.8
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• pp.700-704
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• 2003

This paper describes on characteristics of 2" 3C-SiC wafer bonding using PECVD (plasma enhanced chemical vapor deposition) oxide and HF (hydrofluoride acid) for SiCOI (SiC-on-Insulator) structures and MEMS (micro-electro-mechanical system) applications. In this work, insulator layers were formed on a heteroepitaxial 3C-SiC film grown on a Si (001) wafer by thermal wet oxidation and PECVD process, successively. The pre-bonding of two polished PECVD oxide layers made the surface activation in HF and bonded under applied pressure. The bonding characteristics were evaluated by the effect of HF concentration used in the surface treatment on the roughness of the oxide and pre-bonding strength. Hydrophilic character of the oxidized 3C-SiC film surface was investigated by ATR-FTIR (attenuated total reflection Fourier transformed infrared spectroscopy). The root-mean-square suface roughness of the oxidized SiC layers was measured by AFM (atomic force microscope). The strength of the bond was measured by tensile strength meter. The bonded interface was also analyzed by IR camera and SEM (scanning electron microscope), and there are no bubbles or cavities in the bonding interface. The bonding strength initially increases with increasing HF concentration and reaches the maximum value at 2.0 ％ and then decreases. These results indicate that the 3C-SiC wafer direct bonding technique will offers significant advantages in the harsh MEMS applications.ions.

• Journal of the Korean Wood Science and Technology
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• v.23 no.2
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• pp.70-76
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• 1995

Research was conducted at the Wood Materials and Engineering Laboratory, Washington State University, Pullman, WA to evaluate the effects of the sequence of wax addition, wax level, and wax type on mechanical properties and water resistance performance of isocyanate-bonded particleboard. Mechanical properties and water resistance performance were not influenced significantly by the sequence of wax addition. Internal bond and wet modulus of rupture in bending strength were decreased significantly by increasing the wax emulsion level, but dry modulus of rupture and modulus of elasticity in bending strength were not decreased significantly by increasing the wax emulsion level. Dry internal bond, dry and wet moduli of rupture, and modulus of elasticity were not decreased by increasing the solid wax level except for wet internal bond. The addition of 1.0 and 1.5% wax level did not produce any significant additional water resistance effect when compared to the addition of 0.5% wax level. Internal bond values of boards with solid wax addition showed significantly better results than boards with just a wax emulsion added. Modulus of rupture, modulus of elasticity, and water resistance performance did not show significant difference between solid wax and wax emulsion.

• Journal of the Korean Wood Science and Technology
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• v.29 no.3
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• pp.47-58
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• 2001

For finding both ways of recycling the wood and plastic wastes and solving the problem of free formaldehyde gas emission through manufacturing wood particle-polypropylene fiber composite board without addition of formaldehyde-based thermosetting resin adhesive, control particleboards and nonwoven web composite boards from wood particle and polypropylene fiber formulation of 50 : 50, 60 : 40, and 70 : 30 were manufactured at density levels of 0.5, 0.6, 0.7, and 0.8 g/$cm^3$, and were tested both in the physical and mechanical properties according to ASTM D 1037-93. In the physical properties, control particleboard had significantly higher moisture content than composite board. In composite board, moisture content decreased with the increase of target density only in the board with higher content of polypropylene fiber and also appeared to increase with the increase of wood particle content at a given target density. Control particleboard showed significantly greater water absorption than composite board and its water absorption decreased with the increase of target density. In composite board, water absorption decreased with the increase of target density at a given formulation but increased with the increase of wood particle content at a given target density. After 2 and 24 hours immersion, control particleboard was significantly higher in thickness swelling than composite board and its thickness swelling increased with the increase of target density. In composite board, thickness swelling did not vary significantly with the target density at a given formulation but its thickness swelling increased as wood particle content increased at a given target density. Static bending MOR and MOE under dry and wet conditions increased with the increase of target density at a given formulation of wood particle and polypropylene fiber. Especially, the MOR and MOE under wet condition were considerably larger in composite board than in control particleboard. In general, composite board showed superior bending strength properties to control particleboard, And the composite board made from wood particle and polypropylene fiber formulation of 50 : 50 at target density of 0.8 g/$cm^3$ exhibited the greatest bending strength properties. Though problems in uniform mixing and strong binding of wood particle with polypropylene fiber are unavoidable due to their extremely different shape and polarity, wood particle-polypropylene fiber composite boards with higher performance, as a potential substitute for the commercial particleboards, could be made just by controlling processing variables.

• The Journal of Korean Academy of Prosthodontics
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• v.42 no.2
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• pp.142-153
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• 2004

Statement of problem: Increasing demand of esthetic restorations made lots of kinds of ceramic materials. Among them, zirconia has been being focused by many dentists. But, mechanical properties of zirconia were still unclear. Purpose : The purposes of this study were to analyze the flexural strength of various zirconia ceramics which had been currently used for clinic i.e., In-Ceram Zirconia(Vita Zahnfabrik, Bad $S\"{a}ckingen$, Germany), Celay Zirconia(Vita Zahnfabrik, Bad $S\"{a}ckingen$, Germany) and CAD/CAM Zirconia (Adens Zi-Ceram. Seoul , Korea). Material and methods: The four point bending test(ASTM Cl161) was used to measure the flexural strength of a specimen before and after circular heat treatment and fatigue loading. Results : 1. The average value of flexural strengths of CAD/CAM Zirconia, Celay Zirconia, In-Ceram Zirconia in dry condition were 806.5 MPa, 669.9 MPa, 605.6 MPa, respectively. There was a statistically significant difference in strength among the types (P<0.05). 2. After thermocycling, the average flexural strengths of CAD/CAM Zirconia, Celay Zirconia, In-Ceram Zirconia were 791.2 MPa, 604.2 MPa, 605.4 MPa, respectively. CAD/CAM Zirconia showed statistically significant higher strength(P<0.05). The others showed no significant difference after thermocycling(P>0.05). 3. After fatigue loading in wet condition. the average flexural strengths of CAD/CAM Zirconia, Celay Zirconia, In-Ceram Zirconia were 806.0 MPa, 674.9 MPa, 601.7 MPa, respectively. There was a significant difference in strength among the types(P<0.05). 4. There was no statistically significant difference in strength of the specimens according to experimental methods except for before and after thermocycling in Celay Zirconia(P>0.05). Conclusion: Besides high esthetic quality, zirconia had sufficiently high mechanical strength.

• Applied Chemistry for Engineering
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• v.8 no.6
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• pp.1000-1005
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• 1997

The properties of ceramics by solid-state reaction with hydroxyapatite[$Ca_{10}(PO_4)_6(OH)_2$], which was isolated from tuna bone by wet milling process were investigated. The bulk density $2.93g/cm^3$ at $1350^{\circ}C$ was close to the calculated density $3.21g/cm^3$. On X-ray measurements, the major phases were identified as hydroxyapatite at below $1300^{\circ}C$, but the whitlockite [$Ca_3(PO_4)_2$] phases were appeared due to a decomposition of hydroxyapatite with temperature. The microstructures of sintering specimens were shown as small closed pores between grain boundaries. The mean bending strength of the sintered hydroxyapatite by solid-state reaction is about 58 MPa and this value is higher than that of the articular cartilage maximum strength, 40MPa.