• 제목/요약/키워드: wet direct method

검색결과 103건 처리시간 0.028초

Processing of Porous Ceramics by Direct Foaming: A Review

  • Pokhrel, Ashish;Seo, Dong Nam;Lee, Seung Taek;Kim, Ik Jin
    • 한국세라믹학회지
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    • 제50권2호
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    • pp.93-102
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    • 2013
  • Macro porous ceramics possessing controlled microstructures and chemical compositions have increasingly proven useful in the industrial sphere. Their sintered structures have found application in both established and emerging, areas such as thermal insulation in buildings, filtration of liquids and molten materials, refractory insulation, bone scaffolds and tissue engineering. Stable ceramic foams can be formed by wet chemical methods using inorganic particles(e.g., $Al_2O_3$ or $SiO_2$). The wet foams are dried and sintered with improved porosity and mechanical properties. This review examines the different techniques used to prepare porous ceramics from ceramic foams, focusing on the explanation of this versatile method of direct foaming from the past to the present. Comparisons of the processes and the processing parameters are explained with the produced microstructures.

Transmission Electron Microscopy Specimen Preparation for Layer-area Graphene by a Direct Transfer Method

  • Cho, Youngji;Yang, Jun-Mo;Lam, Do Van;Lee, Seung-Mo;Kim, Jae-Hyun;Han, Kwan-Young;Chang, Jiho
    • Applied Microscopy
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    • 제44권4호
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    • pp.133-137
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    • 2014
  • We suggest a facile transmission electron microscopy (TEM) specimen preparation method for the direct (polymer-free) transfer of layer-area graphene from Cu substrates to a TEM grid. The standard (polymer-based) method and direct transfer method were by TEM, high-resolution TEM, and energy dispersive X-ray spectroscopy (EDS). The folds and crystalline particles were formed in a graphene specimen by the standard method, while the graphene specimen by the direct method with a new etchant solution exhibited clean and full coverage of the graphene surface, which reduced several wet chemical steps and accompanying mechanical stresses and avoided formation of the oxide metal.

Weathering durability of biopolymerized shales and glacial tills

  • Amelian, Soroosh;Song, Chung R.;Kim, Yongrak;Lindemann, Mark;Bitar, Layal
    • Geomechanics and Engineering
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    • 제28권4호
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    • pp.375-384
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    • 2022
  • The glacial tills and shales in Midwestern states of the USA often show strength degradation after construction. They are often in need of applying soil modification techniques to remediate their strength degradation with weathering process. This study investigated the weathering durability of these natural soils and biopolymer treated soils by comparing direct shear test results for wet-dry and wet-freeze-thaw-dry cycled specimens. The tests showed that untreated glacial tills maintained only 62% and 50% initial shear strength after eight wet-dry cycles and eight wet-freeze-thaw-dry cycles, respectively. These untreated soils could not withstand by themselves after 16 weathering cycles. The same soils treated with 1.5% (by dry weight) food-grade Xanthan gum maintained 140% and 88% initial shear strength of untreated soils after 16 weathering cycles for wet-dry cycles and wet-freeze-thaw-dry cycles, respectively. The same soils treated with 1.5% (by dry weight) Gellan gum maintained 82% and 60% initial shear strength of untreated ones after 16 weathering cycles, respectively. Similar results were obtained for crushed shales, manifesting that the biopolymerization method may be adopted as a new eco-friendly method to enhance the weathering durability of these problematic soils of glacial tills and shales.

분무방식에 의한 NFC(Nano-Fibrillated Cellulose)의 제지공정 적용 방안 탐색 연구 (Studies on Application of Spray of Nano-fibrillated Cellulose to Papermaking Process)

  • 이광섭;김창근;이재훈;이태주;류정용
    • 펄프종이기술
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    • 제47권4호
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    • pp.5-12
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    • 2015
  • In recent years, it had focused on the improvement of paper properties by addition of NFC (Nano-fibrillated Cellulose). Although the addition of NFC to wet-end of papermaking process could be suggested as a new solution to improve the strength properties of paper, it was not possible to avoid the bad drainage caused by the added NFC's chocking pores of wet web. Instead of the direct addition to wet-end, spraying of NFC to web in wire-section was tried in this study and evaluated by checking various paper properties including surface smoothness, tensile strength, folding endurance and stiffness. According to the increase of spraying amount of NFC, above mentioned paper properties were enhanced without excessive deterioration of drainage. Compared with direct introduction to wet-end, spraying could be regarded as a more proper method to enhance the surface smoothness and strength properties of paper.

2차원 유한요소해석을 위한 마름/젖음 알고리듬의 민감도 분석 (Sensitivity Analysis of Dry/Wet Algorithm for 2-Dimensional Finite Element Analysis)

  • 한건연;김상호;최승용;황재홍
    • 한국수자원학회:학술대회논문집
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    • 한국수자원학회 2009년도 학술발표회 초록집
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    • pp.827-831
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    • 2009
  • Recently, frequency occurring flood and drought has increased the necessity of an effective water resources control and management of river flows. Therefore, the simulation of the flow distribution in natural rivers is great importance to the solution of a wide variety of practical flow problems in water resources engineering. However The serious problem facing two-dimensional hydraulic model is the treatment of wet and dry areas. The objective of this study is to investigate the wet and dry parameters that have direct relevance to model performance in situations where inundation of initially dry areas occurs. Several numerical simulations were carried out, which examined the performance of the marsh porosity method for the purpose of sensitivity analysis. Experimental channel and a variety of channel were performed for model tests. The results were compared with those of the observation data and simulation data of existing model. The RMA-2 model displayed reasonable flow distribution compare to the observation data and simulation data of existing model in dry area for application of natural river flow. As a result of this study, effectively applied marsh porosity method provide a reliable results for flow distribution of wet and dry area, it could be further developed to basis for extending to water quality and sediment transport analysis.

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하천 및 습지에서 유한요소 해석시 마름/젖음 처리를 위한 매개변수 평가 (Parameter Assessment for the Simulation of Drying/Wetting in Finite Element Analysis in River and Wetland)

  • 최승용;한건연;김병현;김상호
    • 환경영향평가
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    • 제18권6호
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    • pp.331-346
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    • 2009
  • The serious problem facing two-dimensional finite element hydraulic model is the treatment of wet and dry areas. This situation is encountered in most practical river and coastal engineering problems, such as flood propagation, dam break analysis and so on. Especially, dry areas result in mathematical complications and require special treatment. The objective of this study is to investigate the wet and dry parameters that have direct relevance to model performance in situations where inundation of initially dry areas occurs. Several numerical simulations were carried out, which examined the performance of the marsh porosity method of RMA-2 model to investigate for application of parameters. Experimental channel with partly dry side slopes, straight channel with irregular geometry and Han river were performed for tests. As a result of this study, effectively applied marsh porosity method provide a reliable results for flow distribution of wet and dry area, it could be further developed to basis for extending to water quality and sediment transport analysis.

Occurrence of Weedy Rice as Affected by Cultural Practices

  • Kim, Sang-Yeol;Son, Yang;Ha, Woon-Goo;Park, Sung-Tae;Kim, Soon-Chul
    • 한국작물학회지
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    • 제43권2호
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    • pp.124-127
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    • 1998
  • Since weedy rice problems have emerged with the recent advent of direct seeding cultivation in Korea, the establishment of effective control strategies for weedy rice is considered to be one of the urgent issues to be solved for widely practiced direct seeding rice cultivation. A three year experiment was conducted to investigate the occurrence pattern of weedy rice in four different rice cultivation practices: high ridged dry seeding, wet drill seeding, water seeding, and machine transplanting. The highest weedy rice occurrence of 11.0% was observed in high ridged dry seeding practice followed by 9.6% in wet drill seeding, 6.4% in water seeding practice, and 0.2% in machine transplanting practice, respectively. The same trend was observed when we examine the occurrence of contamination of panicle and rice grain by weedy rice. More contamination was observed in high ridged dry seeding than any other practices. It was also found that the possible emergence depths from the soil surface was deeper in both in ridged dry seeding and wet drill seeding practice (0-5 cm from the soil surface) than those in water seeding (0-4 cm), and machine transplanting practice (0-3 cm). The highest yield reduction of 19.5% was observed in high ridged dry seeding practice followed by 13.0% in wet drill seeding, 6.3% in water seeding practice. The reduction may have occurred to the competition between weedy rice and cultivated rice, These findings suggest that among the four cultural practices examined, the machine transplanting practice is the most effective method to control and reduce the weedy rice occurrence and weedy rice seed in soil.

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3차원 소자 적층을 위한 BOE 습식 식각에 따른 Cu-Cu 패턴 접합 특성 평가 (Effect of BOE Wet Etching on Interfacial Characteristics of Cu-Cu Pattern Direct Bonds for 3D-IC Integrations)

  • 박종명;김수형;김사라은경;박영배
    • Journal of Welding and Joining
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    • 제30권3호
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    • pp.26-31
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    • 2012
  • Three-dimensional integrated circuit (3D IC) technology has become increasingly important due to the demand for high system performance and functionality. We have evaluated the effect of Buffered oxide etch (BOE) on the interfacial bonding strength of Cu-Cu pattern direct bonding. X-ray photoelectron spectroscopy (XPS) analysis of Cu surface revealed that Cu surface oxide layer was partially removed by BOE 2min. Two 8-inch Cu pattern wafers were bonded at $400^{\circ}C$ via the thermo-compression method. The interfacial adhesion energy of Cu-Cu bonding was quantitatively measured by the four-point bending method. After BOE 2min wet etching, the measured interfacial adhesion energies of pattern density for 0.06, 0.09, and 0.23 were $4.52J/m^2$, $5.06J/m^2$ and $3.42J/m^2$, respectively, which were lower than $5J/m^2$. Therefore, the effective removal of Cu surface oxide is critical to have reliable bonding quality of Cu pattern direct bonds.

습식 직접 합성법에 의한 Ni-Zn Ferrite의 합성 및 물성 연구 (Synthesis and Properties of Ni-Zn Ferrite by Wet-Direct Process)

  • 이경희;이병하;이융걸;황우연
    • 한국세라믹학회지
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    • 제28권3호
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    • pp.225-233
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    • 1991
  • In this study, we tried to find out the appropriate synthetic condition and magnetic properties of Ni-Zn ferrite {(NixZn1-x)Fe2O4} powders (where X=0, 0.1, 0.2, 0.3, ……0.9, 1). Ferrite powders were prepared by wet-direct method at 86℃ for 6hrs from FeCl36H2O, NiCl26H2O, and ZnCl2. The powders of (NixZn1-x)Fe2O4 (where X=0.4, 0.5, 0.6) have a good crystallinity, but the other ferrite powders consist of crystal and precursor ferrite. The ferrite powder's lattice constant is increased when ratio of ZnO contant is increased in the ferrite composition. And initial permeability was measured after sintering, result indicated regular pattern except (Ni0.4Zn0.6)Fe2O4 when the frequency were changed 10KHz to 10MHz.

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BaTiO3 습식직접합성 반응기구에 관한 연구 (Reaction Mechanism on the Synthesis of BaTiO3 by Direct Wet Process)

  • 이경희;이병하;김대웅
    • 한국세라믹학회지
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    • 제26권3호
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    • pp.371-380
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    • 1989
  • The purpose of this experiment is to elucidate the reaction mechanism concerning to the formation of crystalline BaTiO3 synthesized by adding the pH control agent(KOH soln) in TiCl4 and BaCl2 solution (Wet direct synthetic method). In this expeirment, it is identified that the amorphous barium-titanate having Ba-O-Ti bonding is formed above pH5 due to the -OH- ion and Ti-gel is formed below pH5 due to the polymerization of metatitanic acid. The bonding of the amorphous Ba-O-Ti is identified by FT-IR spectrum and crystallization temperature is about 82$0^{\circ}C$. If the pH of the above system according to the -OH- ion concentration is above 13.8, the polymerized metatitanic acid will be depolymerized and produce [TiO3]2+ion and crystalline BaTiO3 is formed by reacting the produced [TiO3]-- ion with the active Ba++ ion.

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