• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2014년도 추계학술대회 논문집
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• pp.286-288
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• 2014

This study deals with the catalyst free radio frequency plasma assisted polymerization of ethylene glycol using nitrogen as reactive gas to modify the surface chemistry and morphology. The deposited film was characterized through various analysis techniques i.e. surface profilometry, Forier transform infrared spectroscopy, water contact angle and UV-visible spectroscopy to analyze film thickness, chemical structure, surface energy and optical properties respectively. The surface topography was analyzed by Atomic force microscopy. It was observed that the ethylene oxide behaviour and optical transmittance of the film were reduced with the introduction of nitrogen gas due to higher fragmentation of monomer. However the hydrophilic behavior of the film improved due to formation of new water loving functional groups suitable for biomedical applications.

• 설비공학논문집
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• 제25권5호
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• pp.246-254
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• 2013

Some characteristics of nitrogen-water slug flow were optically measured, in vertical acrylic tubes of 2, 5 and 8 mm diameter. Bubble velocity, bubble and unit cell lengths were measured, by analyzing the light intensity signals from two sets of dot laser-infrared sensor modules mounted along the transparent tubes. Optical images of the bubbles were also taken and analyzed, to measure bubble shapes and liquid film thickness. It was found that the measured bubble velocities were in good agreement with the empirical models in the literature, except for those measured under high superficial velocity condition in the 2 mm tube. Bubble length was found to be the longest in the 2 mm tube, being 4 to 5 times those of the other tubes. Liquid film was found to have developed early in the 2 mm tube, which made the blunt shape of the bubble head. Liquid film thickness in the 8 mm tube was measured at almost twice those of the other tubes.

• 한국원자력학회:학술대회논문집
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• 한국원자력학회 1996년도 춘계학술발표회논문집(2)
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• pp.331-336
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• 1996

The effects of a mixing vane on air-water mixed flow have been experimentally studied in this work, to investigate the basic mechanisms that the mixing vane affects critical heat flux (CHF). Experiment was performed for various flow rates focusing on bubbly flow and annular flow patterns. Acrylic tube (1.7m long, 11 mm I.D.) and the split vane type mixing vane were used, and ring-type conductance probes were used to measure the liquid film thickness in annular flow. Experimental results show that, (a) bubbly-to slug flow transition and churn-to-annular flow transition occur respectively near the mixing vane compared to the tests without mixing vane, (b) in bubbly flow region, the mixing vane breaks the bubbles into smaller ones and forwards bubbles to the center region of the tube by the centrifugal force, (c) the liquid film thickness in annular flow is decreased near the mixing vane for mass fluxes.

• 한국해양환경ㆍ에너지학회지
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• 제2권1호
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• pp.34-39
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• 1999

Removal of spilled oil over the sea and the river has become one of the urgent problems in these days. Removing oil using mechanical devices by adhesion method is known to be closely related with the problem of estimating the thickness of film remaining on the surface of solid withdrawn from a quiescent liquid. In the present study a series of experimental results are compared with the analytic estimation for the thickness of film remaining on the solid surface using non-dimensional analysis. For the case of pure water both results show the remarkable agreement. However, discrepancy has been found for the case of Bunker C oil and diesel oil. The analytic estimation over-predicts the experimental value for the case of Bunker C oil and under-predicts it for the case of diesel oil. Further study is required to investigate the real situation including a contact angle and the property difference between oil and water.

• 한국재료학회지
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• 제15권5호
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• pp.285-292
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• 2005

Anti-reflection film was coated by using spherical silica nano colloids. Silica colloid sol was reserved between two inclined slide glasses by capillary force, and particles were convectively stacked to form a film onto the substrate as the water evaporates. As the sliding speed increased, the thickness of the film decreased and the wavelength at the maximum transmittance decreased. The microstructure observed by SEM showed that silica particles were nearly close packed, which enabled the calculation of the effective refractive index of the film. The film thickness was measured by proffer and calculated from the wavelength of maximum transmittance and the effective refractive index. The effective refractive index of the film could be controlled by a subtle controlling of the coating speed and by mixing two different sized silica particles. When the 100 nm and 50 m particles were mixed at 4:1-5:1 volume ratio, the maximum transmittance of $95.2\%$ for one-sided coating was obtained. This is the one that has increased by $3.8\%$ compared to bare glass substrate, and shows that $99.0\%$ of transmittance or $1.0\%$ of reflectance can be achieved by the simple process if both sides of the substrate are coated.

• 한국광학회지
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• 제33권4호
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• pp.159-166
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• 2022

본 연구에서는 이중 슬릿 회절 실험을 이용하여 박막의 두께와 굴절률을 측정하는 실험을 수행하였다. 투명 기판 위에 입혀진 박막이 만드는 투과광의 위상 단층의 크기를 이중 슬릿을 통과하여 나타나는 회절 패턴을 분석하여 측정하였다. 이로부터 두께와 굴절률을 동시에 결정하기 위해 공기와 증류수 속에서 각각 한 번씩 실험을 수행하였다. 이 방법의 유효함을 확인하기 위해 도파로 결합법으로 측정한 두께와 굴절률과 비교하였다. 본 연구에서 제안한 측정법은 기존의 선행 연구들과 더불어 박막의 두께와 굴절률을 동시에 측정할 수 있는 새로운 방법으로 응용될 수 있을 것으로 기대된다.

• 한국염색가공학회지
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• 제35권4호
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• pp.196-205
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• 2023

Water-dispersed pigment is on-going study for without air pollution in the textile and print industry. Primer treatment is essential for the substrate to improve the printing quality of eco-friendly water-dispersed pigment ink. Otherwise in the case of untreated primer, the water-dispersed pigment ink will dry onto the surface and cause defective images. This study was conducted on film substrate coating (primer) to fix eco-friendly water-dispersed pigment ink on film substrate. The drying, bleeding, and color strength of the pigment ink were examined depending on the composition and mixing ratio of the coating solution. The mixing ratio of silica gel in the coating film is increased to 0, 0.5, 1, 2 and 3 and results that DK-1-3 of silica gel ratio of 1 showed the lowest bleeding such as 52%, the letter thickness of 0.76mm and DK-1-5 of SG ratio of 3 showed the highest bleeding such as 304%, the letter thickness of 2.02mm. The mixing ratio of SPA in the coating film is increased to 2.5, 5, 7.5, SPA ratio of 7.5 has a bleeding ratio of 9% and letter thickness of 0.544mm. It showed the closest value to 0.5mm. According to the result, the optimal mixing ratio of binder, polymer coagulant, silica gel is 100:7.5:1.

• 한국자기학회지
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• 제11권3호
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• pp.97-103
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• 2001

Water-based 졸겔 증착법을 이용하여 디결정체 La$_{2}$3/Sr$_{1}$3/MnO$_3$(LSMO) 박막을 2000$\AA$ 두께의 열 산화층을 갖는 Si(100) 기판상에 제조하여 상온에서 LSMO박막의 두께변화 따른 저 자장영역(120 Oe)에서의 터널형 자기저항 변화를 연구하였다. XRD 회절분석 결과 단일상의 페롭스카이트 결정구조임을 알 수 있었으며 RBS 스펙트럼 분석결과 박막의 조성비 La:Sr:Mn:O는 0.67:0.33:1.0:3.0임을 알 수 있었다. LSMO 박막의 자성특성 측정결과 두께 증가에 따라 포화자화는 750$\AA$까지 급격한 증가현상을 보이다 150$\AA$을 기점으로 점차 감소하는 경향을 나타내고 있으며, 보자력은 800 $\AA$ 까지 급격한 증가를 보이다 일정해지는 경향을 볼 수 있었다. 저 자장영역에서의 터널형 자기저항 변화비는 약 1500 $\AA$의 두께 영역에서 최대값을 나타냄을 알 수 있었다. 이러한 저 자장 영역에서 LSMO 박막의 터널형 자기저항 변화비의 두께 의존성은 LSMO 박막과 Si 기판의 계면에 존재하는 상호확산 현상에 의한 dead layer의 존재 및 LSMO 박막의 열처리시 발생되는 열 격자 변형 효과로 설명하였다.

• 한국식품과학회지
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• 제28권3호
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• pp.545-551
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• 1996

카라기난을 사용하여 제조한 생분해성 필름의 분말식품에 대한 응용성을 조사하기 위한 연구의 일환으로 3종의 두께(0.05, 0.08, 0.11 mm)로 제작된 카라기난 필름을 사용하여 5가지의 온도(20, 25, 30, 35, $4^{\circ}C$)와 3가지의 상대습도(50, 70, 90%RH) 조건에서 수증기투과율을 측정하여 카라기난 필름의 투습 특성을 조사하였다. 카라기난 필름의 수증기투과율은 PE 필름보다 2.3배 정도 높았으며, 투습계수는 PE 필름보다 45-230배 정도 높아 수증기투과도가 높음을 알 수 있었다. 카라기난 필름의 투습계수는 다른 친수성의 가식성 필름과 마찬가지로 필름의 두께가 증가할수록 직선적으로 증가하는 경향을 보였다. 카라기난 필름의 투습계수는 온도에 대한 의존성을 나타내지 않았으나, 수증기투과율은 온도에 대한 의존성을 나타냈다. 카라기난 필름의 수증기투과율의 활성화 에너지는 필름의 두께에 따라 7.898-12.872 kj/mol의 값을 보였다. 카라기난 필름의 수증기투과율은 활성화 에너지 값이 커짐에 따라 지수앞인자의 값도 증가하는 kinetic compensation 현상을 나타냈다.

• 한국세라믹학회지
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• 제31권8호
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• pp.911-919
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• 1994

As the study for preparation of single-layer anti-reflective coating on glass, the conditions of synthesis of sol for coating and of reproducible coating procedure were investigated. In case of water-based sol, coating was impossible because of poor wettability of sol. The Substitution of solvent with ethanol improved the wettability of sol on the glass surface, and optimum amount of ethanol for substitution was 70 vol%. Maximum specific surface area and total pore volume of water-based sol were 268.7$m^2$/g and 0.315 cc/g, but after substitution, those values increased to 404.1 $m^2$/g and 0.376 cc/g, respectively. The upper limit withdrawl speed of coating in order to get clean coated films without aggregations or stains was 7 cm/min. In case of addition of 0.1 mol HNO3 and substitution with 70 vol% ethanol and heat-treatment at 40$0^{\circ}C$ for 1 hour, thin film with thickness of 94 nm was obtained at withdrawl speed of 4 cm/min. The thickness of thin film was independent of drying time.