• Title/Summary/Keyword: water curing

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Study on engineering properties of xanthan gum reinforced kaolinite

  • Zhanbo Cheng;Xueyu Geng
    • Computers and Concrete
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    • v.31 no.6
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    • pp.501-511
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    • 2023
  • The strengthening efficiency of biopolymer treated soil depends on biopolymer type, concentration ratio, soil type, initial water content, curing time and mixing method. In this study, the physical and mechanical properties of xanthan gum (XG) treated kaolinite were investigated through compaction test, Atterberg limit test, triaxial test and unconfined compression test. The results indicated that the optimum water content (OWC) increased from 30.3% of untreated clay to 33.5% of 5% XG treated clay, while the maximum dry density has a slight increase from 13.96 kg/m3 to 14 kg/m3 of 0.2% XG treated clay and decrease to 2.7 kg/m3 of 5% XG treated clay. Meanwhile, the plastic limit of XG treated clay increased with the increase of XG concentration, while 0.5% XG treated clay can be observed the maximum liquid limit with 79.5%. Moreover, there are the ideal water content about 1.3-1.5 times of the optimum water content achieving the maximum dry density and curing time to obtain the maximum compressive strength for different XG contents, which the UCS is 1.52 and 2.07 times of the maximum UCS of untreated soil for 0.5% and 1% XG treated clay, respectively. In addition, hot-dry mixing can achieve highest UCS than other mixing methods (e.g., dry mixing, wet mixing and hot-wet mixing).

Comparative analysis of strain according to the deposition of a constant temperature water bath of a denture-base artificial tooth produced using three-dimensional printing ultraviolet-curing resin (3D 프린팅용 광경화 수지를 사용하여 제작한 의치상용 인공치아의 항온수조 침적에 따른 변형률 비교 분석)

  • Kim, Dong-Yeon;Lee, Gwang-Young;Kim, Jae-Hong;Yang, Cheon-Seung
    • Journal of Technologic Dentistry
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    • v.42 no.3
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    • pp.202-207
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    • 2020
  • Purpose: This study is a comparative analysis of the strain according to deposition in a constant temperature water bath after manufacturing ultraviolet (UV)-cured artificial teeth. Methods: As a control group, 10 ready-made artificial teeth were selected as the first molar on the right side of the maxilla (RT group). Silicone was used as a duplicate of the artificial denture teeth. Experimental teeth were prepared in two groups using the prepared silicone mold. In the first experimental group, the UV-cured resin was injected into the negative silicone, followed by irradiation with a UV-curing machine for 5 minutes (5M group). In the second experimental group, the UV-cured resin was injected into the negative silicone, and then irradiated for 30 minutes using a UV-curing machine (30M group). The one-way ANOVA was performed, and post-test was analyzed by Tukey. Results: When immersed in a water bath for 15 days, it was found to be -0.3% in the RT group, -0.6% in the 5M group, and -0.7% in the 30M group. The results revealed -0.2% in the RT group, 0.2% in the 5M group, and -0.2% in the 30M group when they were in the bath for 30 days. Conclusion: In the water bath, the swelling was greater when deposited for 1 to 15 days, but was less when deposited for 15 to 30 days.

Evaluation of physical property and cytotoxicity of resin infiltrant based on a triethylene glycol dimethacrylate (TEGDMA)

  • Min, Ji-Hyun;Roh, Ji-Yeon;Kim, Ki-Rim
    • Journal of Korean society of Dental Hygiene
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    • v.19 no.2
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    • pp.173-181
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    • 2019
  • Objectives: The resin infiltration technique is a promising alternative therapy for arresting the early dental caries. However, there are very few reports on the safety and biocompatibility of this technique. We evaluated various properties of resin infiltrant (RI) based on a triethylene glycol dimethacrylate (TEGDMA).The water sorption (Wsp) and water solubility (Wsl) was assessed. Additionally, the cytotoxicity of RI against both animal and human fibroblast cell lines was investigated. Methods: The RI of the $Icon^{(R)}$, the first product developed for resin infiltration, is mainly composed of TEGDMA in the resin matrix. The Wsp and Wsl for the RI were measured in accordance with ISO 4049 specifications. Fourier-transform infrared spectroscopy (FTIR) was used for analyzing the polymerization before and after curing of RI. The cytotoxicity of RI against the mouse fibroblasts (L929) and human gingival fibroblasts (hTERT-hNOF) was evaluated using MTT [3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide] assay and the data were analyzed using one-way analysis of variance. Results: Wsp and Wsl of the RI specimens were $53.37{\mu}g/mm^3$ and $10.6{\mu}g/mm^3$, respectively. FTIR analysis revealed a slightly higher degree of curing with longer irradiation time. The degree of conversion for RI was high (80.9%) after 40 seconds of light curing. There was a significant decrease in the viability of L929 and hTERT-hNOF cells at RI extraction solution concentrations above 50%, respectively, compared to that in the negative control (p< 0.05). Conclusions: Even though the RI exhibited positive effect on the early prevention of dental caries, the clinicians should also consider the toxicity of RI on periodontal tissues.

Strength Property of Ternary System Non-Cement Matrix according to the Curing Method (3성분계 무시멘트 경화체의 양생방법에 따른 강도특성)

  • Lee, Jin-Woo;Lee, Sang-Soo
    • The Journal of the Korea Contents Association
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    • v.14 no.4
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    • pp.389-396
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    • 2014
  • This study was conducted as the basic research for the replacement of Blast Furnace Slag, Red Mud, Silica Fume, etc., with cement as a solution to the problems arising from the global warming caused by the generation of $CO_2$, and conducted the experimental review to examine the feasibility of matrix having properties identical to those of cement by using the Blast Furnace slag, Red mud, Silica fume, and alkali-activator. For this, by using the the inorganic binder, such as Blast Furnace Slag, Red Mud, Silica Fume, etc., and NaOH, $Na_2SiO_3$ and others as the cement substitute material, the strength characteristic according to the mixture time variation was performed in the tentative experiment. Based on the preceding experiment, this study performed the experiment to analyze the strength properties of hardener through the curing by air-dry temperature, curing by temperature in water, coating curing, and Korean paper curing. For the water curing at $80^{\circ}C$, the compressive strength and flexural strength were found to be the most excellent at the age of the 28th day, and furthermore, it was found that the non-cement hardener could be made, which is considered to affect the production of eco-friendly concrete.

A Study on Durability of High Strength Concrete (고강도(高强度)콘크리트의 내구성(耐久性)에 관한 연구(研究))

  • Kim, Saeng Bin
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.1 no.1
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    • pp.9-19
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    • 1981
  • Using superplasticizer or the methods of autoclave curing is the most typical and practical of the ways to make high strength concrete. In this study the high strength concrete piles by way of centrifugal forming and hand compacting, are put to the freezing and thawing test after the process of autoclave curing, water curing after steam curing, or stand water curing. And the relation of such piles to durability, the rate of strength decrease, and the rate of weight variation is shown. The durability of those test piles throughout freezing and thawing test proves to be comparatively sufficient in the above-mentioned curings when the piles contain a proper quantity of air. But it is also acknowledged that without A.E agent, the high strength concrete piles of autoclave curing is higher than those of the other curing in strength, but lower in modulus of dynamic elasticity and their durability factor after the test is much lower.

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An Experimental Study on Electromagnetic Properties in Early-Aged Cement Mortar under Different Curing Conditions (양생조건에 따른 초기재령 시멘트 모르타르의 전자기 특성에 대한 실험적 연구)

  • Kwon, Seung-Jun;Song, Ha-Won;Maria, Q. Feng
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.28 no.5A
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    • pp.737-746
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    • 2008
  • Recently, NDTs (Non-Destructive Techniques) using electromagnetic(EM) properties are applied to the performance evaluation for RC (Reinforced Concrete) structures. Since nonmetallic materials which are cement-based system have their unique dielectric constant and conductivity, they can be characterized and changed with different mixture conditions like W/C (water to cement) ratios and unit cement weight. In a room condition, cement mortar is generally dry so that porosity plays a major role in EM properties, which is determined at early-aged stage and also be affected by curing condition. In this paper, EM properties (dielectric constant and conductivity) in cement mortar specimens with 4 different W/C ratios are measured in the wide region of 0.2 GHz~20 GHz. Each specimen has different submerged curing period from 0 to 28 days and then EM measurement is performed after 4 weeks. Furthermore, porosity at the age of 28 days is measured through MIP (Mercury Intrusion Porosimeter) and saturation is also measured through amount of water loss in room condition. In order to evaluate the porosity from the initial curing stage, numerical analysis based on the modeling for the behavior in early-aged concrete is performed and the calculated results of porosity and measured EM properties are analyzed. For the convenient comparison with influencing parameters like W/C ratios and curing period, EM properties from 5 GHz to 15 GHz are averaged as one value. For 4 weeks, the averaged dielectric constant and conductivity in cement mortar are linearly decrease with higher W/C ratios and they increase in proportion to the square root of curing period regardless of W/C ratios.

Strength development of ground perlite-based geopolymer mortars

  • Celikten, Serhat;Isikdag, Burak
    • Advances in concrete construction
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    • v.9 no.3
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    • pp.227-234
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    • 2020
  • Raw perlite is a volcanic alumino-silicate and is used as aggregate in the construction industry. The high silica and alumina contained in the raw perlite allows the production of geopolymer mortar with the help of alkaline solutions. In this study, different geopolymer mortars are obtained by mixing ground perlite (GP), sodium hydroxide (NaOH), water and CEN standard sand and the strength and microstructure of these mortars are investigated. Mortar specimens are placed in the oven 24 hours after casting and kept at different temperatures and times, then the specimens are cured under laboratory conditions until the day of strength tests. After curing, unit weight, ultrasound pulse velocity, flexural and compressive strengths are determined. Experimental results indicate that the mechanical properties of the mortars enhance with increasing oven-curing period and temperatures as well as increasing NaOH molarity. In addition, SEM/EDS and XRD analyses are performed on the mortar specimens and the results are interpreted.

Preparation and Curing Studies of Maleimide Bisphenol-A Based Epoxy Resins

  • Nanjunda Gowda, Shivananda Kammasandra;Mahendra, Kadidal Nagappa
    • Bulletin of the Korean Chemical Society
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    • v.27 no.10
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    • pp.1542-1548
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    • 2006
  • Maleimide modified epoxy compounds were prepared by reacting N-(4-hydroxyphenyl) maleimide (HPM) with diglycidylether of bisphenol-A. Triphenylphosphine was used as catalyst and methylethylketone as solvent. The resulting compound possessed both the oxirane ring and maleimide group. The curing reaction of the maleimide epoxy compound with amine curing agents such as 1-(2-aminoethyl) piperazine (AEP) and 5-amino-1,3,3-trimethylcyclohexane methylamine isophorone diamine, IPDA) were studied. Incorporation of maleimide groups in the epoxy resin provides cyclic imide structure and high cross-linking density to the cured resins. The cured samples were found to have good thermal stability, chemical resistance (acid/alkali/solvent) and water absorption resistance.

An Experimental Study on Manufactural Technics of PHC Pile Using Low Pressure Steam Curing Method (상압증기양생방식에 의한 PHC PILE의 제조기술 연구)

  • 김종흡;안상기;이동근;심흥섭
    • Proceedings of the Korea Concrete Institute Conference
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    • 1994.10a
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    • pp.405-414
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    • 1994
  • The High Strength Concrete REsearch Team of the Dong-Ah Construction R&D Institute has achieved the preactical use of the PHC pile manufacture technique at the Dong-Ah Chang-dong PC Plant. Components of the high strength concrete are used high strength cement, admixtures(water reducing high range admixture, micro silion fume, fly ash, gypsum). The design strength required 800kg/$\textrm{cm}^2$ was developed raging from 870kg/$\textrm{cm}^2$ to 1010kg/$\textrm{cm}^2$. The new manufacture procedure of HPC pile which include placing, molding, steam curing is able to apply a current PC pile manufacture procedure easily without using the high pressure steam curing.

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Hydrothermal Reaction Characteristics on the ALC of Pitchstone-Lime System (II) - Effect of the Various Gelling and Curing Conditions (송지암-석회계 ALC에 대한 수열반응 특성(II) - 겔화 및 양생조건에 따른 영향)

  • 최병현;김순환
    • Journal of the Korean Ceramic Society
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    • v.31 no.2
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    • pp.194-200
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    • 1994
  • Pitchstone(Volcanic ejecta) reacts with CaO in hot water and increases its sedimentary volume by forming Ca(OH)2 and calcium silicate hydrates. ALC was prepared from the various gelling and curing conditions using the ratio of pitchstone/CaO was 2(CaO/SiO2 mol ratio=0.81), and then the products, crystalline phases and physical properties of ALC with experimental conditions was investigated. The crystalline phase of tobermorite with laths and plate type and the porosity were increased, the thermal conductivity was decreased with increasing gelling temperature and time. But modulus of rupture has maximum value when gelling time was 2 hrs. Othwrwise the bulk density nearly unchanged with increasing curing temperature, but the modulus of rupture was increased.

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