• 제목/요약/키워드: ultrasonic washing

검색결과 46건 처리시간 0.032초

비활성화된 상용 디젤 산화 촉매의 소형 디젤 기관에서 CVS-75 모드를 이용한 재제조에 관한 연구 (A Study on Remanufacturing of Deactivated Commercial Diesel Oxidation Catalyst by CVS-75 mode in Light Duty Diesel Engine)

  • 이창희;박해경
    • 한국분말재료학회지
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    • 제18권6호
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    • pp.517-525
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    • 2011
  • In this study, the used DOCs, which could remove the air pollutants such as CO and HC in the exhaust gas from diesel vehicle, were remanufactured by various conditions. Their catalytic performances and characterization were also investigated. The remanufacturing process of the deactivated DOCs includes high temperature cleaning of incineration, ultrasonic cleaning for washing with acid/base solutions to remove deactivating materials deposited to the surface of the catalysts, and active component reimpregnation for reactivating catalytic activity of them. The catalytic performance tests of the remanufactured DOCs were carried out by the diesel engine dynamo systems and chassi dynamo systems in CVS-75 mode. All prepared catalysts were characterized by the optical microscopes, SEM, EDX, porosimeter and BET to investigate correlations between catalytic reactivity and surface characteristics of them. The remanufactured DOCs at various conditions showed the improved catalytic performances reaching to 90% of fresh DOC, which is attributed to remove the deactivating materials from the surface of the used DOC through the analysis of catalytic performance test and their characterization.

염 보조 초음파 분무 열분해 공정으로 합성된 TiO2 나노입자의 특성에 열분해 온도가 미치는 영향 (Effect of Pyrolysis temperature on TiO2 Nanoparticles Synthesized by a Salt-assisted Ultrasonic Spray Pyrolysis Process)

  • 유재현;지명준;박우영;이영인
    • 한국분말재료학회지
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    • 제26권3호
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    • pp.237-242
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    • 2019
  • In this study, ultrasonic spray pyrolysis combined with salt-assisted decomposition, a process that adds sodium nitrate ($NaNO_3$) into a titanium precursor solution, is used to synthesize nanosized titanium dioxide ($TiO_2$) particles. The added $NaNO_3$ prevents the agglomeration of the primary nanoparticles in the pyrolysis process. The nanoparticles are obtained after a washing process, removing $NaNO_3$ and NaF from the secondary particles, which consist of the salts and $TiO_2$ nanoparticles. The effects of pyrolysis temperature on the size, crystallographic characteristics, and bandgap energy of the synthesized nanoparticles are systematically investigated. The synthesized $TiO_2$ nanoparticles have a size of approximately 2-10 nm a bandgap energy of 3.1-3.25 eV, depending on the synthetic temperature. These differences in properties affect the photocatalytic activities of the synthesized $TiO_2$ nanoparticles.

Effect of post-rinsing time and method on accuracy of denture base manufactured with stereolithography

  • Katheng, Awutsadaporn;Kanazawa, Manabu;Komagamine, Yuriko;Iwaki, Maiko;Namano, Sahaprom;Minakuchi, Shunsuke
    • The Journal of Advanced Prosthodontics
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    • 제14권1호
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    • pp.45-55
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    • 2022
  • PURPOSE. This in vitro study investigates the effect of different post-rinsing times and methods on the trueness and precision of denture base resin manufactured through stereolithography. MATERIALS AND METHODS. Ninety clear photopolymer resin specimens were fabricated and divided into nine groups (n = 10) based on rinsing times and methods. All specimens were rinsed with 99% isopropanol alcohol for 5, 10, and 15 min using three methods-automated, ultrasonic cleaning, and hand washing. The specimens were polymerized for 30 min at 40℃. For trueness, the scanned intaglio surface of each SLA denture base was superimposed on the original standard tessellation language (STL) file using best-fit alignment (n = 10). For precision, the scanned intaglio surface of the STL file in each specimen group was superimposed across each specimen (n = 45). The root mean square error (RMSE) was measured, and the data were analyzed statistically through one-way ANOVA and Tukey test (α < .05). RESULTS. The 10-min automated group exhibited the lowest RMSE. For trueness, this was significantly different from specimens in the 5-min hand-washed group (P < .05). For precision, this was significantly different from those of other groups (P < .05), except for the 15-min automated and 15-min ultrasonic groups. The color map results indicated that the 10-min automated method exhibited the most uniform distribution of the intaglio surface adaptation. CONCLUSION. The optimal postprocessing rinsing times and methods for achieving clear photopolymer resin were found to be the automated method with rinsing times of 10 and 15 min, and the ultrasonic method with a rinsing time of 15 min.

치과위생사의 감염관리 교육경험에 따른 감염관리 실태 (Infection control among dental hygienists according to infection control education experiences)

  • 김지현;김진경
    • 한국치위생학회지
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    • 제11권4호
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    • pp.547-556
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    • 2011
  • Objectives : The purpose of this study was to examine the relationship between the infection control education experiences of dental hygienists and the state of their infection control. Methods : The subjects in this study were the dental hygienists who worked in Seoul. The relationship of their infection control education experiences to their gender, marital status, academic credential, workplace, length of service, infection control implementation, experience of being exposed to infection, way of coping with it, hand washing, use of personal protection devices and equipment management was analyzed. Results : It is found that the variable to affect the state of infection control was educational experiences about handpiece water pipe management, ultrasonic scaler water pipe management and three-way syringe water pipe management. Conclusions : Dental hygienists who are one of major dental personnels should receive systematic education on infection control to acquire accurate knowledge to ensure the successful prevention of cross infection.

표면살균수 처리 후 진공포장된 신선편이 더덕의 저장 중 품질특성 변화 (Effect of Surface Sterilization on Quality of Vacuum Packaged Fresh-cut Deodeok (Codonopsis lanceolata) during Storage)

  • 최덕주;이윤정;김윤경;김문호;최소례;차환수;박형우;윤예리
    • 한국포장학회지
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    • 제18권1_2호
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    • pp.39-44
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    • 2012
  • 표면살균처리(초음파수, 염소수, 전해수) 후 PE 필름으로 진공포장 되어진 슬라이스 더덕의 저장 중 효과를 살펴보았다. 저장 초기에는 대조구에 비하여 표면살균처리된 신선편이 더덕은 총균수와 대장균군이 10배 이상 적게 측정되었다. 저장 20일 후 초음파수 처리구는 미생물뿐만 아니라 중량감모율, 부패율, 조직감과 표면색택이 대조구와 차이를 보이지 않을 정도로 품질이 저하되었다. Video microscope system을 이용하여 슬라이스더덕의 표면을 측정하였을 때 염소수와 전해수 처리구는 저장 10일까지는 초기와 큰 차이를 보이지 않았다. 그러나 저장 20일 후에는 슬라이스더덕 표면을 전해수 처리하여 PE필름으로 진공포장한 것이 조직감 뿐만 아니라 표면색의 갈변이 가장 적음에 따라, 저장 중 품질 유지에 가장 효과적인 것으로 나타났다.

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강산성차아염소산수와 초음파를 병용처리한 조미오징어 반가공품의 미생물 오염도 저감화에 관한 연구 (Study on Reduction of Microbial Contamination on Daruma by Combination Treatment of Strong Acidic Hypochlorous Water and Ultrasonic Waves)

  • 정원희;고준수;신일식
    • 한국식품위생안전성학회지
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    • 제30권2호
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    • pp.166-172
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    • 2015
  • 본 연구는 강산성차아염소산수(SAHW)와 초음파(UW)를 병용한 조미오징어 반가공품의 미생물 오염도 저감 기술을 개발하고자 수행되었다. SAHW의 유효염소농도는 $69.67{\pm}0.58ppm$, ORP는 $1071.33{\pm}4.16mV$, pH는 $2.79{\pm}0.05$이었다. 오징어 반가공품을 중량대비 20배의 SHS에 120분간 침지하였을 때 일반세균은 1.49 log CFU/g, 황색포도상구균은 1.32 log CFU/g 감소하였으며, 대장균은 검출한계 이하로 감소하였다. 오징어 반가공품 중량대비 10배의 SAHW에 120분간 침지한 경우, 일반세균은 2.69 log CFU/g, 황색포도상구균은 1.74 log CFU/g 감소하였으며, 20배의 SAHW에 120분간 침지한 경우, 일반세균은 3.62 log lCFU/g, 황색포도상구균은 3.22 log CFU/g 감소하였으며, 대장균은 검출되지 않아 SAHW가 같은 유효염소농도의 SHS보다 살균력이 높은 것을 알 수 있었다. SAHW 단독 처리만으로는 만족할 만한 미생물 저감효과를 얻을 수 없었기에 조미오징어 반가공품을 SAEW에 1차 침지 처리한 후, SAHW에 2차 침지 처리한 결과, 오징어 반가공품 중량 대비 20배의 SAEW로 60분 처리한 후, SAHW로 처리하였을 때는 중량대비 10배, 120분 처리, 중량대비 20배, 90분 처리로 일반세균수는 약 4.0 log CFU/g, 황색포도상구균은 규제치(log 2.0 CFU/g 이하) 이하로 감소하였으며 대장균은 검출되지 않았다. 초음파 세정기에 오징어 반가공품과 중량대비 20배의 TW, SHS, SAHW를 각각 넣어 UW 처리한 후 미생물 오염도를 조사한 결과, SAHW로 60분간 처리하였을 때 일반세균은 검출한계(< 1.00 log CFU/g) 이하로 감소하였으며 황색포도상구균은 규제치 이하로 감소하여 가장 좋은 저감효과를 나타내었다. 대장균의 경우, SAHW 10분간 처리로도 검출한계 이하로 감소하여 SAHW와 UW의 병용이 조미오징어 반가공품 미생물 저감화에 가장 효과가 좋은 것을 알 수 있었다.

촉매가 담지된 사용후 경유차 매연저감장치 DPF의 재제조 효과에 관한연구 (A Study on the Effectiveness of Remanufacturing Technology for the Catalyzed Diesel Particulate Filter-trap(DPF) Deactivated by Diesel Exhaust Gas)

  • 최강용;박해경
    • 대한환경공학회지
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    • 제32권10호
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    • pp.957-964
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    • 2010
  • 경유차 배출가스에 의해 활성이 크게 저하된, 촉매가 담지된 자연 재생식 매연 저감장치인 DPF를 대상으로 여러 가지 조건에서 재제조를 수행한 후 재제조된 DPF의 일산화탄소(CO)와 총 탄화수소(THC) 그리고 입자상 물질(PM)의 저감효율과 DPF 표면 물성 특성을 분석하여 사용후 DPF에 대한 재제조 효과를 관찰하였다. 재제조된 DPF에 대한 오염물질 저감성능 평가는 제작된 디젤 엔진 다이나모 장치를 이용, 배기가스를 일부 우회시켜 온도와 공간속도 조절이 가능한 촉매 반응장치로 수행 하였으며, DPF 표면 물성 분석은 광학현미경, EDX, ICP, TGA 그리고 porosimeter를 이용 하였다. 연구 수행 결과 사용 후 DPF를 본 연구에서 적용된 고온 배소 세정, 산성/염기성 용액에 의한 초음파 세정, 세정 후 촉매 활성성분 재 함침에 의한 재제조를 수행할 경우, 재제조된 DPF의 성능이 신품 성능대비 95% 이상으로 회복되는 것을 확인 하였으며, 광학현미경, EDX, TGA와 ICP등의 분석을 통해 본 연구 조건에서의 재제조 과정으로, DPF의 활성저하 원인이 되었던 각종 불순성분 대부분이 사용후 DPF 표면으로 부터 제거되는 것을 확인 하였다.

밀랍도포한지의 탈랍을 위한 최적 유기용매 추출기법 탐색 (Optimal Organic Solvent Extraction Method for Dewaxing of Beeswax-treated Hanji)

  • 최도침;최은연;조병묵;조병욱
    • 펄프종이기술
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    • 제44권6호
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    • pp.50-57
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    • 2012
  • In this study, the beeswax extraction methods using organic solvents were examined to develop a optimal dewaxing technology for beeswax-treated Hanji. Thermally-aged beeswax-treated Hanji was dewaxed using four types of extraction methods including dipping, Soxhlet extraction, ultrasonic washing and shaking methods. Then, the aging stability of the dewaxed Hanji was evaluated in terms of variations in paper strength and in the color of the printed area with muk. The experimental results suggested that the dewaxing methods allowing solvent to flow during extraction showed superior extraction efficiency. The dipping method in which the organic solvent does not flow showed the slowest extraction rate of beeswax compared to three other methods. In terms of variations in tensile strength and folding endurance, however, no obvious differences in the aging stability were observed amongst these four extraction methods. Regarding the aging stability in terms of the color of the printed area with muk, Soxhlet extraction method showed the best performance of dewaxing.

콜로니 픽킹 로봇 시스템의 개발 (II) - 로봇 시스템의 성능실험 - (Development of Robot System for Colony Picking (II) - Performance test of the robot system -)

  • 이현동;김기대;나건영;이영규
    • Journal of Biosystems Engineering
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    • 제28권5호
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    • pp.449-456
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    • 2003
  • A robot system was developed to pick desired colony. This robot system consisted of an image acquisition process which acquires the image information of colony, an illumination device which irradiates the object once when it gets the image of it, a picking head, a replicating head, a bed for fixing well-plates, and a sterilization device of sterilizing pin stained with colony. Picking pins were washed in an ultrasonic wave washing for takes ten seconds. Picking pins were dipped for sterilizing in alcohol for ten seconds. The time for resterilizing picking pins in a heater was five seconds. This performance test resulted 100% success rate for both the colony picking and the colony replication process. Considering the procedure in which 8 pins were smeared by colony, picked on a well plate, and sterilized as one cycle, the system could carry out one cycle in 110 seconds. It took about 138 minutes to pick around 600 colonies.

수용액 중 극미량 니켈(II)과 아연(II)의 흡착농축 및 ICP-AES 정량에 관한 연구 (Adsorptive Preconcentration and ICP-AES Determination for Trace Amount of Ni(II) and Zn(II) in Aqueous Solution)

  • 최종문;최선도
    • 한국환경보건학회지
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    • 제31권1호
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    • pp.73-78
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    • 2005
  • A determination method of trace Ni(II) and Zn(II) in aqueous solution was studied and developed by adsorbing on titanium dioxide. For this purpose, several conditions were optimized such as the pH of sample solution, adsorption time, the types and concentration acid, and desorption time. The titanium dioxide was added in sample solution which was pH adjusted. Then, the sample solution was stirred for 5 minutes. This mixture was stored in room temperature for 30 minutes to allow adsorption. After filtering and washing the titanium dioxide, the analytes were dissolved from the titanium dioxide on membrane filter by an ultrasonic vibration for 10 minutes in 1.0 M $HNO_3$ solution. Then, this sample solution was analysed using ICP-AES. The adsorption equilibrium was achieved in 30 minutes. The desorption was the most of effective with 1.0 M(mol/l) nitric acid solution, and desorption time was 10 minutes. This procedure was applied for the analysis of two real samples, i.e., brown seaweed and tangle. The recoveries of Ni(II) and Zn(II) in spiked samples were 89.4${\sim}$98.9% for analytes.