• Title/Summary/Keyword: ultrapure

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CHARACTERIZATIONS OF IDEAL WEAKLY \delta\theta-REFINABLE SPACES

  • Cho, Myung-Hyun
    • Bulletin of the Korean Mathematical Society
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    • v.36 no.1
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    • pp.33-45
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    • 1999
  • In this paper, we are interested in studying weak covering properties in the presence of a countable compact condition. The purpose of this paper is to characterize an ideal weakly $\delta$$\theta$-refinable space and to show that every ideal weakly $\delta$$\theta$-refinable space is isocompact. Also, we consider the behavior under mappings of ideal weakly $\delta$$\theta$-refinable properties and productivity of ideal weakly $\delta$$\theta$-refinable properties.

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Optimization of Extraction Process for Total Polyphenols from Angelica Using Response Surface Methodology (반응표면분석법을 이용한 안젤리카로부터 폴리페놀 성분의 추출공정 최적화)

  • Lee, Seung Bum;Park, Bo Ra;Hong, In Kwon
    • Applied Chemistry for Engineering
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    • v.29 no.3
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    • pp.325-329
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    • 2018
  • In this study, polyphenols were extracted from Angelica, which are known to have a high antioxidant content and the extraction process was optimized using the response surface methodology. The extraction yield and the total polyphenols were set as response values for the methodology. Quantitative factors in the extraction process were the extraction time, volume ratio of alcohol/ultrapure water, and extraction temperature. When considering both the main and interaction effects, the greatest influence factor on the extraction yield and total polyphenols was the extraction time. The optimum extraction time and temperature and alcohol/ultrapure water volume ratio for angelica were 2.8 h, $56.6^{\circ}C$ and 64.0 vol% respectively. The extraction yield and total polyphenols when using the conditions were calculated to be 24.6% and 8.76 mg GAE/g. respectively. Determination coefficients of regression equations for the extraction yield and total polyphenols were 81.4 and 75.4%, respectively. Also the overall satisfaction level was found to be 0.80 and the significance was confirmed within 5%.

Removal of Residual Antibiotics-Ciprofloxacin, Trimethoprim and Enrofloxacin-from Water by Ozone Oxidation (수중 미량 잔류항생물질 Ciprofloxacin, Trimethoprim, Enrofloxacin의 오존산화제거)

  • Han, Min-Su;Choi, Yeon-Woo;Song, Jun-Hyuck;Wang, Chang-Keun
    • Journal of Korean Society on Water Environment
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    • v.34 no.2
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    • pp.149-156
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    • 2018
  • Oxidation of Ciprofloxacin, Trimethoprim, and Enrofloxacin by ozone was experimentally investigated to observe the effects of background water quality (such as ultrapure water, humic acid, and biologically treated wastewater) and water temperature on the removal rate of these antibiotics, and, thereby, to be able to provide design information when the ozone treatment process is adopted. Initial concentrations of the antibiotics spiked to $10{\mu}g/L$, and the ozone dose was 1, 2, 3, 5, and 8 mg/L. While the removal rate of Ciprofloxacin under ultrapure water background by ozone oxidation was over 99%, the removal rate under humic acid and biologically treated wastewater background was markedly lower, in the range of 49.3% ~ 99% and 19.8 % ~ 99 %, respectively. When water temperature is decreased from $20^{\circ}C$ to $4^{\circ}C$, the removal rate is reduced from the range of 19.8% ~ 99 % to the range of 7.5 % ~ 99 % under a biologically treated wastewater background. The effects of background and temperature on the removal rate of Trimethoprim and Enrofloxacin were similar to that of Ciprofloxacin, but the degree was different. Therefore, it is concluded that the background of water to be treated, as well as water temperature, should be taken into consideration when the design factor, such as ozone dose, is determined, so that the treatment objective of the ozone treatment process can be most effectively met.

Extraction of Flavonoid Components from Persimmon Leaf, Thistle and New Green (감잎, 엉겅퀴, 뉴그린으로부터 플라보노이드성분의 추출)

  • Hong, In Kwon;Park, Bo Ra;Jeon, Gil Song;Lee, Seung Bum
    • Applied Chemistry for Engineering
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    • v.27 no.3
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    • pp.276-279
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    • 2016
  • In this study, we extracted active components from thistle, persimmon leaf, and new green which are known to have a high content of antioxidants and also analyzed the 1,1-Diphenyl-2-picrylhydrazyl (DPPH) radical scavening activity and flavonoid content. Both ultrapure water and alcohol were used as extraction solvents and the ratio of both solvents, sample, amunts extraction time, and extraction temperature were varied. The optimal extraction condition of each natural compounds were 2.5~3.5 h of the extraction time and 50 g/L of the sample amount. The optimal ratio of ultrapure water and alcohol and extraction temperature were as follows; persimmon leaf (55~65 vol%, $50{\sim}60^{\circ}C$), thistle (40~50 vol%, $55{\sim}65^{\circ}C$) and new green (55~65 vol%, $50{\sim}60^{\circ}C$). In addition, the antioxidant capacity and flavonoid content of the extract increased in the order of persimmon leaf, thistle, and new green.

Removal of Residual Antibiotics - Erythromycin, Sulfamethazine and Sulfathiazole - from water by Ozone Oxidation (수중 미량 잔류항생물질 Erythromycin, Sulfamethazine, Sulfathiazole의 오존산화제거)

  • Choi, Yeon-Woo;Han, Min-Su;Song, Jun-Hyuck;Wang, Chang-Keun
    • Journal of Korean Society of Water and Wastewater
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    • v.31 no.4
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    • pp.347-356
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    • 2017
  • Oxidation of erythromycin, sulfamethazine and sulfathiazole by ozone was experimentally investigated to see the effects of background water quality such as ultrapure water, humic acid and biologically treated wastewater and water temperature on the removal rate, consequently to provide design information when the ozone treatment process is adopted. Initial concentration of the antibiotics was spiked to $10{\mu}g/l$ and ozone dose was 1, 2, 3, 5, 8 mg/l. While the removal rate of erythromycin under ultrapure water background by ozone oxidation was over 99%, that under humic acid and biologically treated wastewater background was markedly reduced to the range of 59.8%~99% and 17.0%~99%, respectively. When water temperature is decreased from $20^{\circ}C$ to $4^{\circ}C$, the removal rate is reduced from the range of 17.0%~99% to the range of 9.4%~97.4% under biologically treated wastewater background. The effects of background and temperature on the removal rate of sulfamethazine and sulfathiazole were similar to erythromycin, but the degree was different. Therefore, it is concluded that the background of water to be treated as well as water temperature should be taken into consideration when the design factor such as ozone dose is determined to meet the treatment objective in the ozone treatment process.

Advances in electrodeionization technology for ionic separation - A review

  • Khoiruddin, Khoiruddin;Hakim, A.N.;Wenten, I.G.
    • Membrane and Water Treatment
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    • v.5 no.2
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    • pp.87-108
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    • 2014
  • Electrodeionization (EDI), which combines electrodialysis (ED) and conventional ion-exchange (IX), is a mature process which has been applied since more than twenty years on commercial use for the production of ultrapure water (UPW). Eliminating chemical regeneration is the main reason for its commercial success. The increase in acceptance of EDI technology has led to an installation of very large plant as the commercial state of the art that produces $1,500m^3/h$ of water for high pressure steam boiler. More recently, EDI system has found a number of new interesting applications in wastewater treatment, biotechnology industry, and other potential field. Along with further growth and wider applications, the development of stack construction and configuration are also become a concern. In this paper, the principle of EDI process is described and its recent developments, commercial scale, and various applications are pointed out.

Effects of CaO Impurity on Microstructural Evolution during Sintering of Alumina (알루미나의 소결 중 CaO 불순물의 미세구조에 미치는 영향)

  • 김상섭;백성기
    • Journal of the Korean Ceramic Society
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    • v.29 no.1
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    • pp.1-8
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    • 1992
  • The effect of CaO impurity on the microstructural evolution during the sintering of ultrapure alumina(>99.999%) was studied under "clean" firing conditions. The sinterability of undoped alumina was low, but its microstructure was maintained uniform. In the case of CaO-doped alumina, the distribution of grain size and that of grain boundary dihedral angle became wider, and facetted pores observed frequently. When MgO was doped in addition to CaO, the sinterability increased drastically and the uniform microstructural characteristics resumed. This study suggests that the effect of CaO is to induce inhomogeneous microstructures presumably by anisotropic segregation to grain boundaries and pore surfaces, and that MgO suppresses the anisotropic segregation of Ca.

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The Current of Ultrapure Water System (초순수 제조공정현황)

  • 이창소
    • Membrane Journal
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    • v.6 no.3
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    • pp.127-140
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    • 1996
  • 국내의 초순수 제조장치는 90% 이상이 이온교환수지를 사용하는 이온교환법과 UF, R/O System과 같은 Membrane을 사용하는 Membrane System을 병행하여 적용하고 있다. 국내 초순수처리 Plant에서는 통상 전처리 System과 1차 순수제조 System및 초순수 System이 상호 연결되어 Plant가 구성 운영되고 있다. 전처리 System에는 응집침전, 여과 흡착, 살균 등이 적용되고 있으며 여과 System에 Membrane을 적용할 수 있으나 국내에서는 특별한 경우를 제외하고 대부분 전처리 여과 System에 Media Filter를 사용한다. 전처리 System도 순수처리 장치의 전처리로는 없어서는 안되는 System이지만 여기에는 전처리 System을 제외하고 국내에서 적용하고 있는 초순수처리 System의 공정현황과 각 System별 특징을 설명하였다. 초순수 System에는 요구 수질에 따라 다소 차이가 있지만 반도체 공업에서 사용되는 초순수 System이 이중 최고의 Grade로 반도체공업에서 적용되고 있는 System을 기준하였다. 특히 Membrane을 적용한 초순수제조 System이 증가하고 있어 R/O, ED, EDR, CDI(EDI)와 같은 Membrane System의 특성과 원리를 검토하였다.

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Optimization of Iso-flavonoids Extraction Process from Kudge Using Ultrasonic Irradiation Energy (초음파에너지를 이용한 칡으로부터 이소플라보노이드의 추출공정 최적화)

  • Lee, Seung Bum;Kim, Su In;Hong, In Kwon
    • Applied Chemistry for Engineering
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    • v.29 no.5
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    • pp.503-509
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    • 2018
  • In this study, we used the ultrasonic extraction process as a method to extract antioxidant substances from kudzu, and measured the content of iso-flavonoids puerarin, daidzein, daidzin contained in kudzu. The response surface methodology which is a statistical analysis method for optimizing the extraction amount of iso-flavonoids from the kudzu and the process condition for maximizing the yield was applied. It is the final objective of this study to effectively derive the condition of the process that matches the target response with a minimum number of experiments and analyze the effect of each process condition on the response. In the response surface methodology, the central composite design was applied and the optimum condition was analyzed, and the three independent variables were set to ultrasonic irradiation time, volume ratio of ethanol/ultrapure water, ultrasonic irradiation power. Using the response surface methodology, the optimum conditions with the maximum extraction yield and the content of iso-flavonoids were evaluated as ultrasonic irradiation time (24.75 min), ethanol / ultrapure water volume ratio (39.75 vol%), ultrasonic irradiation power (592.36 W). The overall satisfaction level appears as high as 0.8938, which is recognized at a significance level within 5%. As a result of analyzing the optimization process, it was confirmed that the ultrasonic irradiation time is the factor that most affects the responses.

Optimization of Total Flavonoids Extraction Process from Wheat Sprout using Central Composite Design Model (중심합성계획모델을 이용한 밀싹으로부터 플라보노이드성분의 추출공정 최적화)

  • Lee, Seung Bum;Wang, Xiaozheng;Yoo, Bong-Ho
    • Applied Chemistry for Engineering
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    • v.29 no.4
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    • pp.446-451
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    • 2018
  • Effective ingredients were extracted using wheat sprout with high levels of flavonoids, and the extraction process was optimized with a central composite design model. The response value of the central composite design model establishes the extraction yield and the content of the flavonoids. The main and interactive effects were then analyzed depending on independent variables such as the extraction time, the volume ratio of alcohol to ultrapure water, and the extraction temperature. The extraction time and temperature were relatively large for the extraction yield. For the total flavonoids, the extraction time was most significantly affected. Considering both the extraction yield and the content of the total flavonoids, optimal extraction conditions were as follows: the extraction time (2.44 h), volume ratio of alcohol to ultrapure water (50.00 vol%), extraction temperature ($54.41^{\circ}C$). Under these condition, the extraction yield was 30.14 wt% and the content of the total flavonoids was $35.37{\mu}g\;QE/mL\;dw$. From the actual experimental result, the extraction yield under this condition was 29.92 wt% and the content of the total flavonoids was $35.32{\mu}g\;QE/mL\;dw$, which had an error rate of 0.39% and 0.74%, respectively. This is a multi-analysis comprehensive analysis that analyzes two simultaneous values of responses, but is considered to be highly accurate and also provides an excellent reliability of the optimization process in this study.