• Title/Summary/Keyword: ultra-filtration

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Non Thermal Process and Quality Changes of Foxtail Millet Yakju by Micro Filtration (미세여과에 의한 비 가열살균 좁쌀약주의 제조 및 저장 중 품질변화)

  • Kang, Young-Joo;Oh, Young-Ju;Koh, Jeong-Sam
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.34 no.2
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    • pp.277-284
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    • 2005
  • Micro-filtration (MF) or ultra-filtration (UF) system with hollow-fiber cartridge was introduced in order to improve the Quality level of commercial foxtail millet Yakju, which has an off-flavour and/or undesired colour after the thermal treatment. The filtration effects of cartridges such as MF (0.65, 0.45, 0.2, 0.1 $\mu$m) and UF (500 K dalton) were investigated. The physicochemical and sensory characteristics of the Yakju were then evaluated during the 6 months storage at room temperature. The exclusion ability of microorganism in samples was confirmed in all cartridges, but 0.45 pm MF-cartridge was suitable in the Yakju manufacture due to its superior filtration rate and efficiency. Changes in reducing sugar and colour difference of foxtail millet Yakju untreated or treated by heat ($65^{\circ}C$${\times}$10 min) were observed during the storage; after 6 months the L-value of thermal-treatment sample was decreased and its b-value, however, significantly increased so that its color became dark, in comparison to non-thermal treatment sample. This decrease of reducing sugar is assumed that color change is associated with non-enzymatic browning reaction. Sensory Quality of foxtail millet Yakju produced by non-thermal treatment was better than that of thermal treatment.

Characterization of Humic Acid in the Chemical Oxidation Technology(II) - Characteristics by Ozonation - (화학적 산화법에 의한 부식산의 분해처리 기술에 관한 연구(II) - 오존처리에 따른 분해특성 분석 -)

  • Rhee, Dong Seok;Jung, Young-Rim
    • Analytical Science and Technology
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    • v.13 no.2
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    • pp.241-249
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    • 2000
  • In this paper, ozonation of humic acid in water was characterized using $UV_{254}$ absorbance, TOC, Ultra Filtration and $^{13}C-NMR$. Also, carbonyl compounds in ozonated water were analyzed by GC/MS using PFBOA method. Ozonation by-products of water containing humic acid were determined as formaldehyde, acetaldehyde, acetone, glyoxal and methylglyoxal. Results of $UV_{254}$ absorbance and TOC with ozonation time at humic acid 20, 100ppm represent that decrease rate of 80% within ozonation time is 20 min and TOC removal rate of 40-50% within ozonation time is 30 min. Results for $^{13}C-NMR$ and Ultra Filtration, humic acid of high molecular weight by ozonation are oxidated and decomposed so that it was conversed low molecular weight such as aldehydes, carboxylic acid.

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Fabrication of Transparent Ultra-thin Single-walled Carbon Nanotube Films for Field Emission Applications

  • Jang, Eun-Soo;Goak, Jung-Choon;Lee, Han-Sung;Kim, Myoung-Su;Lee, Nae-Sung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.353-353
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    • 2008
  • Carbon nanotubes (CNTs) are attractive for field emitter because of their outstanding electrical, mechanical, and chemical properties. Several applications using CNTs as field emitters have been demonstrated such as field emission display (FED), backlight unit (BLU), and X-ray source. In this study, we fabricated a CNT cathode using transparent ultra-thin CNT film. First, CNT aqueous solution was prepared by ultrasonically dispersing purified single-walled carbon nanotubes (SWCNTs) in deionized water with sodium dodecyl sulfate (SDS). To obtain the CNT film, the CNT solution in a milliliter or even several tens of micro-litters was deposited onto a porous alumina membrane through vacuum filtration process. Thereafter, the alumina membrane was solvated by the 3 M NaOH solution and the floating CNT film was easily transferred to an indium-tin-oxide (ITO) glass substrate of $0.5\times0.5cm^2$ with a film mask. The transmittance of as-prepared ultra-thin CNT films measured by UV-Vis spectrophotometer was 68~97%, depending on the amount of CNTs dispersed in an aqueous solution. Roller activation, which is a essential process to improve the field emission characteristics of CNT films, increased the UV-Vis transmittance up to 93~98%. This study presents SEM morphology of CNT emitters and their field emission properties according to the concentration of CNTs in an aqueous solutions. Since the ultra-thin CNT emitters prepared from the solutions show a high peak current density of field emission comparable to that of the paste-base CNT emitters and do not contain outgassing sources such as organic binders, they are considered to be very promising for small-size-but-high-end applications including X-ray sources and microwave power amplifiers.

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Study on Removal of DOC for Effluent from Nitrification and Denitrification Process with Zeolite by Combined Process of Coagulation and UF Membrane (제올라이트를 첨가한 질산화 탈질공정에서 응집과 UF공정을 이용한 처리수내 용존 유기물질 제거 연구)

  • Han, Jang Hyuk;Yoon, Tai Il;Cho, Kyung Chul;Song, Jea Yong
    • Journal of Korean Society of Water and Wastewater
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    • v.19 no.5
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    • pp.537-546
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    • 2005
  • This study was carried out to evaluate EPS and SMP variation of sludge and effluent in nitrification and denitrification process with zeolite addition, a possible reduction of effluent DOC by URC(Ultra Rapid Coagulation) process. As a biological wastewater treatment result, EPS formation of both aeration and anoxic sludges are not affect by SRT variation. However, EPS concentration of sludges is higher in aeration tank than in anoxic tank by 6~8 mg EPS/ g VSS. Linear relationship between SMP to DOC indicates that SMP of bulk solution contributes to most of the biological treatment effluent DOC. DOC and turbidity removal efficiency was more improved with URC process than in a conventional coagulation. For pretreatment of UF filtration DOC removal was advanced by URC process than only UF filtration.

Preparation of Fine Silk Powder and It′s Application for Surface Modification (폐견사류의 미세분말화 및 표면 가공제 적용)

  • 이용우;이광길;여주홍;김종호
    • Journal of Sericultural and Entomological Science
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    • v.43 no.1
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    • pp.41-48
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    • 2001
  • The purification, dissolution and powdering of stained waste silk obtained from weaving and dyeing process were studied for the surface modification of textile fabric and plastic materials. The whiteness of stained waste silk could be improved through degumming and bleaching with sodium hydrosulfite. The water-soluble fibroin solution can be obtained by dissoving the degummed waste silk in a boiling solution of 50% calcium chloride for 60 minutes. The salts and heavy metals contained in fibroin solution were removed by electric dialysis, wool fiber filtration and gel filtration chromatography. The fibroin powder was prepared by using a fine grinder after the alkali treatment for weakening the silk fiber. The fine fibroin powder of particle size around 30 ㎛ was obtained with a ultra fine-mill, while it was finer below 10 ㎛ with a ball-mill. The dissolved or powdered silk was applied to the surface of fabric with addition of the binder (a urethane resin). The moisture content of polyester and nylon fabrics treated with the silk solution was improved due to hygroscopic property of silk. The fine fibroin powder mixed with the binder ws coated on the surface of synthetic film by use of the air pressed sprayer. It was revealed that the hygroscopicity as well as the softness of fibroin powder coated film was much improved. Therefore, it is thought that the fine silk fibroin powder is applicable as an coating agent for the surface modification of plastic and synthetic leather.

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Modification of polyethersulfone hollow fiber membrane with different polymeric additives

  • Arahman, Nasrul;Mulyati, Sri;Lubis, Mirna Rahmah;Razi, Fachrul;Takagi, Ryosuke;Matsuyama, Hideto
    • Membrane and Water Treatment
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    • v.7 no.4
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    • pp.355-365
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    • 2016
  • The improvement of fouling resistance of porous polymeric membrane is one of the most important targets in membrane preparation for water purification in many process like wastewater treatment. Membranes can be modified by various techniques, including the treatment of polymer material, blending of hydrophilic polymer into polymer solution, and post treatment of fabricated membrane. This research proposed the modifications of morphology and surface property of hydrophobic membrane by blending polyethersulfone (PES) with three polymeric additives, polyvinylpyrrolidone (PVP), Pluronic F127 (Plu), and Tetronic 1307 (Tet). PES hollow fiber membranes were fabricated via dry-wet spinning process by using a spinneret with inner and outer diameter of 0.7 and 1.0 mm, respectively. The morphology changes of PES blend membrane by those additives, as well as the change of performance in ultrafiltration module were comparatively observed. The surface structure of membranes was characterized by atomic force microscopy and Fourier transform infra red spectroscopy. The cross section morphology of PES blend hollow fiber membranes was investigated by scanning electron microscopy. The results showed that all polymeric additives blended in this system affected to improve the performances of PES membrane. The ultra-filtration experiment confirmed that PES-PVP membrane showed the best performance among the three membranes on the basis of filtration stability.

Ultra- and Nano-Filtration Process Optimization of Isoflavones and Oligosaccharides from Sunmul

  • Kim, Woo-Jung;Kim, Hak-Hyun;Yoo, Sang-Ho
    • Food Science and Biotechnology
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    • v.14 no.3
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    • pp.380-386
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    • 2005
  • Optimal conditions of ultrafiltration (UF) and nanofiltration (NF) were investigated for separation and concentration of isoflavones and oligosaccharides from Sunmul. Levels of COD, BOD, and suspended solids (SS) in UF and NF permeates were also determined to evaluate effectiveness of these processes for reducing water pollution. Optimal UF operation conditions to achieve minimal fouling and maximal flux were $33-34^{\circ}C$ operating temperature and 2.3-2.4 bar trans-membrane pressure. Recovery yields of isoflavones and oligosaccharides in UF retentate were 11.49-28.16% and 12.77-27.57%, respectively. Increase in volumetric concentration factor (VCF) resulted in more functional compounds of isoflavones and oligosaccharides passing through UF membrane. Total isoflavone and oligosaccharide yields decreased by 3% as VCF increased from 6.0 to 8.0 and from 8.0 to 10.0, while decreased significantly by 10% as VCF decreased from 4.0 to 6.0. Optimal NF operating conditions were 192-195 psig operating pressure at $30-33^{\circ}C$. Total yields of isoflavones and oligosaccharides significantly decreased at VCF 8.0, whereas did not decrease up to VCF 6.0 during NF operation. Therefore, VCF 6.0 was recommended for economical process. COD and BOD decreased by more than 98% after NF process, and SS were not detected after UF process. These results indicated sequential filtration process was useful for separation of isoflavones and oligosaccharides from Sunmul and for reducing water contaminants.

Application and Evaluation of Cleaner Production Technology in Zinc Plating Process (아연도금공정에서의 청정생산기술의 적용 및 평가)

  • Lee, H.K.;Koo, S.B.
    • Clean Technology
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    • v.9 no.2
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    • pp.63-69
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    • 2003
  • The metal finishing industry generates a variety of pollutants such as acidic or alkaline wastewater, chromic compounds, cyanide, heavy metals, and toxic materials. Especially, zinc plating process is one of the processes which cause serious environmental problems. In this study, we applied the proven optimum technology to important unit processes in terms of implement effects through the process diagnosis and analysis. This study aimed to improve the working environment and the environmental pollutions in zinc plating process.

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Size Characterization of Sodium Hyaluronate by Field Programming Frit Inlet Asymmetrical Flow Field-Flow Fractionation/Multiangle Light Scattering

  • Kim, Hoon-joo;Lee, Hee-jeong;Moon, Myeong-Hee
    • Bulletin of the Korean Chemical Society
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    • v.27 no.3
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    • pp.413-418
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    • 2006
  • Sodium hyaluronate (NaHA), water soluble polymer having ultra-high molecular weight, is characterized by using on-line frit inlet asymmetrical flow field-flow fractionation (FI-AFlFFF) and multiangle light scattering (MALS). This study demonstrates the capability of power programming FI-AFlFFF for the separation of NaHA and the applicability of FI-AFlFFF with MALS for the characterization of molecular weight distribution and their structural information. Since sample injection and relaxation in FI-AFlFFF are achieved by using hydrodynamic relaxation, separation of high molecular weight polymers can be achieved smoothly without halting the separation flow. Experiments are carried out with the two different NaHA products (a raw NaHA sample and a thermally degraded NaHA product) and molecular weight distribution and conformations in solution are determined. Influence of sample filtration on the change of molecular weight distribution is also discussed.

A study on the disinfection performance of indoor microorganism using energy consumption analysis for indoor bio-safety (건물 재실자의 미생물 안전을 위한 면역건물 기술의 에너지 사용 연구)

  • Choi, Sang-Gon
    • Journal of the Korea Safety Management & Science
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    • v.11 no.4
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    • pp.111-118
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    • 2009
  • In this study the real situation of apartment house in seoul is reproduced with multi-zone modeling program CONTAM2.4. This model include disinfection system which is consist of dilution, filtration, UVGI(ultra violet germicidal irradiation). It's energy consumption was also analyzed through the linked model of CONTAM and TRNSYS according to the combination of components. The comparison of total energy consumption through energy analysis revealed that adjusting the air change rate of the UVGI air sterilizer to maintain the same indoor microbe removal capability was more advantageous in terms of energy consumption.