• Journal of the Korean Applied Science and Technology
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• v.30 no.4
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• pp.586-591
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• 2013

This paper describes the characteristics of thermo-field emission in a freestanding silicon nanomembrane under ion bombardment with various thermal and field conditions. The thermal effect and field effect in thermo-field emission in silicon nanomembrane are investigated by varying kinetic energy of ions and electric field applied to the silicon nanomembrane surface, respectively. We found that thermo-field emission increases linearly as the electric field increases, when the electric field intensity is lower than the threshold. The thermo-field emission (schottky effect) increases proportionally to the power of temperature, which agree well with the predictions of a thermo-field emission model.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.44 no.7
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• pp.568-575
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• 2016

For the combat survivability, an infrared signature emitted from aircraft is needed to be predicted and analyzed. In this study, we studied the infrared signature from the exhaust plume from the viewpoint of Infrared(IR) detector. The Line-By-Line method using the radiation database is used for radiative property, and radiative intensity analysis is conducted along 1-D line of sight based on the radiative property. The numerical thermo-fluid field for the plume is conducted by ANSYS FLUENT, while setting the lines of sight having the different detection angle on the thermo-fluid field. We found the high IR signature on the line of sight passing through the locally high temperature region of the plume inside, and the strongest signature from the line of sight toward the nozzle surface. Based on this, it confirms the influence of the surface radiative emission on the infrared signature.

• Membrane Journal
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• v.22 no.2
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• pp.104-112
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• 2012

Chemically stable Polyvinylidene fluoride-hexa-fluoropropane (PVDF-HFP) copolymer asymmetric membranes were prepared by the conventional phase inversion process, using Dimethyacetamide (DMAc) as a solvent and water as a non-solvent. To control the pore size and porosity of the PVDF-HFP membranes, tetra-ethoxysilane (TEOS) was used as a pore-forming agent. The prepared membranes were characterized, using several analytical methods such as Fourier Transform Infrared spectroscopy (FTIR), Thermo-gravimetric analyzer (TGA), Field Emission Scanning Electronic Microscopy (FESEM). TEOS turned out to increase porosity and make homogeneous pores on the membranes. Depending on the composition of the dope solutions, the pore size was ranged from 0.1 to 1.0 ${\mu}m$. The flux of the PVDF-HFP membranes prepared by using TEOS as a pore forming agent was increased substantially without much decrease in the rejection. When 15 wt% PVDF-HFP solution was blended with 13 wt% TEOS solution at composition ratio of 70/30 in wt%, the water flux at 2 bars was about 2 $m^3/m^2day$.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.25 no.6
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• pp.431-434
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• 2012

In this paper, heat-releasing sheets made of AlN powder and acryl binder as thermoset were prepared using tape casting method. The crystal structure and morphology, the thermal properties as nonvolatile solid content and thermal conductivity, and the surface resistance of heat-releasing sheet were measured by using X-ray diffractometer, field emission-scanning electron microscopy, thermo gravimetric analyzer and laser flash instrument, and surface resistance meter. It was proved that thermal conductivity is greatly affected by the content of binder in heat-releasing sheet. Superior thermal conductivity above 3.5 W/mK and suface resistance were obtained at heat-releasing sheet with above 90% of AlN powder.

• Polymer(Korea)
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• v.35 no.5
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• pp.402-408
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• 2011

To improve $Na^+$-saponite(SPT) film flexibility, we prepared SPT hybrid clay films with various poly(vinyl alcohol) (PVA) concentrations(0~10 wt%) using the solution intercalation method. In this study, we investigated the thermo-optical properties, morphology, and gas permeability of the SPT hybrid films. We also examined the relationship between the film properties and PVA content using wide angle X-ray diffraction measurements(XRD), field emission scanning electron microscopy(FESEM), differential scanning calorimetry(DSC), thermogravimetric analysis(TGA), thermomechanical analysis(TMA), ultraviolet-visible(UV-vis) spectroscopy, and oxygen transmission rate($O_2$TR) testing. The properties of the clay hybrid films were strongly affected by PVA filler content. The presence of a small amount of PVA was sufficient to improve the flexibility of SPT hybrid films.

• Journal of Advanced Marine Engineering and Technology
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• v.35 no.2
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• pp.252-257
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• 2011

Magnesium thin films for marine engine parts such as the engine block and the cylinder head cover etc. were prepared on the magnesium alloy(AZ91D) substrate by Thermo-electron activated Ion-plating method. The influence of gas pressure and substrate bias voltages on the crystal orientation and morphology of the films was investigated with X-ray diffraction and field emission scanning electron microscope(FE-SEM), respectively. Moreover, the effect of crystal orientation and morphology of the magnesium films on the its hardness property was investigated as well. From the results, the hardness of the films was increased in Ar gas pressure due to the grain boundary strengthening and occlusion effects.

• Transactions of the Korean hydrogen and new energy society
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• v.23 no.5
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• pp.429-436
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• 2012

Mg and Mg-based alloys are regarded as strong candidate hydrogen storage materials since their hydrogen capacity exceeds that of known metal hydrides. One of the approaches to improve kinetic is addition of metal oxide. In this paper, we tried to improve the hydrogenation properties of Mg-based hydrogen storage composites. The effect of transition metal oxides, such as $Nb_2O_5$ on the kinetics of the Magnesium hydrogen absorption kinetics was investigated. $MgH_x$-5wt.% $Nb_2O_5$ composites have been synthesized by hydrogen induced mechanical alloying. The powder fabricated was characterized by X-ray diffraction (XRD), Field Emission-Scanning Electron Microscopy (Fe-SEM), Energy Dispersive X-ray (EDX), BET and simultaneous Thermo Gravimetric Analysis / Differential Scanning Calorimetry (TG/DSC) analysis. The Absorption / desorption kinetics of $MgH_x$-5wt.% $Nb_2O_5$ (type I and II) are determined at 423, 473, 523, 573 and 623 K.

• KCI Concrete Journal
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• v.11 no.3
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• pp.127-140
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• 1999

In this paper, a microscopic analysis of prefinitelv strained cement paste specimen was carried out. The microscopic behavior of concrete under triaxial stress must be fully understood in order to explain the additional ductilitv that comes from lateral confinement and to get microstructural information in large deformed and large strained concrete. The so-called "tube-squash" test was applied to achieve enormously high shear and deviatoric strain of concrete under extremly high pressure without fracture. Then, microscopic analyses by focusing on hydration and microstructure of Prefinitely strained cement paste were carried out on cored-out deformed and virgin (undeformed) cement paste specimens : the first specimen being 40 days old, the second one being one year old. The microscopic analysis bv Field Emission Scanning Electronic Microscope (FESEM) was carried out for comparison between the specimens after 40 days and those arter one year. For one year old specimens, X-Ray Diffractometer (XRD) analysis, Energy Dispersive x-rav Spectrometer (EDS) analysis, and Differential Thermal Analysis/Thermo-Gravitv (DTA/TG) analysis were also carried out to study the hydration and the microstructures of prefinitely strained cement paste specimen by focusing on the methodologies of their microscopic analyses. analyses.