• Title/Summary/Keyword: thermal processing

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Effect of Thermal Exposure and Rejuvenation Treatment on Microstructure and Stress Rupture Properties of IN738LC (IN738LC 합금의 열간 노출 및 재생 열처리에 따른 미세조직과 응력 파단 특성의 변화)

  • Choe, Baek-Gyu;Ju, Dong-Won;Kim, In-Su;Jang, Jung-Cheol;Jo, Chang-Yong
    • Korean Journal of Materials Research
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    • v.11 no.10
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    • pp.833-840
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    • 2001
  • Effects of thermal exposure and rejuvenation treatment on the microstructural evolution and the stress-rupture properties of IN738LC have been investigated. The role of precipitates on the stress- rupture properties has been analyzed through microstructural observations. Thermal exposure at $982^{\circ}C$ for 1000 hours gave rise to precipitation of $\sigma$ phase and coarsening of ${\gamma}$'. The microstructural degradation with thermal exposure at $982^{\circ}C$ deteriorated stress rupture properties of the alloy. All the existing phases except MC carbides have completely dissolved into the matrix with homogenization treatment at $1200^{\circ}C$ for 2 hours. Microstructure and stress-rupture properties of the thermal exposed specimens have been successfully rejuvenated by the proposed treatment.

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Effects of Inoculum Level and Pressure Pulse on the Inactivation of Clostridium sporogenes Spores by Pressure-Assisted Thermal Processing

  • Ahn, Ju-Hee;Balasubramaniam, V.M.
    • Journal of Microbiology and Biotechnology
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    • v.17 no.4
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    • pp.616-623
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    • 2007
  • The effects of initial concentration and pulsed pressurization on the inactivation of Clostridium sporogenes spores suspended in deionized water were determined during thermal processing $(TP;\;105^{\circ}C,\;0.1MPa)$ and pressure-assisted thermal processing $(PATP;\;105^{\circ}C\;and\;700MPa)$ treatments for 40 min and 5min holding times, respectively. Different inoculum levels $(10^4,\;10^6\;and\;10^8CFU/ml)$ of C. sporogenes spores suspended in deionized water were treated at $105^{\circ}C$ under 700MPa with single, double, and triple pulses. Thermally treated samples served as control. No statistical significances (p>0.05) were observed among all different inoculum levels during the thermal treatment, whereas the inactivation rates $(k_1\;and\;k_2)$ were decreased with increasing the initial concentrations of C. sporogenes spores during the PATP treatments. Double- and triple-pulsed pressurization reduced more effectively the number of C. sporogenes spores than single-pulse pressurization. The study shows that the spore clumps formed during the PATP may lead to an increase in pressure-thermal resistance, and multiple-pulsed pressurization can be more effective in inactivating bacterial spores. The results provide an interesting insight on the spore inactivation mechanisms with regard to inoculum level and pulsed pressurization.

A Frequency Spectrum Analysis based on FFT of Fire Thermal Image (FFT를 이용한 화재 열영상의 주파수 스펙트럼 분석)

  • Kim, Won-Ho;Jang, Bok-Gyu
    • Journal of the Institute of Convergence Signal Processing
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    • v.12 no.1
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    • pp.33-37
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    • 2011
  • This paper presents the frequency spectral analysis based on FFT of the infrared ray fire thermal image, it is an object to deduce the conditions for determining fire alarm through the image processing with the frequency domain. After the candidate regions are separated by using pre-defined brightness value, the fast fourier transform is performed for consecutive infrared thermal images, the frequency spectral analysis of the thermal image analyzed DC and AC frequency distribution. The fire criterion of the thermal image was presented based on the analyzed result and a practicality was confirmed through the computer simulation.

Synthesis and Characterization of Glold Nanofluid Prepared by the Solution Plasma Processing (용액 플라즈마 공정을 이용하여 제조된 금 나노유체의 특성평가)

  • Heo, Yong-Kang;Lee, Sang-Yul
    • Journal of Powder Materials
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    • v.17 no.4
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    • pp.342-346
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    • 2010
  • In the present work, water-based gold nanofluids were synthesized by the solution plasma processing (SPP). The size distribution and the shape of gold nanoparticles in the nanofluids were investigated using high resolution transmission electron microscopy (HR-TEM). The dispersion stability of gold nanofluids was characterized using zeta potential, as well. The thermal properties of gold nanofluids were measured by utilizing lambda measurement device. Nanofluids containing nanoparticles with $64.0{\pm}42.1\;nm{\sim}18.10{\pm}5.0\;nm$ in diameter were successfully synthesized. As diameter of nanoparticles decreased, dispersion stability of nanofluids increased and the enhanced ratio of thermal conductivity increased. The nanofluid with nanoparticles of $18.10\;{\pm}\;5.0\;nm$ in diameter showed approximately 3% improvement in thermal conductivity measurement and this could be due to the enhanced Brownian movement.

Progresses on the Optimal Processing and Properties of Highly Porous Rare Earth Silicate Thermal Insulators

  • Wu, Zhen;Sun, Luchao;Wang, Jingyang
    • Journal of the Korean Ceramic Society
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    • v.55 no.6
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    • pp.527-555
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    • 2018
  • High-temperature thermal insulation materials challenge extensive oxide candidates such as porus $SiO_2$, $Al_2O_3$, yttria-stabilized zirconia, and mullite, due to the needs of good mechanical, thermal, and chemical reliabilities at high temperatures simultaneously. Recently, porous rare earth (RE) silicates have been revealed to be excellent thermal insulators in harsh environments. These materials display attractive properties, including high porosity, moderately high compressive strength, low processing shrinkage (near-net-shaping), and very low thermal conductivity. The current critical challenge is to balance the excellent thermal insulation property (extremely high porosity) with their good mechanical properties, especially at high temperatures. Herein, we review the recent developments in processing techniques to achieve extremely high porosity and multiscale strengthening strategy, including solid solution strengthening and fiber reinforcement methods, for enhancing the mechanical properties of porous RE silicate ceramics. Highly porous RE silicates are highlighted as emerging high-temperature thermal insulators for extreme environments.

Estimation of Temperature Distribution on Wafer Surface in Rapid Thermal Processing Systems (고속 열처리공정 시스템에서의 웨이퍼 상의 온도분포 추정)

  • Yi, Seok-Joo;Sim, Young-Tae;Koh, Taek-Beom;Woo, Kwang-Bang
    • Journal of Institute of Control, Robotics and Systems
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    • v.5 no.4
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    • pp.481-488
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    • 1999
  • A thermal model based on the chamber geometry of the industry-standard AST SHS200MA rapid thermal processing system has been developed for the study of thermal uniformity and process repeatability thermal model combines radiation energy transfer directly from the tungsten-halogen lamps and the steady-state thermal conducting equations. Because of the difficulties of solving partial differential equation, calculation of wafer temperature was performed by using finite-difference approximation. The proposed thermal model was verified via titanium silicidation experiments. As a result, we can conclude that the thermal model show good estimation of wafer surface temperature distribution.

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Implementation of a Thermal Imaging System with Focal Plane Array Typed Sensor (초점면 배열 방식의 열상카메라 시스템의 구현)

  • 박세화;원동혁;오세중;윤대섭
    • Journal of Institute of Control, Robotics and Systems
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    • v.6 no.5
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    • pp.396-403
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    • 2000
  • A thermal imaging system is implemented for the measurement and the analysis of the thermal distribution of the target objects. The main part of the system is a thermal camera in which a focal plane array typed sensor is introduced. The sensor detects the mid-range infrared spectrum of target objects and then it outputs a generic video signal which should be processed to form a frame thermal image. Here, a digital signal processor(DSP) is applied for the high speed processing of the sensor signals. The DSP controls analog-to-digital converter, performs correction algorithms and outputs the frame thermal data to frame buffers. With the frame buffers can be generated a NTSC signal and transferred the frame data to personal computer(PC) for the analysis and a monitoring of the thermal scenes. By performing the signal processing functions in the DSP the overall system achieves a simple configuration. Several experimental results indicate the performance of the overall system.

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Development of numerical-computation program to predict thermal shock induced by fs laser processing of meatals (펨토초 레이저 금속 가공시 발생하는 열충격 수치계산 프로그램 개발)

  • O, Bu-Guk;Kim, Dong-Sik;Kim, Jae-Gu;Lee, Je-Hun
    • Laser Solutions
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    • v.11 no.1
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    • pp.19-24
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    • 2008
  • It has been recognized that laser dicing of wafers results in low mechanical strength compared to the conventional sawing techniques. Thermal shock generated by rapid thermal loading is responsible for this problem. This work presents a two-dimensional ultra-short thermo elastic model for numerical simulation of femtosecond laser ablation of metals in the high-fluence regime where the phase explosion is dominant. Laser-induced thermoelastic stress is analyzed for Ni. The results show that the laser-induced thermal shock is large enough to induce mechanical damages.

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High Resolution Electronic Processor Design for Thermal Imager with 320x240 Staring Array Infrared Detector (320x240 적외선 배열검출기를 이용한 고분해능 열상 신호처리기 구현)

  • Hong, Seok-Min;Yu, Wee-Kyung;Yoon, Eun-Suk
    • Journal of the Korea Institute of Military Science and Technology
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    • v.9 no.2 s.25
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    • pp.111-117
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    • 2006
  • This paper describes the design principles and methods of electronic processor for thermal imager with 320$\times$240 staring array infrared detector. For the detector's nonuniformity correction and excellent image quality, we have designed the multi-point correction method using the defocusing technique of the optics. And to enhance the image of low contrast and improve the detection capability, the new technique of histogram processing has been designed. Through these image processing techniques, we have developed the high quality thermal imager and acquired a satisfactory thermal image. The result of MRTD(Minimum Resolvable Temperature Difference) is $0.1^{\circ}C$ at 4cycles/mard.

A Study on the Thermal Characteristics and Fire Hazard of Iron Powder Accumulated on Circuit Break (차단기 누적 철분진의 열적특성과 발화위험성 연구)

  • Kim, Doo-Hyun;Kang, Yang-Hyun
    • Journal of the Korean Society of Safety
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    • v.27 no.4
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    • pp.20-25
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    • 2012
  • The purpose of this study is to analyze the thermal characteristics and to study fire hazard of electric leakage by iron power accumulated on circuit breaker in an iron processing factory. The thermal characteristics were analyzed while current was applied to the powder for ten minutes. Results showed that temperature of iron powder at 100 mA is $160^{\circ}C$ and at 175mA is $240^{\circ}C$. The sparks have occurred as iron powder drops between two(hot line and neutral line) wires and then iron powder explosion occurred while dropping continuously the iron powder on two lines. Those who work in the iron processing industry need to periodically remove and maintain the iron powder. The thermal characteristics in this paper can be used for electrical fire investigation and for basic data of thermal characteristic of leakage current through iron powder at iron processing factories.