• Title/Summary/Keyword: thermal gradient furnace

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Mineral and Chemical Changes in Silica Brick After Service in Arc-furnace Roofs (아-크로 천장 사용후의 규석벽돌의 광물 및 화학적 변화)

  • 오기동;박홍채
    • Journal of the Korean Ceramic Society
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    • v.18 no.4
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    • pp.247-256
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    • 1981
  • Silica bricks had been in arc-furnace roofs of various sizes and steelmaking practices. The resulting materials were examined with reference to mineral and chemical changes. Silica bricks develope definite zones while in service. These zones represent a concentration gradient through the brick that results from the thermal gradient across the brick and from the furnace atmosphere. There are major brick losses by spalling as well as by melting of the hot-face surface in an iron-oxide rich liquid.

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The Effect of Solidification Rates and Thermal Gradients on Directionally Solidified Microstructure in the Ni-base Superalloy GTD111M (GTD111M 초내열합금에서 응고속도 및 온도구배가 일방향응고 조직 에 미치는 영향)

  • Ye, Dae-Hee;Kim, Cyun-Choul;Lee, Je-Hyun;Yoo, Young-Soo;Jo, Chang-Yong
    • Korean Journal of Materials Research
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    • v.12 no.12
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    • pp.897-903
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    • 2002
  • Morphological evolution and growth mechanism at the solid/liquid interface during solidification were investigated in the Ni-base superalloy GTD111M by directional soldification and quenching(DSQ) technique. The experiments were conducted by changing solidification rate(V) and thermal gradient(G) which are major solidification process variables. High thermal gradient condition could be obtained by increasing the furnace temperature and closely attaching the heating and cooling zones in the Bridgeman type furnace. The dendritic/equiaxed transition was found in the G/V value lower than $0.05$\times$10{^3}^{\circ}C$s/$\textrm{mm}^2$, and the planar interface of the MC-${\gamma}$ eutectic was found under $17 $\times$ 10{^3}^{\circ}C$ s/$\textrm{mm}^2$. It was confirmed that the dendrite spacing depended on the cooling rate(GV), and the primary spacing was affected by the thermal gradient more than solidification rate. The dendrite lengths were decreased as increasing the thermal graditne, and the dendrite tip temperature was close to the liquidus temperature at $50 \mu\textrm{m}$/s.

A Study on Thermal Shock Characteristics of Functionally Gradient Ceramic/Metal Composites (경사기능성 세라믹/ 금속 복합재료의 열충격특성에 관한 연구)

  • Song, Jun-Hee;Lim, Jae-Kyoo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.20 no.7
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    • pp.2134-2140
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    • 1996
  • This study was carried out to anlayze the heat-resistant characteristics of functionally gradient material(FGM) composed with ceramic and metal. The thermal fracture behavior of plasma-sprayed FGM and conventional coating material(NFGM) was exaimined by acoustic emession technique under heating and cooling. Furnace cooling and rapid cooling tests were used to examine the effect of temperature change under various conditions, respectively. At the high temperature above $800^{\circ}C$, it was shown that FGM gives higher thermal resistance compared to NFGM by AE signal and fracture surface analysis.

Dendrite Arm Spacing and Carbide Morphology with Thermal Gradient and Solidification Rate in Directionally Solidified Ni-Base Superalloy (일방향 초내열합금에서 응고속도 및 온도구배 따른 수지상간격 및 탄화물 형상 변화)

  • Son, S.D.;Kim, Y.H.;Choi, G.S.;Lee, J.H.;Seo, S.M.;Jo, C.Y.
    • Journal of Korea Foundry Society
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    • v.27 no.2
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    • pp.77-82
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    • 2007
  • The effects of thermal gradient and solidification rate on the dendrite arm spacing and carbide morphology were investigated in directionally solidified Ni-base superalloy, CM 247LC. Thermal gradient was controlled by changing the position of the cold chamber and the furnace set temperature. The interface morphology changed from the planar to dendritic as increasing solidification rate. It was found that the dendrite spacing decreased as increasing the thermal gradient as well as the solidification rate. Also, as increasing solidification rate, carbide morphology changed from blocky shape to script and spotty shapes.

Thermal Gradient Change of T-shaped Mg Alloy Specimen Exposed to Electropulses (전류펄스 인가된 T자형 Mg 합금 시편의 온도 구배 변화)

  • J.H. Song;D.J. Park;S. Cheon;J. Yu;S.H. Lee;T. Lee
    • Transactions of Materials Processing
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    • v.33 no.4
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    • pp.285-290
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    • 2024
  • Electropulsing treatment (EPT) has been developed as an alternative to furnace heat treatment (FHT) to exploit its engineering advantages in rapidly annealing metallic materials. Conventionally, the separation of thermal and athermal effects of EPT has been attempted by comparing EPT and FHT specimens processed under identical temperature and duration. However, this method inherently introduces experimental and measurement errors. This study proposes a novel approach to distinguish the thermal and athermal effects of EPT-processed metals using T-shaped specimen with two observation points, namely 'C' and 'D'. For verification, the thermal gradient of T-shaped Mg alloys was examined under various EPT conditions. The points C exhibited higher temperatures compared to those at points D at a given electric current density, because only the former received both thermal and athermal effects. It was confirmed from twelve specimens that the point C at an electric current density of 65 A·mm-2 and point D at 70 A·mm-2 exhibited similar temperatures. This developed method is expected to reduce measurement errors in distinguishing thermal and athermal effects, thus providing a deeper understanding of their quantitative contributions in future studies.

Development of the RE indirect-heating LPE furnace and the effect of impurity in YIG film on the MSSW properties

  • Fujino, M.;Fujii, T.;Sakabe, Y.
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.12 no.6
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    • pp.288-291
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    • 2002
  • We developed a new RF indirect-heating LPE furnace. The thermal gradient of our newly developed furnace is less than that of direct heating, and is as gentle as that of the resistance-heating LPE furnace. With this new furnace, the heating and/or cooling is faster than that of the resistance-heating furnace. Impurity-doped YIG film was grown from a $PbO-B_{2}O_{3}$, based flux on a (111) GGG substrate. To study the effect of the impurities on the MSSW threshold power and the saturation response time, we used two microstrip lines to excite and propagate the MSSW at 1.9 GHz. The MSSW threshold power and saturation response time was found to be related to the $\Delta$H.

Fabrication of 6.4 cm single grain $YBa_2$$Cu_3$$O_x$ (6.4cm 크기의 일방향 성장된Y$Ba_2$$Cu_3$$O_x$ 제조)

  • 박병삼;한상철;한영희;정년호;윤희중;김경진;성태현;오제명
    • Progress in Superconductivity
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    • v.5 no.2
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    • pp.114-117
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    • 2004
  • We fabricated large single grain YBa$_2$Cu$_3$O$_{x}$ (Y-123) superconductors. The single grain Y-123 was grown by top seeded melt growth (TSMG) method. In a conventional box furnace with uniform temperature distribution, it was very difficult to grow large single grain Y-123 superconductors due to the size limitation in growth. To overcome the size limitation, we applied a radial thermal gradient (lower temperature at sample center and higher temperature on the sample edge) to the TSMG process. In this case, large single grain Y-123 could be easily grown. This is attributed that the liquid of the sample edge was maintained at the high temperature compared to the growth front. Using this method, we successfully fabricated a large single grain Y-123 of 6.4 cm X6.4 cm

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Characteristics of the Unidirectionally Solidified Al-Co Alloy (일방향응고시킨 Al-Co 합금의 특성에 관한 연구)

  • Park, Su-Jung;Jun, Hyun-Yong;Lee, Hyun-Kyu
    • Journal of Korea Foundry Society
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    • v.25 no.1
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    • pp.30-35
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    • 2005
  • The structures and mechanical property of the unidirectionally solidified Al-Co eutectic alloy were investigated. Al-Co eutectic alloy was unidirectionally solidified with growth rates(R) between I cm/hr and 10 cm/hr in the induction furnace maintaining the thermal gradient (G) at solid-liquid interface, $32^{\circ}C$/cm. The eutectic microstructure was varied with the growth condition(G/R ratio). When the G/R ratio was larger than $8.5{\times}10^{3}^{\circ}C/cm^{2}/sec$, a lamellar structure was formed, But the G/R ratio was smaller than $8.5{\times}10^{3}^{\circ}C/cm^{2}/sec$, a colony structure was formed. It was found that the interlamellar spacing(${\lambda}$) was dependent on the growth rate(R) with the relationship, ${\lambda}^{2}{\cdot}R=constant$. The microhardness of this eutectic alloy increased with increase in the growth rate.

Microstructural Evolution in the Unidirectional Heat Treatment of Cu-35%Sn Alloys (Cu-35%Sn 합금의 일방향 열처리에서 출현하는 미세조직)

  • Choi, K.J.;Jee, T.G.;Park, J.S.
    • Journal of the Korean Society for Heat Treatment
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    • v.16 no.6
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    • pp.320-328
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    • 2003
  • A specimen of Cu-35%Sn alloy has been subjected to the unidirectional heat treatment in an attempt to examine the evolution of microstructures under varying thermal conditions. The specimen was cast in the form of a cylinder 10 mm in diameter and 200 mm in length, which was then installed in the temperature gradient field established inside a vertical tube furnace. The furnace temperature was adjusted to make the upper part at $750^{\circ}C$ and bottom end part at $300^{\circ}C$ of the specimen. The experiment was terminated by dropping it into water after the 30 minutes holding at given temperature. By the rapid cooling, the high temperature phases, ${\gamma}$ and ${\zeta}$, were retained at ambient temperature with some of ${\gamma}$ phase transformed to ${\varepsilon}$ phase, especially at the grain boundaries of ${\gamma}$ phase. The presence of ${\varepsilon}$ phase was found to determine the nature of phase transformations of the ${\zeta}$ phase undergoes upon cooling. In the close area of the ${\varepsilon}$ phase, ${\varepsilon}$ phase grew separately out of ${\zeta}$, and adds to the preexisting ${\varepsilon}$ whereas in areas away from ${\varepsilon}$, both ${\delta}$ and ${\varepsilon}$ grew simultaneously out of ${\zeta}$, and formed a lamella eutectoid structure. The transformation to ${\delta}$ was found to occur only in slow cooling. The hardness on each phase showed that the retained phases, ${\gamma}$ and ${\zeta}$, could be plastically deformed without brittle fracture while the phases, ${\varepsilon}$ and ${\delta}$, were too brittle to be deformed.

Analysis with Directional Solidification in Silicon Melting Process (실리콘 용융 공정에서 방향성 응고에 관한 특성 분석)

  • Cho, Hyun-Seob
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.15 no.3
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    • pp.1707-1710
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    • 2014
  • This paper is the study for the directional solidification of the ingot through the thermal analysis simulation and structural change of casting furnace. The activation analysis of metal impurities were also detected the total number of 10 different metals, but the concentration distribution showed no significant positional deviations in the same position from the top to the bottom. With the results of thermal analysis simulation, the silicon as a whole has reached the melting temperature as the retention time 80 min. The best cooling conditions showed at the upper cooling temperature $1,400^{\circ}C$ and cooling time 60min. The fabricated wafers showed the superior etching result at the grain boundary than that of existing commercial wafers.