• 한국표면공학회지
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• 제48권6호
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• pp.253-259
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• 2015

The test equipment becomes more important with the development of semiconductor industry. MEMS probe is an important testing component to detect the defects from the generated electric signal when it contacts the metal pad of semiconductor devices. Ni-Pd alloy has been paid attention to as a candidate of MEMS probe material because of its high surface hardness and relatively low resistivity. In this study, electroplated Ni-Pd alloy has been prepared by using ethylene diamine as a complexing agent. Solid solution alloy coating could be formed when concentration of palladium chloride and current density were in the ranges of 1~5 mM and $0.2{\sim}1.5A/dm^2$, respectively. The increase of current density brought about an decrease in palladium content, which made both of lattice parameter and grain size smaller. As a result of grain refinement, high hardness could be obtained. However, surface cracking was observed due to residual stress when the current density was above $1.3A/dm^2$. When effects of heat treatment temperature on hardness and sheet resistance were investigated, the accompanied grain growth decreased both of them. The decrease of hardness remained stable at a temperature of $200^{\circ}C$. The sheet resistance was drastically reduced at $100^{\circ}C$. After that, it was found to become constant.

• 전기화학회지
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• 제7권4호
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• pp.189-193
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• 2004

본 연구에서는 POAGA와 TEGDMA로 구성된 반응성 단량체에서 두 단량체 및 개시제의 조성에 따른 겔폴리머전해질전지를 제조하고 전지특성을 평가하였다 POAGA계 겔폴리머전해질은 단량체의 함량이 증가함에 따라 겔화 시간은 감소하였다. POAGA계 겔폴리머전해질은 4.5V까지 전기화학적으로 안정하였으며, 상온 이온전도도는 약 $5.2\times10^{-3}Scm^{-1}$이었다. POAGA계 겔폴리머전해질을 채용한 리튬이온폴리머전지는 반응성 단량체의 함량이 $5.0wt\%$ 및 $7.0wt\%$인 경우에 비하여 $3.0wt\%$인 경우가 고율, 저온 및 사이클 특성이 우수하였다 또한 개시제 함량은 $1.0\~3.0wt\%$ 범위에서는 $1.0wt\%$인 경우가 우수한 전지특성을 나타내었다.

• 한국건축시공학회지
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• 제10권1호
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• pp.39-47
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• 2010

플라이애시는 콘크리트의 특성 개선, 콘크리트 제품의 가격 저감 및 내구성 개선, 수화열 감소 등의 이점이 있으나 다량 첨가시 콘크리트의 강도 부족 및 AE제 사용량의 증가 등으로 인하여 그 사용량이 제한되고 있다. 이에 본 연구에서는 플라이애시의 고부가 가치적 활용을 목적으로 플라이애시의 고분말도화($4000{\sim}8000cm^2/g$), 양생방법, 알카리자극제의 첨가 등을 통하여 플라이애시의 대량 사용에 대한 문제점을 해결하고자 하였으며, 연구결과 플라이애시의 분말도를 높여 양생온도 $40^{\circ}C$전후로 하여 자극제 첨가율을 적정하게 사용할 경우 수화물이 안정한 상태로 되어 강도발현이 아주 우수하게 나타나, 이에 대한 연구가 지속될 경우 플라이애쉬의 다량치환에 대한 효과적 가치 창출이 가능할 것으로 사료된다.

• 한국진공학회지
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• 제19권2호
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• pp.148-154
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• 2010

본 논문에서는 유기발광다이오드의 보호막 적용을 위하여 TCP-CVD를 이용한 실리콘 산화막 형성에서 산화막의 특성에 영향을 미치는 Power, 가스종류 및 유량, 소스와 기판거리 및 공정온도 등의 공정조건에 따른 증착된 산화막의 특성을 나타내는 증착률, 굴절률을 제어하고자 한다. 그 결과 $SiH_4$ : $O_2$ = 30 : 60 [sccm], 70 [mm]의 source와 기판 거리, Bias를 인가하지 않은 조건에서 80 [$^{\circ}C$] 이하의 공정온도를 보였으며 투과율 90% 이상, 높은 증착률 및 굴절률 1.4~1.5인 안정된 $SiO_2$ 산화박막을 제조할 수 있었다.

• 한국수소및신에너지학회논문집
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• 제17권2호
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• pp.149-157
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• 2006

Hydrogen as new energy sources is highly efficient and have very low environmental emissions. The proton exchange membrane fuel cell (PEMFC) is an emerging technology that can meet these demands. Therefore, the preparation of stable polymeric membranes with good proton conductivity and durability are very important for hydrogen production via water electrolysis with PEM at medium temperature above $80^{\circ}C$. Currently Nafion of Dupont and Aciflex of Asahi, etc., solid polymer electrolytes of perfluorosulfonic acid membrane, are the best performing commercially available polymer electrolytes. However, these membrane have several flaws including its high cost, and its limited operational temperature above $80^{\circ}C$. Because of this, significant research efforts have been devoted to the development of newer and cheaper membranes. In order to make up for the weak points and to improve the mechanical characteristics with cross -linking, acid-base complexes were prepared by the combination PSf-co-PPSS-$NH_2$ with PEEK-$SO_3H$. The results showed that the proton conductivity decreased in 17.6% and 40% but tensile strength increased in 78% and 98%, about $20.65\;{\times}\;10^6N/m^2$, in comparison with SBPSf/HPA and SPEEK/HPA complex membrane.

• Applied Microscopy
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• 제36권spc1호
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• pp.35-40
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• 2006

Self-assembled InAs/GaAs quantum dots (QDs) were grown by the atomic layer epitaxy (ALE) and molecular beam epitaxy (MBE) techniques, The structure and the thermal stability of QDs have been studied by high resolution electron microscopy with in-situ heating experiment capability, The ALE and MBE QDs were found to form a hemispherical structure with side facets in the early stage of growth, Upon capping by GaAs layer, however, the apex of QDs changed to a flat one. The ALE QDs have larger size and more regular shape than those of MBE QDs. The QDs collapse due to elevated temperature was observed directly in atomic scale, In situ heating experiment within TEM revealed that the uncapped QDs remained stable up to $580^{\circ}C$, However, at temperature above $600^{\circ}C$, the QDs collapsed due to the diffusion and evaporation of In and As from the QDs, The density of the QDs decreased abruptly by this collapse and most of them disappeared at above $600^{\circ}C$.

• Journal of Microbiology and Biotechnology
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• 제17권5호
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• pp.792-799
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• 2007

A gene encoding a putative glycogen-debranching enzyme in Sulfolobus shibatae(abbreviated as SSGDE) was cloned and expressed in Escherichia coli. The recombinant enzyme was purified to homogeneity by heat treatment and Ni-NTA affinity chromatography. The recombinant SSGDE was extremely thermostable, with an optimal temperature at $85^{\circ}C$. The enzyme had an optimum pH of 5.5 and was highly stable from pH 4.5 to 6.5. The substrate specificity of SSGDE suggested that it possesses characteristics of both amylo-1,6-glucosidase and $\alpha$-1,4-glucanotransferase. SSGDE clearly hydrolyzed pullulan to maltotriose, and $6-O-\alpha-maltosyl-\beta-cyclodextrin(G2-\beta-CD)$ to maltose and $\beta$-cyclodextrin. At the same time, SSGDE transferred maltooligosyl residues to the maltooligosaccharides employed, and maltosyl residues to $G2-\beta-CD$. The enzyme preferentially hydrolyzed amylopectin, followed in a decreasing order by glycogen, pullulan, and amylose. Therefore, the present results suggest that the glycogen-debranching enzyme from S. shibatae may have industrial application for the efficient debranching and modification of starch to dextrins at a high temperature.

• Journal of Electrical Engineering and Technology
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• 제13권3호
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• pp.1166-1172
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• 2018

Degradation due to delamination occurs frequently in the high temperature superconductors (HTS) coil of rotating machines made with 2nd generation (2G) HTS wire, and the authors have observed other similar cases. Since an HTS field coil for a rotating machine is required to have stable current control and maintain a steady state, co-winding techniques for insulation material and epoxy resin for shape retention and heat transfer improvement are applied during coil fabrication. However, the most important limiting factor of this technique is delamination, which is known to be caused by the difference in thermal expansion between the epoxy resin and 2G HTS wire. Therefore, in this study, the experimental results of mixing the ratio of epoxy resin and alumina ($Al_2O3$) filler were applied to the fabrication of small and large test coils to solve the problem of degradation. For the verification of this scheme, eight prototypes of single pancake coils with different shapes were fabricated. They showed good results. The energization and operation maintenance tests of the stacked coils were carried out under liquid neon conditions similar to the operation temperature of an MW-class rotating machine. In conclusion, it was confirmed that the alumina powder mixed with epoxy resin in an appropriate ratio is an effective solution of de-lamination problem of 2G HTS coil.

• 한국정보통신학회:학술대회논문집
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• 한국정보통신학회 2017년도 추계학술대회
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• pp.514-517
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• 2017

태양광 발전 시스템에서 전력 생산은 기상 상태에 따라 크게 영향을 받으므로 안정적인 부하 운용을 위해 태양광 에너지에 대한 예측이 필수적이다. 따라서 태양광 에너지 예측을 위한 기계학습 알고리즘의 입력으로 기상 상태에 대한 데이터가 필요하다. 본 논문에서는 알고리즘에 대한 입력 데이터로 표면의 3시간 동안 누적된 강수량, 상 하향 장파 복사선 평균, 상 하향 단파 복사선 평균, 지상 2m에서의 3시간 동안 온도, 표면에서의 온도 등 15가지 종류의 기상 데이터를 사용한다. 기상 데이터의 통계적 특성을 파악하고 상관관계를 분석하여 태양광 에너지와 70% 이상의 높은 상관성을 갖는 하향 단파 복사선 평균과 상향 단파 복사선 평균을 특징벡터의 주요 원소로 추출하였다.

• 한국재료학회지
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• 제22권10호
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• pp.499-503
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• 2012

The present study is intended to comparatively investigate the changes in microstructure and tensile properties at room and elevated temperatures in commercial AM50(Mg-5%Al-0.3%Mn) and 0.3 wt%CaO added ECO-AM50 alloys produced by permanent mould casting. The typical microstructure of AM50 alloy was distinctively characterized using two intermetallic compounds, ${\beta}(Mg_{17}Al_{12})$ and $Al_8Mn_5$, along with ${\alpha}$-(Mg) matrix in an as-cast state. The addition of a small amount of CaO played a role in reducing dendrite cell size and quantity of the ${\beta}$ phase in the AM50 alloy. It is interesting to note that the added CaO introduced a small amount of $Al_2Ca$ adjacent to the ${\beta}$ compounds, and that inhomogeneous enrichment of elemental Ca was observed within the ${\beta}$ phase. The ECO-AM50 alloy showed higher hardness and better YS and UTS at room temperature than did the AM50 alloy, which characteristics can be mainly ascribed to the finer-grained microstructure that originated from the CaO addition. At $175^{\circ}C$, higher levels of YS and UTS and higher elongation were obtained for the ECO-AM50 alloy, demonstrating that even 0.3 wt%CaO addition can be beneficial in promoting the heat resistance of the AM50 alloy. The combinational contributions of enhanced thermal stability of the Ca-containing ${\beta}$ phase and the introduction of a stable $Al_2Ca$ phase with high melting point are thought to be responsible for the improvement of the high temperature tensile properties in the ECO-AM50 alloy.